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SU587725A1 - Method of preparing polyurethan-bityminous composition - Google Patents

Method of preparing polyurethan-bityminous composition Download PDF

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Publication number
SU587725A1
SU587725A1 SU752195903A SU2195903A SU587725A1 SU 587725 A1 SU587725 A1 SU 587725A1 SU 752195903 A SU752195903 A SU 752195903A SU 2195903 A SU2195903 A SU 2195903A SU 587725 A1 SU587725 A1 SU 587725A1
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SU
USSR - Soviet Union
Prior art keywords
weight
composition
bityminous
polyurethan
preparing
Prior art date
Application number
SU752195903A
Other languages
Russian (ru)
Inventor
Б.П. Смирнов
В.Н. Кузьмин
Н.М. Белова
Т.И. Костенко
Л.П. Головина
Original Assignee
Предприятие П/Я Г-4059
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Application filed by Предприятие П/Я Г-4059 filed Critical Предприятие П/Я Г-4059
Priority to SU752195903A priority Critical patent/SU587725A1/en
Application granted granted Critical
Publication of SU587725A1 publication Critical patent/SU587725A1/en

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  • Polyurethanes Or Polyureas (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Description

изоцианата и отверждают без дополнительного подогрева.isocyanate and cure without additional heating.

Использова 1ие предлагаемого способа позвол ет упростить технологию получени  композиции. Введение карбоновых кислот и их производных в композицию дает возможность улзчшить совместимость полиэфиров с битумом и тем самым повысить физико-механические свойства. Исключение из композиции растворител  снижает ее токсичность и пожароопасность.Using 1 of the proposed method allows to simplify the technology of the composition. The introduction of carboxylic acids and their derivatives into the composition makes it possible to improve the compatibility of polyesters with bitumen and thereby increase the physicomechanical properties. The exclusion from the composition of the solvent reduces its toxicity and fire hazard.

Пример 1. К раствору 15 вес. ч. битума в 15 вес. ч. оксипропилированной олеиновой кислоты (кислотное число (к. ч.) 6,5) добавл ют 18 вес. ч. простого полиэфира триола с мол. вес. 5000, 15 вес. ч. простого полиэфира с мол. вес. 500, 4 вес. ч. алюмосиликата - цеолита марки NaA, 20 вес. ч. талька, 1 вес. ч. диметилбензиламина и смешивают с 21 вес. ч. полиизоцианата. Покрытие имеет прочность на разрыв 5 кг/см, относительное удлинение при разрыве 90%.Example 1. To a solution of 15 wt. including bitumen in 15 wt. including hydroxypropylated oleic acid (acid number (q.) 6.5), 18 wt. including polyether triol mol. weight. 5000, 15 weight. including polyether with mol. weight. 500, 4 weight. including aluminosilicate - zeolite brand NaA, 20 wt. talc, 1 wt. including dimethylbenzylamine and mixed with 21 wt. including polyisocyanate. The coating has a tensile strength of 5 kg / cm, an elongation at break of 90%.

Пример 2. К раствору 15 вес. ч. битума в 15 вес. ч. оксипропилированного таллового масла (к. ч. 5,2) добавл ют 15 вес. ч. простого полиэфира триола с мол. вес. 5000, 15 вес. ч. простого полиэфира триола с мол. вес. 500, 4 вес. ч. алюмосиликата цеолита марки NaA, 15 вес. ч. окиси цинка, 1 вес. ч. диметилбензиламина и смешивают с 20 вес. ч. полиизоцианата. Покрытие имеет прочность на разрыв 79 кг/см, относительное удлинение при разрыве 110%.Example 2. To a solution of 15 wt. including bitumen in 15 wt. h oxypropylated tall oil (r h 5.2) add 15 weight. including polyether triol mol. weight. 5000, 15 weight. including polyether triol mol. weight. 500, 4 weight. including aluminosilicate zeolite brand NaA, 15 wt. including zinc oxide, 1 wt. including dimethylbenzylamine and mixed with 20 wt. including polyisocyanate. The coating has a tensile strength of 79 kg / cm, an elongation at break of 110%.

Пример 3. К 30 вес. ч. смеси, содержащей 15 вес. ч. простого полиэфира триола с мол. вес. 500 и 15 вес. ч. простого полиэфира диола с мол. вес. 1000, добавл ют раствор 30 вес. ч. нефт ного битума в 30. вес. ч. оксипропилированного таллового масла (к. ч. 5,2), 9 вес. ч. цеолита и 0,5 вес. ч. диметилбензиламина, затем отверждают 10 вес. ч. полиизоцианата. Покрытие имеет прочность на разрыв 10 кг/см, относительное удлинение при разрыве 20%.Example 3. To 30 wt. including mixtures containing 15 wt. including polyether triol mol. weight. 500 and 15 weight. including polyether diol mol. weight. 1000, add a solution of 30 wt. including oil bitumen in 30. weight. h oxypropylated tall oil (r. 5,2), 9 weight. including zeolite and 0.5 wt. including dimethylbenzylamine, then cured 10 weight. including polyisocyanate. The coating has a tensile strength of 10 kg / cm, an elongation at break of 20%.

