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US20120211015A1 - Application of neophytadiene as an additive for liquid cigarettes - Google Patents

Application of neophytadiene as an additive for liquid cigarettes Download PDF

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Publication number
US20120211015A1
US20120211015A1 US13/330,505 US201113330505A US2012211015A1 US 20120211015 A1 US20120211015 A1 US 20120211015A1 US 201113330505 A US201113330505 A US 201113330505A US 2012211015 A1 US2012211015 A1 US 2012211015A1
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United States
Prior art keywords
neophytadiene
liquid
weight percent
additive
cigarettes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
US13/330,505
Inventor
Wenbo Li
Lik Hon
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Fontem Ventures BV
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Individual
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Filing date
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Assigned to RUYAN INVESTMENT (HOLDINGS) LIMITED reassignment RUYAN INVESTMENT (HOLDINGS) LIMITED ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: HON, LIK, LI, WENBO
Publication of US20120211015A1 publication Critical patent/US20120211015A1/en
Assigned to FONTEM HOLDINGS 1 B.V. reassignment FONTEM HOLDINGS 1 B.V. ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: RUYAN INVESTMENT (HOLDINGS) LIMITED
Abandoned legal-status Critical Current

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Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/12—Alkadienes

Definitions

  • the present invention relates to evaporation in liquid cigarettes or additive for atomizing cigarettes, and particularly to applications of neophytadiene as an additive for liquid cigarettes.
  • sucking devices are known as cigarette substitutes and being useful for smoking cessation.
  • One of them includes a porous body having a relatively large surface area retaining a liquid mixture of various components, which has a smell of cigarette.
  • the other kind of sucking device places the liquid in an atomizing electronic cigarette, which vaporizes the liquid by an atomizer and provide the generated vapor to the user, so as to simulate functions of a regular cigarette.
  • an important disadvantage of such devices is that they cannot simulate the taste and smell of regular cigarettes.
  • the present invention discloses an application of neophytadiene as an additive for liquid cigarettes.
  • Neophytadiene is used as an additive for liquid cigarettes.
  • Neophytadiene is a diterpenoid compound and is liquid at room temperature.
  • the molecular weight of the neophytadiene is 278.52
  • its molecular formula is C 20 H 38
  • its structural formula is:
  • Such a liquid cigarette contains atomizing liquid and neophytadiene, specifically, 25 ⁇ 99.9% weight percent atomizing liquid and 0.01 ⁇ 75% weight percent neophytadiene.
  • the atomizing liquid contains 60 ⁇ 95% weight percent propylene glycol, 1 ⁇ 30% weight percent glycerin, the rest contains flavoring essence, water and ethanol.
  • the 0.01 ⁇ 20% addition of neophytadiene can generate smell of a cigarette.
  • the 20 ⁇ 75% addition of neophytadiene can speed up the atomization.
  • neophytadiene is used as an additive for liquid cigarettes, so as to improve the taste of the inhaled gas or vapor, to make them have a smell of a regular cigarette.
  • the addition of neophytadiene facilitates the transformation of the liquid into gas, especially the vaporization in a liquid cigarette, by speeding up the atomization, so as to save electric power for batteries.
  • the 0.01 ⁇ 20% neophytadiene addition in liquid cigarettes can improve the taste of the inhaled gas or vapor to have a smell of regular cigarettes; 20 ⁇ 75% neophytadiene addition can speed up the volatilization of the liquid into gas.
  • Neophytadiene exists widely in tobaccos, and is one of the components of cigarette combustion smoke. Neophytadiene is almost odorless and has a smell of cerolipoid which is adverse to the smell of the smoke. Neophytadiene is a diterpenoid compound and is liquid at room temperature. The molecular weight of the neophytadiene is 278.52, and its molecular formula is C 20 H 38.
  • Neophytadiene can be extracted from tobacco leaves, tobacco stems and wastes, or generated by dehydration of phytol.
  • a Chlorophyll molecule comprises two parts, a polar porphyrin head (N has a part of negative charges, Mg has a part of positive charges) and an apolar phytol tail.
  • Chlorophyll is hydrolyzed under an alkaline condition to generate phytol (C 20 H 39 OH):
  • phytol Under the catalytic action and dehydration action of concentrated sulfuric acid, phytol is heated to 170° C., an elimination reaction happens and then generates neophytadiene (C 20 H 38 ).
  • the generated neophytadiene is used as an additive for liquid cigarettes. It is formed by adding 0.01 ⁇ 75% neophytadiene into conventional atomizing liquid; the conventional liquid typically contains 60 ⁇ 95% weight percent propylene glycol, 1 ⁇ 30% weight percent glycerin, the rest contains flavoring essence, water and ethanol.
  • the liquid cigarette contains atomizing liquid and neophytadiene, specifically, 25 ⁇ 99.9% weight percent atomizing liquid and 0.01 ⁇ 75% weight percent neophytadiene.
  • the 0.01 ⁇ 20% neophytadiene addition in liquid cigarettes can improve the taste of the inhaled gas or vapor to have a smell of regular cigarettes.
  • the 20 ⁇ 75% neophytadiene addition can speed up the volatilization of the liquid into gas.
  • Adding 0.01 ⁇ 3% weight percent neophytadiene into conventional atomizing liquid as a liquid cigarette additive can generate smell of cigarettes, and improve the taste of inhaled gas or vapor, so as to provide it with smell of regular cigarettes.
  • Adding 20 ⁇ 75% weight percent neophytadiene into conventional atomizing liquid as a liquid cigarette additive can speed up the vaporization of the liquid, increase the speed of the liquid's volatilization to become gas.
  • Adding 3 ⁇ 10% weight percent neophytadiene into conventional atomizing liquid as a liquid cigarette additive can generate smell of cigarettes, and improve the taste of inhaled gas or vapor, so as to provide it with smell of regular cigarettes.
  • Adding 50 ⁇ 70% weight percent neophytadiene into conventional atomizing liquid as a liquid cigarette additive can speed up the vaporization of the liquid, increase the speed of the liquid's volatilization to become gas.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Organic Chemistry (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Fats And Perfumes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

