US3381748A - Method for sealing leaks in production packers - Google Patents
Method for sealing leaks in production packers Download PDFInfo
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- US3381748A US3381748A US514264A US51426465A US3381748A US 3381748 A US3381748 A US 3381748A US 514264 A US514264 A US 514264A US 51426465 A US51426465 A US 51426465A US 3381748 A US3381748 A US 3381748A
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- 238000004519 manufacturing process Methods 0.000 title description 19
- 238000000034 method Methods 0.000 title description 18
- 238000007789 sealing Methods 0.000 title description 9
- 239000012530 fluid Substances 0.000 description 52
- 239000000565 sealant Substances 0.000 description 32
- 239000002245 particle Substances 0.000 description 23
- 230000005484 gravity Effects 0.000 description 8
- 239000003921 oil Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 239000004033 plastic Substances 0.000 description 6
- 229920003023 plastic Polymers 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 5
- -1 polyethylene Polymers 0.000 description 5
- 239000004743 Polypropylene Substances 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 239000012267 brine Substances 0.000 description 4
- 229920001971 elastomer Polymers 0.000 description 4
- 238000002347 injection Methods 0.000 description 4
- 239000007924 injection Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 229920000642 polymer Polymers 0.000 description 4
- 229920001155 polypropylene Polymers 0.000 description 4
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 4
- 239000008187 granular material Substances 0.000 description 3
- 239000008119 colloidal silica Substances 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 229920006158 high molecular weight polymer Polymers 0.000 description 2
- 210000002445 nipple Anatomy 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000375 suspending agent Substances 0.000 description 2
- 229920000459 Nitrile rubber Polymers 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 229920002367 Polyisobutene Polymers 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- CEGOLXSVJUTHNZ-UHFFFAOYSA-K aluminium tristearate Chemical compound [Al+3].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CEGOLXSVJUTHNZ-UHFFFAOYSA-K 0.000 description 1
- 229940063655 aluminum stearate Drugs 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- 238000009530 blood pressure measurement Methods 0.000 description 1
- NTXGQCSETZTARF-UHFFFAOYSA-N buta-1,3-diene;prop-2-enenitrile Chemical compound C=CC=C.C=CC#N NTXGQCSETZTARF-UHFFFAOYSA-N 0.000 description 1
- 229920002301 cellulose acetate Polymers 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 239000002283 diesel fuel Substances 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000003129 oil well Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 229920001084 poly(chloroprene) Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920002689 polyvinyl acetate Polymers 0.000 description 1
- 239000011118 polyvinyl acetate Substances 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
- 239000007762 w/o emulsion Substances 0.000 description 1
Images
Classifications
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B33/00—Sealing or packing boreholes or wells
- E21B33/10—Sealing or packing boreholes or wells in the borehole
- E21B33/13—Methods or devices for cementing, for plugging holes, crevices or the like
- E21B33/134—Bridging plugs
Definitions
- ABSTRACT OF THE DKSCLOSURE A method for repairing leaks in a production packer wherein a low density sealant fluid containing particles of an insoluble polymer is forced through the tubing string between two piston-like members until the lowermost member emerges from the lower end of the tubing and at least part of the sealant is displaced into the wellbore beneath the packer.
- the present invention relates to oil and gas wells and is particularly concerned with an improved method for repairing leaks in the tubing strings and production packers used in such wells.
- tubing strings and production packers used in oil and gas wells often develop leaks due to corrosion, sand blasting and excessive pressure. Such leaks are generally repaired by killing the well, withdrawing the tubing string and packer assembly, replacing the faulty components, and then reinstalling the apparatus in the wellbore. This procedure interrupts production for prolonged periods, requires the use of expensive workover equipment which may not be readily available at the well site, and sometimes results in damage to the producing formation by the fluids used to kill the well. These disadvantages are particularly pronounced in deep well and in offshore areas.
- the present invention provides an improved method for sealing leaks in the tubing strings and production packers in oil and gas wells.
- This method involves the injection of a rubber ball or similar piston-like member and a sealant fluid containing graded plastic particles having a specific gravity less than that of Water into the tubing string at the surface, the use of a second piston-like member and a later-injected fluid to force the sealant fluid through the tubing into the space beneath the production packer, and the subsequent removal of the second piston-like member and excess fluid from the tubing string.
