US1854321A - Decorative treatment of textile fabrics - Google Patents
Decorative treatment of textile fabrics Download PDFInfo
- Publication number
- US1854321A US1854321A US409427A US40942729A US1854321A US 1854321 A US1854321 A US 1854321A US 409427 A US409427 A US 409427A US 40942729 A US40942729 A US 40942729A US 1854321 A US1854321 A US 1854321A
- Authority
- US
- United States
- Prior art keywords
- fabric
- diazo
- colour
- component
- naphthol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000004744 fabric Substances 0.000 title description 62
- 238000011282 treatment Methods 0.000 title description 11
- 239000004753 textile Substances 0.000 title description 5
- 239000000306 component Substances 0.000 description 21
- 150000008049 diazo compounds Chemical class 0.000 description 13
- 239000003086 colorant Substances 0.000 description 10
- KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 description 9
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 description 9
- 238000000034 method Methods 0.000 description 8
- 239000000975 dye Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 239000000463 material Substances 0.000 description 6
- RUFPHBVGCFYCNW-UHFFFAOYSA-N 1-naphthylamine Chemical compound C1=CC=C2C(N)=CC=CC2=C1 RUFPHBVGCFYCNW-UHFFFAOYSA-N 0.000 description 4
- JWAZRIHNYRIHIV-UHFFFAOYSA-N 2-naphthol Chemical compound C1=CC=CC2=CC(O)=CC=C21 JWAZRIHNYRIHIV-UHFFFAOYSA-N 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000003993 interaction Effects 0.000 description 2
- JRBJSXQPQWSCCF-UHFFFAOYSA-N 3,3'-Dimethoxybenzidine Chemical compound C1=C(N)C(OC)=CC(C=2C=C(OC)C(N)=CC=2)=C1 JRBJSXQPQWSCCF-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 241000322338 Loeseliastrum Species 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 229950011260 betanaphthol Drugs 0.000 description 1
- ZLFVRXUOSPRRKQ-UHFFFAOYSA-N chembl2138372 Chemical compound [O-][N+](=O)C1=CC(C)=CC=C1N=NC1=C(O)C=CC2=CC=CC=C12 ZLFVRXUOSPRRKQ-UHFFFAOYSA-N 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- -1 for example Chemical class 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- COHYTHOBJLSHDF-BUHFOSPRSA-N indigo dye Chemical compound N\1C2=CC=CC=C2C(=O)C/1=C1/C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-BUHFOSPRSA-N 0.000 description 1
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- KIEOKOFEPABQKJ-UHFFFAOYSA-N sodium dichromate Chemical compound [Na+].[Na+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KIEOKOFEPABQKJ-UHFFFAOYSA-N 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000001117 sulphuric acid Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 239000000984 vat dye Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/0004—General aspects of dyeing
- D06P1/002—Processing by repeated dyeing, e.g. in different baths
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/0096—Multicolour dyeing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
- D06P3/68—Preparing azo dyes on the material
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
- Y10S8/916—Natural fiber dyeing
- Y10S8/918—Cellulose textile
Definitions
- This invention relates to the decorative treatment of textile fabrics, and more particularly to the production of two-sided or reversible prints in which, whilst the patterns or portions of the patterns at the two sides are the same and in perfect register, they are in contrasting colours.
- the invention comprises the separate treatment of the opposite sides of the fabric followed by or subsequent to a treatment of one side thereof with a material or materials which penetrates or penetrate through the fabric and reacts or react differently with the materials used in the separate treatments, so as to produce the same pattern but different colour shades or contrasting colours at the opposite sides of the fabric.
- the invention further comprises the incorporation with the materials used in the treatment of the fabric of suitable discharges or resists for the purpose of varying the colour effects.
- one side of the fabric is prepared by means of an engraved padding or printing roller with a suitably thickened solution of an azo-dyestufi component capable of forming insoluble azo colours by interaction with a diazo solution, such as b-eta-naphthol, the body commercially known as Naphthol A. S. (Col. Ind. p. 333), and the like, and then after drying, the other side of the fabric is similarly prepared with a different component, such as for example, the body com suddenly known as Naphthol A. S. G. (Col. Ind. p. 359), and dried.
- a diazo solution such as b-eta-naphthol
- the fabric is printed at one side only by means of a copper printing roller having engraving of exceptional depth, such as is usual for bangthrough work, with a diazo-compound capable of producing an insoluble azo colour of one shade with the component on one side, and of another contrasting shade with the component on the other side of the fabric.
