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US2298908A - Powdered metal - Google Patents

Powdered metal Download PDF

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Publication number
US2298908A
US2298908A US372435A US37243540A US2298908A US 2298908 A US2298908 A US 2298908A US 372435 A US372435 A US 372435A US 37243540 A US37243540 A US 37243540A US 2298908 A US2298908 A US 2298908A
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US
United States
Prior art keywords
particles
metal
spongy
lubricant
powdered metal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US372435A
Inventor
Wentworth Chandler
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RCA Corp
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RCA Corp
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Publication date
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Priority to US372435A priority Critical patent/US2298908A/en
Application granted granted Critical
Publication of US2298908A publication Critical patent/US2298908A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/01Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
    • H01F1/03Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
    • H01F1/12Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials
    • H01F1/14Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys
    • H01F1/20Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of particles, e.g. powder
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S264/00Plastic and nonmetallic article shaping or treating: processes
    • Y10S264/50Use of fluid pressure in molding
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S425/00Plastic article or earthenware shaping or treating: apparatus
    • Y10S425/019Flexible fluid pressure
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S425/00Plastic article or earthenware shaping or treating: apparatus
    • Y10S425/044Rubber mold

Definitions

  • This invention relates to the treatment of socalled powdered metal, particularly spongy paramagnetic particles, such, for example, as comminuted..S wedish iron, and to the manufacture of cores andduher structures from such materials.
  • an object of the present invention is to provide paramagnetic particles of a density greater than that obtaining in the natural or 1.111.- treated but otherwise similar spongy metal particles.
  • a related object of the invention is to provide an improved and economical method of compressing and permanently increasing the density of the individual particles, and one which, in its practice, obviates the danger of sintering the metal.
  • Previous attempts to increase the density of such materials by compression have not been altogether satisfactory principally because of the tendency of the particles to lose their identity and to form a coherent permanently solid mass, as if sintered. This difficulty is obviated in accordance with the invention by lubricating the metal particles prior to their compression and, when necessary or desirable, subsequently rern0v ing the lubricant.
  • spongy iron particles which will pass through the mesh of sieve having 300 or more openings per square inch and to thoroughly mix a batch of the particles with common motor oil or other inorganic or organic lubricant, such, for example, as
  • Thecontents of the bag may then be dumped into a solvent (e. g., gasoline) bath to remove the lubricant, since the presence of the lubricant may be objectionable in any substantial quantity in magnetic structures of the general character described.
  • a solvent e. g., gasoline
  • the washed and dried compressed particles may be molded in any desired form in accordance with the usual procedure and percentages of insulating materials.
  • the 'increase in the factor of merit of such structures may be of the order of twenty-five per cent.
  • Method of treating comminuted spongy metal which comprises coating the spongy metal particles with a material which will prevent sintering of the particles when subjected to a com pressive force, and thereafter applying to said coated particles a compressive force in substantially all directions and of an intensity sufiicient to reduce the size of said particles.
  • Method of decreasing the particle size of comminuted spongy iron comprismfanhit l'i lfi lwillowmm] vnryctuhlc oil, etc. inn lubricuthm tllu :utid HlmnHy particles mm m subjecting them to a compression force applied substantially in all directions.
  • Method of making a structure of coml0 minuted spongy paramagnetic spongy particles comprising lubricating said particles, subjecting said lubricated particles to a compression force applied in substantially all directions and of an intensity suificient to reduce their particle size, removing the lubricant and thereafter molding said particles together with a suitable insulating material in the form of the structure desired.

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  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Power Engineering (AREA)
  • Powder Metallurgy (AREA)
  • Soft Magnetic Materials (AREA)