- FIGURE 1 is a schematic sectional view of a well showing the injection of a sealant fluid through the tubing;
- FIGURE 2 is a schematic view of the same well following the plugging of a leak around the production packer.
- FIGURE 1 of the drawing contains a string of casing 11 which has been cemented in place in the wellbore and perforated in the usual manner.
- the cement is indicated by reference numeral 12.
- Tubing string 13 extends downwardly through the casing from the earths surface to a point adjacent perforations 14 in producing zone 15.
- a production packer 16 of conventional design is mounted on the tubing string above the producing zone to provide a seal between the tubing and the inner wall of the casing. Pressure measurements made at the surface have indicated that a leak exists in the tubing or production packer and that fluids are escaping from the well into the annulus above the packer. The methods generally used to detect such leaks do not indicate their precise location and hence both the tubing and the packer may be defective.
- the leak in the apparatus of FIGURE 1 is repaired by first preparing a sealant fluid containing graded particles of a high molecular weight polymer which is substantially insoluble in both oil and water.
- Suitable polymers include butadiene-styrene copolymers, butadiene-acrylonitrile copolymers, polychloroprene, isobutylene-diolefin copolymers, polyethylene, polypropylene, polystyrene, cellulose acetate, polyvinyl chloride, polyvinyl acetate, phenolformaldehyde resins and the like. It will be understood that not all of these materials are equally effective for purposes of the invention. It is preferred to employ plastics and resins which have specific gravities less than that of water, although slightly heaver materials can also be used. The use of polypropylene has been found to be particularly effective.
- the plastic solids utilized in accordance with the invention are employed in the form of graded granular particles between about 10 and about 400 Tyler mesh in size. It is preferred to employ granules between about 10 and about 40 mesh in size in a concentration of about 10 to percent, granules between about and about 200 mesh in size in a concentration of about 30 to 56 percent, and granules between about 200 and about 400 mesh in size in a concentration of about 30 to percent.
- the sealant fluid is prepared by suspending the graded polymer particles in crude il, in diesel fuel, heating oil, lubricating oil or a similar petroleum fraction, or in a water-in-oil emulsion in a concentration between about one-half and about three pounds per gallon, preferably between about one and about two pounds per gallon.
- the specific gravity of the total slurry including the suspended particles should be less than that of the water or brine in the well and hence the amount of plastic particles per volume of fluid will depend in part upon the specific gravities of the materials used.
- Polypropylene particles having a specific gravity of about 0.9 give satisfactory results when suspended in SAE 20 to 30 refined oils and can also be used in most crude oils.
- a suspending agent such as blown asphalt, low molecular weight polyisobutylene, aluminum stearate or colloidal silica
- a suspending agent such as blown asphalt, low molecular weight polyisobutylene, aluminum stearate or colloidal silica
- silica flour or similar oil-insoluble colloidal solids also improves the sealing ability of the fluid and is therefore particularly effective.
- Such materials may be used in concentrations between about 0.01 and about 3 percent by weight.
- the sealant fluid is employed for repairing leaks in the tubing and production packer in the well of FIGURE 1 by first venting the annulus between casing 11 and tubing 13 at the earths surface in order to create a differential pressure between the annulus and the interior of the tubing. Assuming that the well is an oil well, rather than a gas well, gas is bled from tubing string 13 at the surface until the string is filled with a column of liquid. A rubber ball or similar piston-like member 18 of sutficient size to plug the tubing and prevent the flow of fluids past it is then inserted into the tubing string through a lubricator or similar device at the earths surface.
- the injection method will depend upon the manner in which the well is completed at the surface and hence is not necessarily restricted to insertion of the ball or similar member through a lubricator.
- a volume of sealant fluid slightly greater than the volume of the annular space between the tubing and casing which extends from the bottom of production packer 16 to the bottom of tubing string 13 is pumped into the tubing string at the surface.
- the column of sealant fluid thus injected into the well is indicated by reference numeral 19 in FIGURE 1.
