US2474617A - Manufacture of artificial fibers - Google Patents
Manufacture of artificial fibers Download PDFInfo
- Publication number
- US2474617A US2474617A US720099A US72009947A US2474617A US 2474617 A US2474617 A US 2474617A US 720099 A US720099 A US 720099A US 72009947 A US72009947 A US 72009947A US 2474617 A US2474617 A US 2474617A
- Authority
- US
- United States
- Prior art keywords
- yarn
- wind
- filaments
- bath
- tension
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004519 manufacturing process Methods 0.000 title description 3
- 229920002994 synthetic fiber Polymers 0.000 title 1
- 229920000642 polymer Polymers 0.000 description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 23
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 20
- 239000005977 Ethylene Substances 0.000 description 20
- 230000001112 coagulating effect Effects 0.000 description 19
- 239000000835 fiber Substances 0.000 description 18
- 238000000034 method Methods 0.000 description 14
- 239000007864 aqueous solution Substances 0.000 description 13
- 150000003839 salts Chemical class 0.000 description 13
- 239000004372 Polyvinyl alcohol Substances 0.000 description 12
- 235000019422 polyvinyl alcohol Nutrition 0.000 description 12
- 229920002451 polyvinyl alcohol Polymers 0.000 description 12
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 9
- 238000001035 drying Methods 0.000 description 9
- 238000005406 washing Methods 0.000 description 9
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 8
- 238000009987 spinning Methods 0.000 description 8
- 230000002093 peripheral effect Effects 0.000 description 7
- 239000000243 solution Substances 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- 229920001567 vinyl ester resin Polymers 0.000 description 5
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 230000001476 alcoholic effect Effects 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- 229910017053 inorganic salt Inorganic materials 0.000 description 3
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 3
- 235000019341 magnesium sulphate Nutrition 0.000 description 3
- 229920001290 polyvinyl ester Polymers 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- 230000035945 sensitivity Effects 0.000 description 3
- 239000004094 surface-active agent Substances 0.000 description 3
- 229920002554 vinyl polymer Polymers 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 2
- 238000010936 aqueous wash Methods 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 2
- 238000004804 winding Methods 0.000 description 2
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 1
- BAUHCOVJMSUSOW-UHFFFAOYSA-M 1,2,3-trimethylpyridin-1-ium bromide Chemical compound [Br-].Cc1ccc[n+](C)c1C BAUHCOVJMSUSOW-UHFFFAOYSA-M 0.000 description 1
- OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 241000899771 Arenga undulatifolia Species 0.000 description 1
- 241000969130 Atthis Species 0.000 description 1
- 241001589086 Bellapiscis medius Species 0.000 description 1
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- IMROMDMJAWUWLK-UHFFFAOYSA-N Ethenol Chemical compound OC=C IMROMDMJAWUWLK-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 229920000297 Rayon Polymers 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 description 1
- 125000003158 alcohol group Chemical group 0.000 description 1
- -1 aliphatic alcohols Chemical class 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 239000002152 aqueous-organic solution Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000009954 braiding Methods 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-M dihydrogenphosphate Chemical compound OP(O)([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-M 0.000 description 1
- 238000000578 dry spinning Methods 0.000 description 1
- 238000010292 electrical insulation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- XUCNUKMRBVNAPB-UHFFFAOYSA-N fluoroethene Chemical compound FC=C XUCNUKMRBVNAPB-UHFFFAOYSA-N 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 230000000266 injurious effect Effects 0.000 description 1
- 150000002762 monocarboxylic acid derivatives Chemical class 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000003791 organic solvent mixture Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920002689 polyvinyl acetate Polymers 0.000 description 1
- 239000011118 polyvinyl acetate Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000002040 relaxant effect Effects 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical group [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 238000002166 wet spinning Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/02—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F6/14—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds from polymers of unsaturated alcohols, e.g. polyvinyl alcohol, or of their acetals or ketals
Definitions
- Filaments have been prepared by the dry-spinning of aqueous solutions such asby the rapid evaporation of the aqueous solvent when a fine stream of the aqueous polymer solution is injected into a heated chamber.
