US1959973A - Apparatus for the manufacture of superphosphate and like products - Google Patents
Apparatus for the manufacture of superphosphate and like products Download PDFInfo
- Publication number
- US1959973A US1959973A US387238A US38723829A US1959973A US 1959973 A US1959973 A US 1959973A US 387238 A US387238 A US 387238A US 38723829 A US38723829 A US 38723829A US 1959973 A US1959973 A US 1959973A
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- Prior art keywords
- superphosphate
- chamber
- manufacture
- products
- stationary
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/10—Apparatus for the manufacture of superphosphates
Definitions
- the chief cause of the defects of the superphosphate reaction chambers hitherto generally employed, resides in the intermittent manner in which they operate.
- the present invention aims at providing reaction chambers which are adapted to enable the my work to be carried on continuously, in that the reaction mass and the support on which it rests and adheres is moved in relation to that part of the chamber which contains the intake (mixing machine) and the discharge device, so that the dissociated portions of the charge canbe conveyed continuously to the discharging device and fresh raw'material can be fed into the vacant portion of the chamber.
- the stationary hollow cylinder b prevents the liquid superphosphate from spreading towards The drum 0 and reaction mass rotate on the horizontal rotational axis y--@:-and
- the mixer 'm and discharging device I of the knife the latter "material and detaches dislodged material falls through are stationary whilst the other parts and walls can be connected either to the stationary or the 3p rotary systems, as may be most convenient.
- the hollow cylinder is providedwith ,an opening of ample dimensions, extending from near the one end wall a to the other end wall a and from the auxiliary wall a to about a line under the knives 5 14. Through this opening the dislodged material passes into the hollow cylinder, from which it is led into the open by means of any convenient conveyor.
- the auxiliary wall a is connected with the hollow cylinder and merely serves as a boun- 449 dary for the dissociation chamber, so that the gases liberated by the dissociation process can be evacuated.
- Fig. l is a longitudinal section of a cylindrical chamber with a horizontal rotational axis;
- Fig. 2. shows the same in cross section, and Fig. 3 in plan;
- Fig. 5 is a cross section of a spherical chamber
- Fig. 6 shows an annular chamber, the annular space of which is circular in cross section
- Fig. 4 represents a cylindrical chamber with tionary portion consists THE MANUFACTURE OF 20, 1929, Serial No. 387,238
- the contact surfaces between I a, and c, and also between'a and b, are self tightening.
- the auxiliary wall a is disposed vertically and tangentially in relation to the hollow cylinder b. It carries the exhaust gas flue l, which passes out of the chamber through a and is connected with a fan.
- the discharging device consists of the knife 14,
- a is provided with a slot through which the knife 14 passes out of the interior of the chamber and is thus detached from the block of material. While the knife is in this position the cylinder 0 is moved forward so that, in the next forward movement encounters a thin layer of it from the block.
- auxot extend down to the cythe block of material
- the discharged stream of compressed air is directed upwards. staggered in relation nearer the auxiliary wall a succeeding pipe.
- the second pipe is above, and
- FIG. 4 shows a cylindrical chamber in which the cylinder 0 consists. of two parts separated by an annular gap, cylindrical ring 41, The ring q carries posed centrally in rial. the hollow cylinder the which, in turn,
- the discharging device consists of a number of knives 14, which are attached to two endless chains 17.
- the knives may also be arranged parallel with the rotational axis yy.
- the embodiment shown in Figs. 1-3 would be provided with a knife, clamped on one side in a sliding shoe and swinging up and down in a guide track provided in a. In the ex-.
- the reaction chamber shown in Fig. 6 is in the form of a ring of circular cross section.
- the stationary cylinder is connected to the end wall a, and the rotary support 0 is connected to the end wall a
- the block is broken down by means of a revolving knife disc 14, driven by the pair of pinions 7c and :i.
- the toothed crown 2 serves to drive the support 0, and the conveyor 23 to remove the dislodged material.
- I is the gas .exhaust flue.
- Reaction chamber for the manufacture of superphosphate and like products which comprises one portion which carries the reaction material-and which is movable in relation to a second stationary portion the first portion being constructed as a rotational body rotating about a stationary hollow round shaped body with a horizontal "axis.
- Reaction chamber for the manufacture of superphosphate and like products which comprises one portion which carries the reaction material and which is movable in relation to a second stationary portion the first portion being constructed as a rotational body rotating about a stationary hollow round shaped body with a horizontal axis, this hollow body being provided with a spacious opening for the discharging of the material.
- Reaction chamber for the manufacture of superphosphate and like products which comprises one portion which carries the reaction material and which is movable in relation to a second stationary portion the first portion being constructed as a rotational body rotating about a stationary hollow round shaped body with a horizontal axis'and two end walls one of which being attached to the rotating portion, the other to the stationary portion of the reaction chamber.
- Reaction chamber for the manufacture of superphosphate and like products which comprises one portion constructed as a rotational cylinder rotating about a stationary hollow cylinder with a horizontal axis which is provided with a spacious opening for the discharging of the material and carries one of the end walls, the other end wall being attached to the rotating cylinder.