- a second rubber ball or similar pistonlike member 20 is then inserted into the tubing immediately above the column of sealant fluid.
- the tubing string 13 is opened at the surface and the well is allowed to flow.
- the entry of fluids from the reservoir forces ball 2b to move upwardly through the tubing, swabbing the sealant fluid from the tubing string.
- the ball 20 is removed from the flow line when it reaches the production choke or other restrictions at the surface. Sealant fluid not consumed can be withdrawn into the original container for reuse at a later date. The well may then be returned to normal production.
- ball or similar piston-like member should precede the brine or other fluid so that gas does not rise through this fluid as it traverses the tubing.
- the annulus is then vented, ball 18, sealant fluid 19 and ball 20- are injected into the tubing string, and fluid is then injected behind the second ball to force it downwardly to a point adjacent the end of the tubing.
- the sealant fluid rises into the space beneath the production packer and leaks off through the leak until the particles accumulate in suflicient quantitics to provide an effective plug.
- the invention is not restricted to the particular well arrangement shown in FIGURES l and 2 of the drawing and may be employed in wells containing multiple tubing strings, crossovers, landing nipples and the like.
- the balls utilized can generally be pumped through landing nipples and other restrictions having diameters slightly less than that of the tubing string without difliculty.
- the well can be swabbed to permit their recovery.
- An alternate procedure is to pump in additional fluid so that the balls are forced through the end of the tubing and drop into the bottom of the well. below the producing zone. The sealant fluid can then be recovered, if necessary, by swabbing the tubing string.
- a method for sealing a leak in a production packer within a well containing a string of tubing extending downwardly through said packer and open at its lower end which comprises:
- sealant fluid contains a suspension of polypropylene particles.
- sealant fluid contains said polymer particles in a concentration of from about 1 to 2 pounds per gallon.
- sealant fluid contains a small amount of a suspending agent.
- sealant fluid contains from about 0.01 to about 3 weight percent of colloidal silica.
- Cited polymer particles include particles between about 10 and UNITED STATES PATENTS about 40 mesh in size in a concentration between about 10 to percent, particles between about and about 2,715,943 8/1955 True 166163 200 mesh in size in a concentration between about 30 to 5 2,804,147 8/1957 Pistole et a1. 166-14 percent, and particles between about 200 and about 31 5 5/1967 Watanabe 166 33 400 mesh in size in a concentration between about 30 to 50 percent.
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Geology (AREA)
- Mining & Mineral Resources (AREA)
- Physics & Mathematics (AREA)
- Environmental & Geological Engineering (AREA)
- Fluid Mechanics (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Pipe Accessories (AREA)
- Sealing Material Composition (AREA)
Description
y 1968 B. A. PETERS ETAL 3,381,748
METHOD FOR SEALING LEAKS IN PRODUCTION PACKERS Filed Dec. 16, 1965 :Eg fun'i BELDON A. PETERS, WELDON W. WHITAKER,& INVENTORS WARREN E. HOLLAND BY %MNA) E.
ATTORNEY limited States Patent @flflse 353L748 Patented May 3968 3,381,748 METHOD FOR SEALING LEAKS KN PRODUCTION PACKERS Beldon A. Peters and Weldon W. Whitaker, Houston, and
Warren E. Holland, Kingsville, Tex., assignors to R550 Production Research Company, a corporation of Delaware Filed Dec. 16, 1965, Ser. No. 51 3364 8 (Ilaims. (Cl. 16614) ABSTRACT OF THE DKSCLOSURE A method for repairing leaks in a production packer wherein a low density sealant fluid containing particles of an insoluble polymer is forced through the tubing string between two piston-like members until the lowermost member emerges from the lower end of the tubing and at least part of the sealant is displaced into the wellbore beneath the packer.
The present invention relates to oil and gas wells and is particularly concerned with an improved method for repairing leaks in the tubing strings and production packers used in such wells.
The tubing strings and production packers used in oil and gas wells often develop leaks due to corrosion, sand blasting and excessive pressure. Such leaks are generally repaired by killing the well, withdrawing the tubing string and packer assembly, replacing the faulty components, and then reinstalling the apparatus in the wellbore. This procedure interrupts production for prolonged periods, requires the use of expensive workover equipment which may not be readily available at the well site, and sometimes results in damage to the producing formation by the fluids used to kill the well. These disadvantages are particularly pronounced in deep well and in offshore areas.