- One example of this method is as follows Pad one face of the cloth with Beta Naphthol R. (Col. Ind. p. 359). Pad the other face of the cloth with Naphthol A. S. Print, using bang-through engraving, one side of the fabric with a two-colour pattern, using in oneprinting roller Chromacetine Blue S.
- a plurality of diazo compounds may be printed in fit on the one side of the fabric for producing a variation in the colour effects at each side of the fabric.
- the diazo compound printed by the deeply engraved roller or rollers may be printed along with, for example, chrome colours to produce multi-coloured effects.
- a typical printing combination is diazotized para-nitro-orthoanisidine in one roller with Chromacetine Blue S. (Colour Index 884) printed in fit in a second roller. Or diazotized' para-nitroortho-anisidine in one roller, diazotized paranitraniline in a second roller and Chromacetine Blue S. (Colour Index 884) in a third roller, the patterns on the three rollers being in fit.
- the character of the cloth andthe thickness of the pad or cover with which the two sides of the fabric are separately prepared should be such that a minimum'of the prepare on one side of the fabric penetrates to the other side.
- a fixed organic acid such as, for example, citric acid, may be added to the diazo compound to moderate the-speed of coupling with the component on the face of the cloth, upon which the diazo compound is printed, and thus ensure a sufficiency of such compound to couple with the other component on the back of the cloth.
- I print the colour or colours of the design (which is to appear with contrasting shades on the opposite sides of the cloth) with one or more components which penetrate to the opposite sides of the fabric, and subsequently pad or cover the so printed goods on one side of the cloth with one diazo solution and on the other side of the cloth with a different diazo solution.
- I may modify or vary the effects produced by incorporating with the diazo printing colours suitable materials to produce resist or discharge effects, or the resists or discharges may be printed by a separate roller or rollers, either fitting with or .fallingon the patterns produced by the engraved rollers which print the diazo colours.
- acetate of soda might be printed along with the diazo colour for the purpose of resisting, for example, an indigosol (Disulphuric ether of a leuco-vat dye) afterwards applied to the fabric; or as another example, bichromate of soda may be incorporated with the diazo colour to discharge indigo dye which has already been applied to the fabric, the discharging being completed. by passing the goods through an appropriate bath of sulphuric acid and oxalic acid in the well known manner.
- I may apply the azo dyestuff components to the opposite sides of the fabric by spraying instead of by padding or printing. Or one side may be sprayed and the other padded or printed.
- a process for the decorative treatment of a textile fabric which comprises preparing one side of a textile fabric with a suitably thickened solution of an azo dyestuff compo nent capable of forming insoluble azo colours, by interaction with a diazo solution, drying the fabric, preparing the other side of the fabric with a different component, drying the fabric, and printing the fabric at one side only with a printing roller having engraving of exceptional depth, with a diazo compound capable of producing an insoluble azo colour of one shade with the component on one side and of another contrasting shade with the component on the other side of the fabric.
- a process for the decorative treatment of fabric which comprises, applying an azo dyestuff component to one side of the fabric, applying a different azo dyestuff component to the other side thereof, and applying to the fabric so that it penetrates to both sides thereof a diazo compound which reacts differently with the said components to produce the same pattern at the opposite sides of the fabric in contrasting colours.
- a process for the decorative treatment of fabrics which comprises producing a pattern in a thickened solution of an azo dyestuff component at one side of the fabric, producing a pattern in a thickened solution of another azo dyestuif component at the other side of the fabric and printing one side only of the fabric with a diazo compound which penetrates to both sides of the fabric and forms insoluble azo colours of contrasting shades with the azo dyestuff components at the opposite sides of the fabric.
- a process for the decorative treatment of fabrics which comprises printing one side of the fabric with at least one azo dyestuffs component which penetrates to the opposite sides of the fabric, treating one side of the fabric with at least one diazo compound and treating the other side of the fabric with a different diazo compound or compounds.
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Description
Patented Apr. 19, 1932 UNITED STATES PATENT orricr.
JAMESv DAVIDSON W'EBSTEB, 0F BONHILL, ENGLAND, ASSIGNOR TO THE CALICO I PRINTERS ASSOCIATION LIMITED, OF MANCHESTER, ENGLAND, A BRITISH COM.-
IPANY DECORATIVE TREATMENT OF TEXTILE FABRICS No Drawing. Application filed. November 2-3, 1929, Serial No. 409,427, and in Great Britain December 20, 1928.