- Reaction chamber for the manufacture of superphosphate and like products which com superphosphate and like products which comprises one portion which carries the reaction material and which is movable in relation to a second stationary portion, the first portion being constructed as a rotational body rotating about a stationary hollow round-shaped body with a horizontal axis revolving knives being providedin the reaction chamber to break down the block of superphosphate.
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- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
1,959,973 APPARATUS FOR THE MANUFACTURE OF SUPERPHOSPHATE AND LIKE PRODUCTS D. WELLISCH May 22, 1934.
Filed Aug. 20, 1929 25 the conveyor.
reamed ma 22, 134
APPARATUS FUR Application August In Germany '3 Claims. (01!. 71-4) In the chambers shown in Figs; 1-3, the sta- This invention relates to apparatus for the manufacture of superphosphate and the like products.
The chief cause of =the defects of the superphosphate reaction chambers hitherto generally employed, resides in the intermittent manner in which they operate.
The present invention aims at providing reaction chambers which are adapted to enable the my work to be carried on continuously, in that the reaction mass and the support on which it rests and adheres is moved in relation to that part of the chamber which contains the intake (mixing machine) and the discharge device, so that the dissociated portions of the charge canbe conveyed continuously to the discharging device and fresh raw'material can be fed into the vacant portion of the chamber.
In-the embodiments illustrated in the accomgg panying drawing, these parts rotate on a horizontal axis.
As the apparatus rotates on a horizontal axis, the stationary hollow cylinder b prevents the liquid superphosphate from spreading towards The drum 0 and reaction mass rotate on the horizontal rotational axis y--@:-and
accordingly, the mixer 'm and discharging device I of the knife the latter "material and detaches dislodged material falls through are stationary whilst the other parts and walls can be connected either to the stationary or the 3p rotary systems, as may be most convenient. The hollow cylinder is providedwith ,an opening of ample dimensions, extending from near the one end wall a to the other end wall a and from the auxiliary wall a to about a line under the knives 5 14. Through this opening the dislodged material passes into the hollow cylinder, from which it is led into the open by means of any convenient conveyor. The auxiliary wall a is connected with the hollow cylinder and merely serves as a boun- 449 dary for the dissociation chamber, so that the gases liberated by the dissociation process can be evacuated.
In order to make clear the character of my invention, a preferred embodiment is illustrated in the drawing wherein:
Fig. l is a longitudinal section of a cylindrical chamber with a horizontal rotational axis; Fig. 2. shows the same in cross section, and Fig. 3 in plan;
' sub-dividedf cylinder;
Fig. 5 is a cross section of a spherical chamber; en
Fig. 6 shows an annular chamber, the annular space of which is circular in cross section,
Fig. 4 represents a cylindrical chamber with tionary portion consists THE MANUFACTURE OF 20, 1929, Serial No. 387,238
February 2!, 1929 of an end wall a in which is placed a hollow cylinder b, concentric with the rotational axis. The end wall a (in which is sunk the mixer m) and the hollow cylinder in are held in place by an iron structure. The opposite end wall a is connected with the cylindrical shell 0, with which it turns in the direction of the arrow s. The cylinder, which is mounted on rollers r,
is driven, in the usual manner, by a pinion '1 with driving wheel 2 The contact surfaces between I a, and c, and also between'a and b, are self tightening. The auxiliary wall a is disposed vertically and tangentially in relation to the hollow cylinder b. It carries the exhaust gas flue l, which passes out of the chamber through a and is connected with a fan. The discharging device consists of the knife 14,
which is disposed at right angles to the rotational axis and is reciprocated in the direction of the double arrow s", by means of the guide rods 15 which slide in the bearing 16 and are moved by a crank or the like. a is provided with a slot through which the knife 14 passes out of the interior of the chamber and is thus detached from the block of material. While the knife is in this position the cylinder 0 is moved forward so that, in the next forward movement encounters a thin layer of it from the block. The
the opening provided in the hollow cylinder onto a conveyor 23 which is disposed in the interior of the hollow cylinder 1) and conveys; the dislodged material into the open. The
,iliary wall a does n knife 14, and also the auxot extend down to the cythe block of material,
the requisite pipes are disposed parallel with the rotational axisil-Zl. and
mounted in the end wall a. pipes is situated under The first of these the generating line e, and
the discharged stream of compressed air is directed upwards. staggered in relation nearer the auxiliary wall a succeeding pipe.
The second pipe is above, and
to, the first, so that it lies and so on with each Fig. 4 shows a cylindrical chamber in which the cylinder 0 consists. of two parts separated by an annular gap, cylindrical ring 41, The ring q carries posed centrally in rial. the hollow cylinder the which, in turn,
so that a tight joint is formed.
is covered by the mixer m which is thus disrelation to the block of mate- The end Walls a and a are connected to b, and are carried by an iron structure. The surfaces of contact with the cylinders c are close fitting. The cylinders c are mounted on rollers r, and are uniformly moved by means of the toothed crowns z. The discharging device consists of a number of knives 14, which are attached to two endless chains 17.