The present invention provides an improved method for sealing leaks in the tubing strings and production packers in oil and gas wells. This method involves the injection of a rubber ball or similar piston-like member and a sealant fluid containing graded plastic particles having a specific gravity less than that of Water into the tubing string at the surface, the use of a second piston-like member and a later-injected fluid to force the sealant fluid through the tubing into the space beneath the production packer, and the subsequent removal of the second piston-like member and excess fluid from the tubing string. This provides a simple and inexpensive way of establishing a reliable seal on the high pressure side of a production packer, permits the concomitant sealing of any leaks in the tubing string, and does not preclude the subsequent removal of both the tubing and packer if desired.
The nature and objects of the invention can best be understood by referring to the following detailed description and the accompanying drawing, in which:
FIGURE 1 is a schematic sectional view of a well showing the injection of a sealant fluid through the tubing; and
FIGURE 2 is a schematic view of the same well following the plugging of a leak around the production packer.
The well shown in FIGURE 1 of the drawing contains a string of casing 11 which has been cemented in place in the wellbore and perforated in the usual manner. The cement is indicated by reference numeral 12. Tubing string 13 extends downwardly through the casing from the earths surface to a point adjacent perforations 14 in producing zone 15. A production packer 16 of conventional designis mounted on the tubing string above the producing zone to provide a seal between the tubing and the inner wall of the casing. Pressure measurements made at the surface have indicated that a leak exists in the tubing or production packer and that fluids are escaping from the well into the annulus above the packer. The methods generally used to detect such leaks do not indicate their precise location and hence both the tubing and the packer may be defective.
The leak in the apparatus of FIGURE 1 is repaired by first preparing a sealant fluid containing graded particles of a high molecular weight polymer which is substantially insoluble in both oil and water. Suitable polymers include butadiene-styrene copolymers, butadiene-acrylonitrile copolymers, polychloroprene, isobutylene-diolefin copolymers, polyethylene, polypropylene, polystyrene, cellulose acetate, polyvinyl chloride, polyvinyl acetate, phenolformaldehyde resins and the like. It will be understood that not all of these materials are equally effective for purposes of the invention. It is preferred to employ plastics and resins which have specific gravities less than that of water, although slightly heaver materials can also be used. The use of polypropylene has been found to be particularly effective.
The plastic solids utilized in accordance with the invention are employed in the form of graded granular particles between about 10 and about 400 Tyler mesh in size. It is preferred to employ granules between about 10 and about 40 mesh in size in a concentration of about 10 to percent, granules between about and about 200 mesh in size in a concentration of about 30 to 56 percent, and granules between about 200 and about 400 mesh in size in a concentration of about 30 to percent.
The sealant fluid is prepared by suspending the graded polymer particles in crude il, in diesel fuel, heating oil, lubricating oil or a similar petroleum fraction, or in a water-in-oil emulsion in a concentration between about one-half and about three pounds per gallon, preferably between about one and about two pounds per gallon. The specific gravity of the total slurry including the suspended particles should be less than that of the water or brine in the well and hence the amount of plastic particles per volume of fluid will depend in part upon the specific gravities of the materials used. Polypropylene particles having a specific gravity of about 0.9 give satisfactory results when suspended in SAE 20 to 30 refined oils and can also be used in most crude oils. In some cases, however, the addition of small amounts of a suspending agent such as blown asphalt, low molecular weight polyisobutylene, aluminum stearate or colloidal silica to the oil will improve the suspending properties and result in fluids which can be suspended for indefinite periods without settling of the particles. The addition of silica flour or similar oil-insoluble colloidal solids also improves the sealing ability of the fluid and is therefore particularly effective. Such materials may be used in concentrations between about 0.01 and about 3 percent by weight.