Neophytadiene used as additive for liquid cigarette can improve aroma and evaporation rate thereof. The liquid cigarette is composed of from 25 to 99.9% by weight percentage of atomized liquid and from 0.01 to 75% by weight percentage of neophytadiene.

Description

    CROSS REFERENCE TO RELATED APPLICATIONS
  • This application is a continuation of International Application No. PCT/CN2010/073621, filed Jun. 7, 2010 and designating the U.S., which claims priority to Chinese Patent Application No. 200910012125.5, filed Jun. 19, 2009, both of which are incorporated herein by reference in their entirety.
    • TECHNICAL FIELD
  • The present invention relates to evaporation in liquid cigarettes or additive for atomizing cigarettes, and particularly to applications of neophytadiene as an additive for liquid cigarettes.
    • BACKGROUND
  • Presently, two kinds of sucking devices are known as cigarette substitutes and being useful for smoking cessation. One of them includes a porous body having a relatively large surface area retaining a liquid mixture of various components, which has a smell of cigarette. When inhaled air flows through the porous body, a good deal of liquid is vaporized and mixed with the air so as to provide satisfaction to the smoker; the other kind of sucking device places the liquid in an atomizing electronic cigarette, which vaporizes the liquid by an atomizer and provide the generated vapor to the user, so as to simulate functions of a regular cigarette. However, an important disadvantage of such devices is that they cannot simulate the taste and smell of regular cigarettes.
    • SUMMARY OF THE INVENTION
  • To overcome the disadvantage of the arts, the present invention discloses an application of neophytadiene as an additive for liquid cigarettes.
  • In order to achieve the objects above, in a technology according to the present invention:
  • Neophytadiene is used as an additive for liquid cigarettes. Neophytadiene is a diterpenoid compound and is liquid at room temperature. The molecular weight of the neophytadiene is 278.52, its molecular formula is C20H38, and its structural formula is:
  • Figure US20120211015A1-20120823-C00001
  • Such a liquid cigarette contains atomizing liquid and neophytadiene, specifically, 25˜99.9% weight percent atomizing liquid and 0.01˜75% weight percent neophytadiene. The atomizing liquid contains 60˜95% weight percent propylene glycol, 1˜30% weight percent glycerin, the rest contains flavoring essence, water and ethanol. The 0.01˜20% addition of neophytadiene can generate smell of a cigarette. The 20˜75% addition of neophytadiene can speed up the atomization.
  • Advantages of the present invention include:
  • 1. In the present invention, neophytadiene is used as an additive for liquid cigarettes, so as to improve the taste of the inhaled gas or vapor, to make them have a smell of a regular cigarette.
  • 2. In the present invention, the addition of neophytadiene facilitates the transformation of the liquid into gas, especially the vaporization in a liquid cigarette, by speeding up the atomization, so as to save electric power for batteries.
  • 3. The 0.01˜20% neophytadiene addition in liquid cigarettes can improve the taste of the inhaled gas or vapor to have a smell of regular cigarettes; 20˜75% neophytadiene addition can speed up the volatilization of the liquid into gas.
  • Neophytadiene exists widely in tobaccos, and is one of the components of cigarette combustion smoke. Neophytadiene is almost odorless and has a smell of cerolipoid which is adverse to the smell of the smoke. Neophytadiene is a diterpenoid compound and is liquid at room temperature. The molecular weight of the neophytadiene is 278.52, and its molecular formula is C20H38.
    • DETAIL EMBODIMENT OF THE INVENTION
  • Neophytadiene can be extracted from tobacco leaves, tobacco stems and wastes, or generated by dehydration of phytol.
  • Specifically, a method for preparing neophytadiene:
  • Figure US20120211015A1-20120823-C00002
    • Chlorophyll
  • A Chlorophyll molecule comprises two parts, a polar porphyrin head (N has a part of negative charges, Mg has a part of positive charges) and an apolar phytol tail.
  • Chlorophyll is hydrolyzed under an alkaline condition to generate phytol (C20H39OH):
  • C55H72O5N4Mg+2KOH →CH3OH+C20H39OH+C34H30O5N4MgK2
  • Under the catalytic action and dehydration action of concentrated sulfuric acid, phytol is heated to 170° C., an elimination reaction happens and then generates neophytadiene (C20H38).
  • The generated neophytadiene is used as an additive for liquid cigarettes. It is formed by adding 0.01˜75% neophytadiene into conventional atomizing liquid; the conventional liquid typically contains 60˜95% weight percent propylene glycol, 1˜30% weight percent glycerin, the rest contains flavoring essence, water and ethanol.
  • The liquid cigarette contains atomizing liquid and neophytadiene, specifically, 25˜99.9% weight percent atomizing liquid and 0.01˜75% weight percent neophytadiene.
  • The 0.01˜20% neophytadiene addition in liquid cigarettes can improve the taste of the inhaled gas or vapor to have a smell of regular cigarettes.
  • The 20˜75% neophytadiene addition can speed up the volatilization of the liquid into gas.
    • Embodiment 2
  • Adding 0.01˜3% weight percent neophytadiene into conventional atomizing liquid as a liquid cigarette additive can generate smell of cigarettes, and improve the taste of inhaled gas or vapor, so as to provide it with smell of regular cigarettes.
  • Adding 20˜75% weight percent neophytadiene into conventional atomizing liquid as a liquid cigarette additive can speed up the vaporization of the liquid, increase the speed of the liquid's volatilization to become gas.
    • Embodiment 3
  • Adding 3˜10% weight percent neophytadiene into conventional atomizing liquid as a liquid cigarette additive can generate smell of cigarettes, and improve the taste of inhaled gas or vapor, so as to provide it with smell of regular cigarettes.
  • Adding 50˜70% weight percent neophytadiene into conventional atomizing liquid as a liquid cigarette additive can speed up the vaporization of the liquid, increase the speed of the liquid's volatilization to become gas.