This invention relates to the decorative treatment of textile fabrics, and more particularly to the production of two-sided or reversible prints in which, whilst the patterns or portions of the patterns at the two sides are the same and in perfect register, they are in contrasting colours.
The invention comprises the separate treatment of the opposite sides of the fabric followed by or subsequent to a treatment of one side thereof with a material or materials which penetrates or penetrate through the fabric and reacts or react differently with the materials used in the separate treatments, so as to produce the same pattern but different colour shades or contrasting colours at the opposite sides of the fabric.
The invention further comprises the incorporation with the materials used in the treatment of the fabric of suitable discharges or resists for the purpose of varying the colour effects.
In one convenient application of my invention, one side of the fabric is prepared by means of an engraved padding or printing roller with a suitably thickened solution of an azo-dyestufi component capable of forming insoluble azo colours by interaction with a diazo solution, such as b-eta-naphthol, the body commercially known as Naphthol A. S. (Col. Ind. p. 333), and the like, and then after drying, the other side of the fabric is similarly prepared with a different component, such as for example, the body com mercially known as Naphthol A. S. G. (Col. Ind. p. 359), and dried. Thereafter, the fabric is printed at one side only by means of a copper printing roller having engraving of exceptional depth, such as is usual for bangthrough work, with a diazo-compound capable of producing an insoluble azo colour of one shade with the component on one side, and of another contrasting shade with the component on the other side of the fabric.
One example of this method is as follows Pad one face of the cloth with Beta Naphthol R. (Col. Ind. p. 359). Pad the other face of the cloth with Naphthol A. S. Print, using bang-through engraving, one side of the fabric with a two-colour pattern, using in oneprinting roller Chromacetine Blue S.
(Colour Index 884) and in the other roller Fast Red R. L. base (Col. Ind. Suppl. p. 41). The fabric shows orange and blue at one side and red and blue at the other side.
If desired, a plurality of diazo compounds may be printed in fit on the one side of the fabric for producing a variation in the colour effects at each side of the fabric. The diazo compound printed by the deeply engraved roller or rollers may be printed along with, for example, chrome colours to produce multi-coloured effects. A typical printing combination is diazotized para-nitro-orthoanisidine in one roller with Chromacetine Blue S. (Colour Index 884) printed in fit in a second roller. Or diazotized' para-nitroortho-anisidine in one roller, diazotized paranitraniline in a second roller and Chromacetine Blue S. (Colour Index 884) in a third roller, the patterns on the three rollers being in fit. The character of the cloth andthe thickness of the pad or cover with which the two sides of the fabric are separately prepared should be such that a minimum'of the prepare on one side of the fabric penetrates to the other side. A fixed organic acid such as, for example, citric acid, may be added to the diazo compound to moderate the-speed of coupling with the component on the face of the cloth, upon which the diazo compound is printed, and thus ensure a sufficiency of such compound to couple with the other component on the back of the cloth.
In another application of my invention, I print the colour or colours of the design (which is to appear with contrasting shades on the opposite sides of the cloth) with one or more components which penetrate to the opposite sides of the fabric, and subsequently pad or cover the so printed goods on one side of the cloth with one diazo solution and on the other side of the cloth with a different diazo solution. 1
I may modify or vary the effects produced by incorporating with the diazo printing colours suitable materials to produce resist or discharge effects, or the resists or discharges may be printed by a separate roller or rollers, either fitting with or .fallingon the patterns produced by the engraved rollers which print the diazo colours. As an example, acetate of soda might be printed along with the diazo colour for the purpose of resisting, for example, an indigosol (Disulphuric ether of a leuco-vat dye) afterwards applied to the fabric; or as another example, bichromate of soda may be incorporated with the diazo colour to discharge indigo dye which has already been applied to the fabric, the discharging being completed. by passing the goods through an appropriate bath of sulphuric acid and oxalic acid in the well known manner.
If desired, I may apply the azo dyestuff components to the opposite sides of the fabric by spraying instead of by padding or printing. Or one side may be sprayed and the other padded or printed.