The sealant fluid is employed for repairing leaks in the tubing and production packer in the well of FIGURE 1 by first venting the annulus between casing 11 and tubing 13 at the earths surface in order to create a differential pressure between the annulus and the interior of the tubing. Assuming that the well is an oil well, rather than a gas well, gas is bled from tubing string 13 at the surface until the string is filled with a column of liquid. A rubber ball or similar piston-like member 18 of sutficient size to plug the tubing and prevent the flow of fluids past it is then inserted into the tubing string through a lubricator or similar device at the earths surface. The injection method will depend upon the manner in which the well is completed at the surface and hence is not necessarily restricted to insertion of the ball or similar member through a lubricator. A volume of sealant fluid slightly greater than the volume of the annular space between the tubing and casing which extends from the bottom of production packer 16 to the bottom of tubing string 13 is pumped into the tubing string at the surface. The column of sealant fluid thus injected into the well is indicated by reference numeral 19 in FIGURE 1. A second rubber ball or similar pistonlike member 20 is then inserted into the tubing immediately above the column of sealant fluid. Water, oil or other fluid is pumped into the tubing behind this second ball or similar member in a quantity sufiicient to force the second ball to a po nt just above the bottom of tubing string '13 as shown in FIGURE 2 of the drawing. As the column of sealant fluid between the two balls moves down the tubing, the sealant will tend to escape into any leaks in the tubing and flow into the annulus. The plastic particles suspended in the fluid are carried into the openings and effectively seal them. Wedging of the particles in place and gradual swelling in the presence of oil tend to improve the tightness of the seal. The time required for complete sealing can be determined by pressure and flow drawdown measurements for the tubing-casing annulus.
After pumping the column of sealant fluid through the tubing until the second ball 26 rests a short distance above the lower end of tubing string 13 as indicated in FIGURE 2, the tubing string is closed off at the surface. The first ball 18 has at this point dropped into the bottom of the well below the tubing and is left there. The sealant fluid which. has emerged from the tubing, eing lighter than the water or brine present, rises in the annular space surrounding the tubing below production packer 16. If the packer contains a leak, the sealant fluid escapes through it until the plastic particles bridge the opening. As the particles accumulate beneath the packer as indicated by reference numeral 21 in FIGURE 2, the pressure differential across the leak increases so that the bridged particles are deformed and wedged tightly in place to form an effective seal. Since the particles are deposited on the high pressure side of the packer, they cannot be readily dislodged. If no leak exists in the packer, the sealant fluid remains in the annulus beneath it. Because of the limited volume of sealant fluid employed and the low density, there is little danger of the fluid entering the perforations 14 and damaging the producing formation.
After the leak has been stopped, the tubing string 13 is opened at the surface and the well is allowed to flow. The entry of fluids from the reservoir forces ball 2b to move upwardly through the tubing, swabbing the sealant fluid from the tubing string. The ball 20 is removed from the flow line when it reaches the production choke or other restrictions at the surface. Sealant fluid not consumed can be withdrawn into the original container for reuse at a later date. The well may then be returned to normal production.
The procedure employed in sealing leaks in dry gas wells similar to that described above for wells normally containing salt water beneath the production packer but requires that brine or a similar fluid having a specific gravity greater than that of the sealant fluid be injected into the well in an amount suflicient to fill the gas space below the packer. The fluid employed for this purpose should be one which is compatible with and will not damage the producing formation. As the gas initially present below the packer escapes through the leak, the injected fluid will rise into the space below the packer so that the sealant fluid will then displace it by gravity. A
ball or similar piston-like member should precede the brine or other fluid so that gas does not rise through this fluid as it traverses the tubing. The annulus is then vented, ball 18, sealant fluid 19 and ball 20- are injected into the tubing string, and fluid is then injected behind the second ball to force it downwardly to a point adjacent the end of the tubing. The sealant fluid rises into the space beneath the production packer and leaks off through the leak until the particles accumulate in suflicient quantitics to provide an effective plug.
The invention is not restricted to the particular well arrangement shown in FIGURES l and 2 of the drawing and may be employed in wells containing multiple tubing strings, crossovers, landing nipples and the like. The balls utilized can generally be pumped through landing nipples and other restrictions having diameters slightly less than that of the tubing string without difliculty. In cases where the formation pressure is insuflicient to force the balls back through such restrictions, the well can be swabbed to permit their recovery. An alternate procedure is to pump in additional fluid so that the balls are forced through the end of the tubing and drop into the bottom of the well. below the producing zone. The sealant fluid can then be recovered, if necessary, by swabbing the tubing string.