Claims (6)

1. A method to improve a liquid cigarette, comprising:
adding neophytadiene as an additive for a liquid cigarette.
2. The method of claim 1, wherein neophytadiene is a diterpenoid compound and is liquid at room temperature, the molecular weight of neophytadiene is 278.52, the molecular formula of neophytadiene is C20H38, and the structural formula of neophytadiene is:
Figure US20120211015A1-20120823-C00003
3. The method of claim 1, wherein the liquid cigarette comprises 25˜99.9% weight percent atomizing liquid and 0.01˜75% weight percent neophytadiene.
4. The method of claim 3, wherein the atomizing liquid contains 60˜95% weight percent propylene glycol, 1˜30% weight percent glycerin, and the rest contains flavoring essence, water and ethanol.
5. The method of claim 3, wherein an addition of 0.01˜20% neophytadiene generates a smell of cigarettes.
6. The method of claim 3, wherein an addition of 20˜75% neophytadiene increases a speed of vaporization.
US13/330,505 2009-06-19 2011-12-19 Application of neophytadiene as an additive for liquid cigarettes Abandoned US20120211015A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN200910012125.5 2009-06-19
CN2009100121255A CN101926506B (en) 2009-06-19 2009-06-19 Application of neophytadiene being taken as cigarette additive
PCT/CN2010/073621 WO2010145469A1 (en) 2009-06-19 2010-06-07 Use of neophytadiene as additive for liquid cigarette

Related Parent Applications (1)

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PCT/CN2010/073621 Continuation WO2010145469A1 (en) 2009-06-19 2010-06-07 Use of neophytadiene as additive for liquid cigarette

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EP (1) EP2444384A1 (en)
JP (1) JP2012529893A (en)
KR (1) KR20120065995A (en)
CN (1) CN101926506B (en)
AU (1) AU2010262386A1 (en)
BR (1) BRPI1011607A2 (en)
CA (1) CA2765872A1 (en)
EA (1) EA201270045A1 (en)
SG (1) SG177259A1 (en)
WO (1) WO2010145469A1 (en)

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