- wet spinning of aqueous solutions is preferable. This involves injecting an aqueous solution of the polymer into a coagulating bath.
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Artificial Filaments (AREA)
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE479037D BE479037A (fr) | 1947-01-03 | ||
| FR957835D FR957835A (fr) | 1947-01-03 | ||
| US720099A US2474617A (en) | 1947-01-03 | 1947-01-03 | Manufacture of artificial fibers |
| GB114/48A GB656467A (en) | 1947-01-03 | 1948-01-02 | Manufacture of artificial fibres |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US720099A US2474617A (en) | 1947-01-03 | 1947-01-03 | Manufacture of artificial fibers |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US2474617A true US2474617A (en) | 1949-06-28 |
Family
ID=24892633
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US720099A Expired - Lifetime US2474617A (en) | 1947-01-03 | 1947-01-03 | Manufacture of artificial fibers |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US2474617A (fr) |
| BE (1) | BE479037A (fr) |
| FR (1) | FR957835A (fr) |
| GB (1) | GB656467A (fr) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2599494A (en) * | 1947-08-09 | 1952-06-03 | Du Pont | Photographic emulsions |
| US2994576A (en) * | 1954-09-09 | 1961-08-01 | Celanese Corp | Process for spinning polyvinyl alcohol filaments and remaining impurities therefrom |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB482216A (en) * | 1936-09-30 | 1938-03-25 | William Alexander Dickie | Improvements in the manufacture of artificial filaments, films and similar materials |
| US2146295A (en) * | 1931-03-10 | 1939-02-07 | Chemische Forschungs Gmbh | Polymerized vinyl alcohol articles and process of making same |
| US2190265A (en) * | 1931-10-19 | 1940-02-13 | Ig Farbenindustrie Ag | Spinning artificial threads |
| US2236061A (en) * | 1937-05-27 | 1941-03-25 | Du Pont | Method of making films, threads, and the like |
| US2322976A (en) * | 1939-11-03 | 1943-06-29 | Schmitz Hilger Peter | Method of producing thin threads from polyvinyl alcohol and its water-soluble derivatives |
| US2388325A (en) * | 1944-03-04 | 1945-11-06 | Du Pont | Spinning process for artificial filaments |
-
0
- BE BE479037D patent/BE479037A/xx unknown
- FR FR957835D patent/FR957835A/fr not_active Expired
-
1947
- 1947-01-03 US US720099A patent/US2474617A/en not_active Expired - Lifetime
-
1948
- 1948-01-02 GB GB114/48A patent/GB656467A/en not_active Expired
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2146295A (en) * | 1931-03-10 | 1939-02-07 | Chemische Forschungs Gmbh | Polymerized vinyl alcohol articles and process of making same |
| US2190265A (en) * | 1931-10-19 | 1940-02-13 | Ig Farbenindustrie Ag | Spinning artificial threads |
| GB482216A (en) * | 1936-09-30 | 1938-03-25 | William Alexander Dickie | Improvements in the manufacture of artificial filaments, films and similar materials |
| US2236061A (en) * | 1937-05-27 | 1941-03-25 | Du Pont | Method of making films, threads, and the like |
| US2322976A (en) * | 1939-11-03 | 1943-06-29 | Schmitz Hilger Peter | Method of producing thin threads from polyvinyl alcohol and its water-soluble derivatives |
| US2388325A (en) * | 1944-03-04 | 1945-11-06 | Du Pont | Spinning process for artificial filaments |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2599494A (en) * | 1947-08-09 | 1952-06-03 | Du Pont | Photographic emulsions |
| US2994576A (en) * | 1954-09-09 | 1961-08-01 | Celanese Corp | Process for spinning polyvinyl alcohol filaments and remaining impurities therefrom |
Also Published As
| Publication number | Publication date |
|---|---|
| FR957835A (fr) | 1950-02-25 |
| BE479037A (fr) | |
| GB656467A (en) | 1951-08-22 |
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