What is claimed is: r
1. A method for sealing a leak in a production packer within a well containing a string of tubing extending downwardly through said packer and open at its lower end which comprises:
(a) injecting a first piston-like member into said string of tubing at the earths surface;
(b) injecting an oil-containing sealant fluid having graded particles of an oiland water-insoluble high molecular weight polymer between about 10 mesh and about 400 mesh in size suspended therein into said string of tubing behind said first piston-1ike member, said sealant fluid including the suspended particles having a specific gravity less than that of the water in said well and the volume of sealant fluid injected being slightly in excess of the volume of the annular space between the bottom of said production packer and the bottom of the tubing;
(0) injecting a second piston-like member into said string of tubing above said sealant fluid;
(d) pumping fluid into said string of tubing behind said second piston-like member until said first piston-like member has emerged from the lower end of the tubing, said second member has been displaced downwardly in said string of tubing to a point near the bottom of the tubing, and at least part of said sealant fluid has been displaced into the wellbore beneath said packer; and,
(e) thereafter backfiowing said well.
2. A method as defined by claim 1 wherein said sealant fluid contains a suspension of polypropylene particles.
3. A method as defined by claim 1 wherein a fluid compatible with the producing formation is injected into said well through said string of tubing prior to the injection of said first piston-like member.
4. A method as defined by claim 1 wherein said sealant fluid contains said polymer particles in a concentration of from about 1 to 2 pounds per gallon.
5. A method as defined by claim 1 wherein said first and second piston-like members are rubber balls.
6. A method as defined by claim 1 wherein said sealant fluid contains a small amount of a suspending agent.
7. A method as defined by claim 1 wherein said sealant fluid contains from about 0.01 to about 3 weight percent of colloidal silica.
6 8. A method as defined by claim 1 wherein said References Cited polymer particles include particles between about 10 and UNITED STATES PATENTS about 40 mesh in size in a concentration between about 10 to percent, particles between about and about 2,715,943 8/1955 True 166163 200 mesh in size in a concentration between about 30 to 5 2,804,147 8/1957 Pistole et a1. 166-14 percent, and particles between about 200 and about 31 5 5/1967 Watanabe 166 33 400 mesh in size in a concentration between about 30 to 50 percent. JAMES A. LEPPINK, Primary Examiner.
Priority Applications (1)
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US514264A US3381748A (en) | 1965-12-16 | 1965-12-16 | Method for sealing leaks in production packers |
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US514264A US3381748A (en) | 1965-12-16 | 1965-12-16 | Method for sealing leaks in production packers |
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US4869321A (en) * | 1989-02-10 | 1989-09-26 | Camco, Incorporated | Method of plugging openings in well conduits |
US20090071650A1 (en) * | 2005-09-09 | 2009-03-19 | Roddy Craig W | Foamed cement compositions comprising oil-swellable particles and methods of use |
US20100025039A1 (en) * | 2007-05-10 | 2010-02-04 | Halliburton Energy Services, Inc. | Cement Compositions and Methods Utilizing Nano-Clay |
US8476203B2 (en) | 2007-05-10 | 2013-07-02 | Halliburton Energy Services, Inc. | Cement compositions comprising sub-micron alumina and associated methods |
US8685903B2 (en) | 2007-05-10 | 2014-04-01 | Halliburton Energy Services, Inc. | Lost circulation compositions and associated methods |
US9199879B2 (en) | 2007-05-10 | 2015-12-01 | Halliburton Energy Serives, Inc. | Well treatment compositions and methods utilizing nano-particles |
US9206344B2 (en) | 2007-05-10 | 2015-12-08 | Halliburton Energy Services, Inc. | Sealant compositions and methods utilizing nano-particles |
US9512352B2 (en) | 2007-05-10 | 2016-12-06 | Halliburton Energy Services, Inc. | Well treatment fluids and methods utilizing nano-particles |
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