Description

Search Room 1942- c. WENTWORTH 2,298,908
PQWDERED METAL I Filed Dec. 31, 1940 I I v,1 IIIIIIIIIIIII Inventor Chandler l/ l ntworth attorney Patented st. 1135, 19422 nits.
POWDER/ED METAL Application-December 31, 1940, Serial No. 372,435
6 Claims.
This invention relates to the treatment of socalled powdered metal, particularly spongy paramagnetic particles, such, for example, as comminuted..S wedish iron, and to the manufacture of cores andduher structures from such materials.
It will be appreciated by those skilled in the art of molding coherent structures from paramagnetic particles mixed or coated with insulating materials that the more dense the individual metal particles, the smaller the stroke required in the molding operation. The smaller the molding stroke, the better the electrical characteristics of the finished product. This is so because the friction between the particles during the molding operation is lowered and, as a consequence, there is less likelihood of puncturing or otherwise damaging the insulation which must necessarily be present between the individual metallic particles in the finished structure.
Accordingly, an object of the present invention is to provide paramagnetic particles of a density greater than that obtaining in the natural or 1.111.- treated but otherwise similar spongy metal particles.
A related object of the invention is to provide an improved and economical method of compressing and permanently increasing the density of the individual particles, and one which, in its practice, obviates the danger of sintering the metal.
Certain metals, in particle size, e. g., Swedish spongy iron, are ductile, not friable, and hence when subjected to a compression force of considerable intensity, may be compressed and rendered of permanently increased .density. Previous attempts to increase the density of such materials by compression have not been altogether satisfactory principally because of the tendency of the particles to lose their identity and to form a coherent permanently solid mass, as if sintered. This difficulty is obviated in accordance with the invention by lubricating the metal particles prior to their compression and, when necessary or desirable, subsequently rern0v ing the lubricant.
In utilizing the invention in the production of cores and other magnetic structures for use in signaling apparatus it is preferable to start with spongy iron particles which will pass through the mesh of sieve having 300 or more openings per square inch and to thoroughly mix a batch of the particles with common motor oil or other inorganic or organic lubricant, such, for example, as
Only suiflcient lubricant to thoroughly coat the particles need be employed in the mix. The coated particles are then subjected to a compression force of the order of one hundred tons per square inch either in an ordinary piston or plunger type mold or in one operating on the hydraulic principle, such, for example, as the one shown in the drawing. In this latter case the batch may be enclosed in a bag 2 formed of synthetic rubber, or other strong material, which is immune to the oil and the bag placed in a tank 4 having a tightly sealed cap 6 and port 8 for the admission of the hydraulic fluid. The fluid pumped into the mold exerts its compression force equally in all directions upon the bag containing the lubricated metal particles and com-- presses the individual particles so that they are rendered smaller and more dense. At the indicated pressure, the reduction in bulk and in particle size will be of the order of twenty-five percent. The lubricant permits the particles to change their shape and slide one against another but prevents them from adhering together.
Thecontents of the bag may then be dumped into a solvent (e. g., gasoline) bath to remove the lubricant, since the presence of the lubricant may be objectionable in any substantial quantity in magnetic structures of the general character described. The washed and dried compressed particles may be molded in any desired form in accordance with the usual procedure and percentages of insulating materials.
Cores and other magnetic structures formed of comminuted metals which have been compressed and densified in accordance with the invention exhibit higher permeability and lower eddy current losses than those formed of untreated but otherwise similar metals. The 'increase in the factor of merit of such structures may be of the order of twenty-five per cent.
What is claimed is:
1. Method of treating comminuted spongy metal which comprises coating the spongy metal particles with a material which will prevent sintering of the particles when subjected to a com pressive force, and thereafter applying to said coated particles a compressive force in substantially all directions and of an intensity sufiicient to reduce the size of said particles.
2. Method in accordance with claim 1 and wherein said coating comprises a lubricating material.
3. Method of decreasing the particle size of comminuted spongy iron, said method comprismfanhit l'i lfi lwillowmm] vnryctuhlc oil, etc. inn lubricuthm tllu :utid HlmnHy particles mm m subjecting them to a compression force applied substantially in all directions.
4. Method in accordance with claim 3 and wherein said lubricant comprises a petroleum product.
5. Method in accordance with claim 3 and wherein said lubricated particles are subjected to a compression force of the order of one hundred ton s per square inch.
'15. Method of making a structure of coml0 minuted spongy paramagnetic spongy particles, said method comprising lubricating said particles, subjecting said lubricated particles to a compression force applied in substantially all directions and of an intensity suificient to reduce their particle size, removing the lubricant and thereafter molding said particles together with a suitable insulating material in the form of the structure desired.
CHANDLER \VENTWORTH.
US372435A 1940-12-31 1940-12-31 Powdered metal Expired - Lifetime US2298908A (en)