These chains, together with the knives, are moved' by a toothed wheel not illustrated in the direction of the arrow s pass out of the chamber through a slot in a, are diverted from this direction of movement by rollers not shown and passed round the outside of the chamber, to be led over other rollers and into the chamber again through a slot in (1 This arrangement of the discharging device enables the two cylinders c to be moved in a uniform manner. The dislodged material drops through the opening provided in the hollow cylinder b and on to the conveyor 23.
Instead of being vertically disposed, as shown, the knives may also be arranged parallel with the rotational axis yy. The embodiment shown in Figs. 1-3 would be provided with a knife, clamped on one side in a sliding shoe and swinging up and down in a guide track provided in a. In the ex-.
ample shown in Fig. 5, a number of knives, attached to two endless chains, would be provided. These chains would run at right angles to the rotational axis and guided, in each case, by two rollers mounted in the end walls a and a respectively.
In the embodiment according to Fig. 5, the
parts a, c and a as a whole, assume approximately a spherical form. The end wall a is connected to the stationary hollow cylinder b, and
carries the mixer m. a and c constitute a unit,,
are mounted on rollers 1', and are rotated by means of the toothed crown z. The block is broken down by'means of the knife 14 which rocks on the shaft 13 driven by a crank or the like. The reaction mass is moved forward intermittently, and at the moment when the knife 14 is inside the cylinder 1). .The dislodged material is carried away by the conveyor 23. The contact surfaces between a and c, and between a and b, are self-tightening. Z is the gas exhaust flue.
The reaction chamber shown in Fig. 6 is in the form of a ring of circular cross section. The stationary cylinder is connected to the end wall a, and the rotary support 0 is connected to the end wall a The block is broken down by means of a revolving knife disc 14, driven by the pair of pinions 7c and :i. The toothed crown 2 serves to drive the support 0, and the conveyor 23 to remove the dislodged material. I is the gas .exhaust flue.
What I claim is:-
1. Reaction chamber for the manufacture of superphosphate and like products which comprises one portion which carries the reaction material-and which is movable in relation to a second stationary portion the first portion being constructed as a rotational body rotating about a stationary hollow round shaped body with a horizontal "axis.
2. Reaction chamber for the manufacture of superphosphate and like products which comprises one portion which carries the reaction material and which is movable in relation to a second stationary portion the first portion being constructed as a rotational body rotating about a stationary hollow round shaped body with a horizontal axis, this hollow body being provided with a spacious opening for the discharging of the material.
3. Reaction chamber for the manufacture of superphosphate and like products which comprises one portion which carries the reaction material and which is movable in relation to a second stationary portion the first portion being constructed as a rotational body rotating about a stationary hollow round shaped body with a horizontal axis'and two end walls one of which being attached to the rotating portion, the other to the stationary portion of the reaction chamber.
4. Reaction chamber for the manufacture of superphosphate and like products which comprises one portion which carries the reaction material and which is movable in relation to a second stationary portion, the first portion being constructed as a rotational body rotating about a stationary hollow round shaped body with a horizontal axis the specific reaction room being separated from the discharging room by an auxiliary wall.
5. Reaction chamber for the manufacture of superphosphate and like products which comprises one portion constructed as a rotational cylinder rotating about a stationary hollow cylinder with a horizontal axis which is provided with a spacious opening for the discharging of the material and carries one of the end walls, the other end wall being attached to the rotating cylinder.
6. Reaction chamber for the manufacture of superphosphate and like products which com superphosphate and like products which comprises one portion which carries the reaction material and which is movable in relation to a second stationary portion, the first portion being constructed as a rotational body rotating about a stationary hollow round-shaped body with a horizontal axis revolving knives being providedin the reaction chamber to break down the block of superphosphate.
DRAG UTIN WELLISCH.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE1959973X | 1929-02-07 |
Publications (1)
Publication Number | Publication Date |
---|---|
US1959973A true US1959973A (en) | 1934-05-22 |
Family
ID=7782043
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US387238A Expired - Lifetime US1959973A (en) | 1929-02-07 | 1929-08-20 | Apparatus for the manufacture of superphosphate and like products |
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US (1) | US1959973A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2587367A (en) * | 1939-01-06 | 1952-02-26 | Moritz Jean | Continuous apparatus for the manufacture of superphosphates and similar products |
US2729554A (en) * | 1952-12-26 | 1956-01-03 | Tennessee Valley Authority | Ammoniation of superphosphate |
US2886426A (en) * | 1953-05-30 | 1959-05-12 | Montedison Spa | Process for continuously manufacturing superphosphate |
-
1929
- 1929-08-20 US US387238A patent/US1959973A/en not_active Expired - Lifetime
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2587367A (en) * | 1939-01-06 | 1952-02-26 | Moritz Jean | Continuous apparatus for the manufacture of superphosphates and similar products |
US2729554A (en) * | 1952-12-26 | 1956-01-03 | Tennessee Valley Authority | Ammoniation of superphosphate |
US2886426A (en) * | 1953-05-30 | 1959-05-12 | Montedison Spa | Process for continuously manufacturing superphosphate |
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