Further examples of the application of my invention are as follows:
(1) Print or pad one face of a cotton cloth with Naphthol A. S. Print or pad the other face of the cloth with Naphthol A. S. G. Print one side of the cloth using bangthrough engraving, with a three colour pattern using (1) tetrazotised dianisidine, (2) diazo-para-nitro-ortlio-anisidine and diazo meta-nitraniline.
(2) Print one side of a cotton fabric (using bang-through engraving) as a two colour fitting pattern with (l) Naphthol A. S. and (2) Naphthol A. S. G. Print one face of the fabric with diazotized para-nitro-orthoanisidine and the other face with diazotized alpha naphthylamine.
(3) Pad one face of a cotton fabric with Naphthol A. S. and the other face with a mixture of three parts Naphthol A. S. G. and one part Naphthol A. S. R. L. (001. Ind. Suppl. p. 46). Print (using bang-through engraving), one side of the fabric with diazotized alpha naphthylamine as a one colour stripe, and develop in diazotized para-nitroortho-toluidine. The fabric will be scarlet and claret on one side and orange and brown on the other.
lVhat I claim is 1. A process for the decorative treatment of a textile fabric which comprises preparing one side of a textile fabric with a suitably thickened solution of an azo dyestuff compo nent capable of forming insoluble azo colours, by interaction with a diazo solution, drying the fabric, preparing the other side of the fabric with a different component, drying the fabric, and printing the fabric at one side only with a printing roller having engraving of exceptional depth, with a diazo compound capable of producing an insoluble azo colour of one shade with the component on one side and of another contrasting shade with the component on the other side of the fabric.
2. In the process of claim 1, printing a plurality of diazo compounds on the one side of the fabric for producing a variation in the colour effects at each side of the fabric.
3. In the process of claim 1, printing the fabric at one side by a printing roller or rollers having engraving of exceptional depth with an azo dyestuff component or components before preparing the two sides with separate diazo compounds.
4. A process for the decorative treatment of fabric, which comprises, applying an azo dyestuff component to one side of the fabric, applying a different azo dyestuff component to the other side thereof, and applying to the fabric so that it penetrates to both sides thereof a diazo compound which reacts differently with the said components to produce the same pattern at the opposite sides of the fabric in contrasting colours.
5. A process for the decorative treatment of fabrics which comprises producing a pattern in a thickened solution of an azo dyestuff component at one side of the fabric, producing a pattern in a thickened solution of another azo dyestuif component at the other side of the fabric and printing one side only of the fabric with a diazo compound which penetrates to both sides of the fabric and forms insoluble azo colours of contrasting shades with the azo dyestuff components at the opposite sides of the fabric.
6. A process for the decorative treatment of fabrics which comprises printing one side of the fabric with at least one azo dyestuffs component which penetrates to the opposite sides of the fabric, treating one side of the fabric with at least one diazo compound and treating the other side of the fabric with a different diazo compound or compounds.
7. In the process of claim 5 incorporating materials to produce resist or discharge effects in the diazo compound.
In testimony whereof I have signed my name to this specification.
JAMES DAVIDSON WEBSTER.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB37657/28A GB326823A (en) | 1928-12-20 | 1928-12-20 | Improvements relating to the decorative treatment of textile fabrics |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US1854321A true US1854321A (en) | 1932-04-19 |
Family
ID=10398039
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US409427A Expired - Lifetime US1854321A (en) | 1928-12-20 | 1929-11-23 | Decorative treatment of textile fabrics |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US1854321A (en) |
| BE (1) | BE362237A (en) |
| DE (1) | DE539091C (en) |
| GB (1) | GB326823A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5180401A (en) * | 1991-09-30 | 1993-01-19 | Beacon Manufacturing Company | Printed woven blanket |
-
1928
- 1928-12-20 GB GB37657/28A patent/GB326823A/en not_active Expired
-
1929
- 1929-07-06 DE DEC43365D patent/DE539091C/en not_active Expired
- 1929-07-11 BE BE362237A patent/BE362237A/en unknown
- 1929-11-23 US US409427A patent/US1854321A/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5180401A (en) * | 1991-09-30 | 1993-01-19 | Beacon Manufacturing Company | Printed woven blanket |
| US5368611A (en) * | 1991-09-30 | 1994-11-29 | Deacon Manufacturing Company | Printed woven blanket and method for the manufacture thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| BE362237A (en) | 1929-08-31 |
| DE539091C (en) | 1931-11-23 |
| GB326823A (en) | 1930-03-20 |
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