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Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2431690A (en) * 1945-02-21 1947-12-02 Westinghouse Electric Corp Consolidation of metal powder
US2464517A (en) * 1943-05-13 1949-03-15 Callite Tungsten Corp Method of making porous metallic bodies
US2478037A (en) * 1944-09-02 1949-08-02 Joseph B Brennan Method of applying a silver layer to a steel bearing blank
US2725288A (en) * 1952-08-26 1955-11-29 Harry W Dodds Process and apparatus for fabricating metallic articles
US2783504A (en) * 1953-05-06 1957-03-05 Utica Drop Forge & Tool Corp Method of forming articles from comminuted material
DE958261C (en) * 1943-10-08 1957-03-21 Deutsche Edelstahlwerke Ag Device for pressing powdery substances
US2823419A (en) * 1952-03-14 1958-02-18 Fansteel Metallurgical Corp Machine for pressing tantalum capacitor elements
US3044113A (en) * 1959-01-08 1962-07-17 Engineering Supervision Compan Super-high pressure apparatus
US3089189A (en) * 1959-08-07 1963-05-14 Westinghouse Electric Corp Apparatus and process for forming high density compacts
US3269826A (en) * 1963-10-08 1966-08-30 Du Pont Compaction of finely divided metals
US3539472A (en) * 1966-12-23 1970-11-10 Hoechst Ag Process for molding articles from metal powders
US3850557A (en) * 1972-12-05 1974-11-26 Asea Ab Container for manufacturing sintered products
US3939241A (en) * 1974-10-04 1976-02-17 Crucible Inc. Method for powder metallurgy compacting
US4000235A (en) * 1975-05-13 1976-12-28 National Forge Company Method for molding particulate material into rods
US4370294A (en) * 1981-01-05 1983-01-25 Western Electric Co., Inc. Compacting particulate material into a body
US4395219A (en) * 1981-01-05 1983-07-26 Western Electric Co., Inc. Apparatus for forming compactible material into a body

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2464517A (en) * 1943-05-13 1949-03-15 Callite Tungsten Corp Method of making porous metallic bodies
DE958261C (en) * 1943-10-08 1957-03-21 Deutsche Edelstahlwerke Ag Device for pressing powdery substances
US2478037A (en) * 1944-09-02 1949-08-02 Joseph B Brennan Method of applying a silver layer to a steel bearing blank
US2431690A (en) * 1945-02-21 1947-12-02 Westinghouse Electric Corp Consolidation of metal powder
US2823419A (en) * 1952-03-14 1958-02-18 Fansteel Metallurgical Corp Machine for pressing tantalum capacitor elements
US2725288A (en) * 1952-08-26 1955-11-29 Harry W Dodds Process and apparatus for fabricating metallic articles
US2783504A (en) * 1953-05-06 1957-03-05 Utica Drop Forge & Tool Corp Method of forming articles from comminuted material
US3044113A (en) * 1959-01-08 1962-07-17 Engineering Supervision Compan Super-high pressure apparatus
US3089189A (en) * 1959-08-07 1963-05-14 Westinghouse Electric Corp Apparatus and process for forming high density compacts
US3269826A (en) * 1963-10-08 1966-08-30 Du Pont Compaction of finely divided metals
US3539472A (en) * 1966-12-23 1970-11-10 Hoechst Ag Process for molding articles from metal powders
US3850557A (en) * 1972-12-05 1974-11-26 Asea Ab Container for manufacturing sintered products
US3939241A (en) * 1974-10-04 1976-02-17 Crucible Inc. Method for powder metallurgy compacting
US4000235A (en) * 1975-05-13 1976-12-28 National Forge Company Method for molding particulate material into rods
US4370294A (en) * 1981-01-05 1983-01-25 Western Electric Co., Inc. Compacting particulate material into a body
US4395219A (en) * 1981-01-05 1983-07-26 Western Electric Co., Inc. Apparatus for forming compactible material into a body

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