Пример 4. Берут раствор 8 вес. ч. битума в 8 вес. ч. таллового масла, добавл ют 3 вес. ч. простого полиэфира триола с мол. вес. 5000, 75 вес. ч. резиновой крошки , 1 вес. ч. диметилбензиламина и смешивают с 5 вес. ч. кодицина. Полученное покрытие имеет прочность на разрыв 4 кг/см относительное удлинение при разрыве 25%.Example 4. Take a solution of 8 wt. including bitumen in 8 wt. including tall oil, add 3 wt. including polyether triol mol. weight. 5000, 75 weight. including rubber crumb, 1 wt. including dimethylbenzylamine and mixed with 5 wt. including codicin. The resulting coating has a tensile strength of 4 kg / cm elongation at break of 25%.

Пример 5. К раствору 16,5 вес. ч. нефт ного битума в 16,5 вес. ч. оксиэтилированной олеиновой кислоты (к. ч. 3,15) добавл ют 23,4 вес. ч. простого полиэфира триола с мол. вес. 500, 9,6. вес. ч. простого полиэфира триола с мол. вес. 5000, 6,3 вес. ч. цеолита, 1 вес. ч. диметилбензиламина,Example 5. To a solution of 16.5 wt. including oil bitumen in 16.5 wt. including ethoxylated oleic acid (for example 3.15), 23.4 wt. including polyether triol mol. weight. 500, 9.6. weight. including polyether triol mol. weight. 5000, 6.3 weight. h. zeolite, 1 wt. including dimethylbenzylamine,

перемешивают и отверждают с 26,7 вес. ч. полиизоцианата. Материал имеет прочность на разрыв 185 кг/см, относительное удлинение 30%.mix and cure with 26.7 wt. including polyisocyanate. The material has a tensile strength of 185 kg / cm, an elongation of 30%.

Claims (3)

1.Патент США № 3372083, кл. 106--278, опубл. 1961.1. US Patent No. 3372083, cl. 106--278, publ. 1961. 2.Патент США № 3615802, кл. 106-278, опубл. 1962.2. US patent number 3615802, cl. 106-278, publ. 1962. 3.Патент Франции № 1583664, кл. В 29с, опубл. 1962.3.Patent of France No. 1583664, cl. In 29s, publ. 1962.
SU752195903A 1975-12-04 1975-12-04 Method of preparing polyurethan-bityminous composition SU587725A1 (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
SU752195903A SU587725A1 (en) 1975-12-04 1975-12-04 Method of preparing polyurethan-bityminous composition

Publications (1)

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SU587725A1 true SU587725A1 (en) 1980-01-30

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5008311A (en) * 1989-03-17 1991-04-16 Tremco Incorporated Substantially solvent free asphaltic and method relating thereto
US5319008A (en) * 1990-03-21 1994-06-07 Tremco, Inc. Substantially solvent-free, stable dispersion of a bituminous material in a liquid prepolymer, and method for forming the dispersion
US5421876A (en) * 1990-12-21 1995-06-06 Tremco, Inc. Solvent-free, organoclay-filled asphaltic polyurethane dispersion and method of making and using it
WO2000011111A2 (en) * 1998-08-19 2000-03-02 Urecoats International, Inc. Bituminous polyurethane interpenetrating elastomeric network compositions

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5008311A (en) * 1989-03-17 1991-04-16 Tremco Incorporated Substantially solvent free asphaltic and method relating thereto
US5319008A (en) * 1990-03-21 1994-06-07 Tremco, Inc. Substantially solvent-free, stable dispersion of a bituminous material in a liquid prepolymer, and method for forming the dispersion
US5421876A (en) * 1990-12-21 1995-06-06 Tremco, Inc. Solvent-free, organoclay-filled asphaltic polyurethane dispersion and method of making and using it
WO2000011111A2 (en) * 1998-08-19 2000-03-02 Urecoats International, Inc. Bituminous polyurethane interpenetrating elastomeric network compositions
WO2000011111A3 (en) * 1998-08-19 2000-06-02 Urecoats International Inc Bituminous polyurethane interpenetrating elastomeric network compositions

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