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SU566847A1 - Method of preparing chloralkyl-s-organochlorthio- - Google Patents

Method of preparing chloralkyl-s-organochlorthio-

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Publication number
SU566847A1
SU566847A1 SU7502120931A SU2120931A SU566847A1 SU 566847 A1 SU566847 A1 SU 566847A1 SU 7502120931 A SU7502120931 A SU 7502120931A SU 2120931 A SU2120931 A SU 2120931A SU 566847 A1 SU566847 A1 SU 566847A1
Authority
SU
USSR - Soviet Union
Prior art keywords
organochlorthio
chloralkyl
preparing
calculated
s1ang
Prior art date
Application number
SU7502120931A
Other languages
Russian (ru)
Inventor
Николай Кириллович Близнюк
Зоя Николаевна Кваша
Людмила Викторовна Чверткина
Лидия Михайловна Солнцева
Original Assignee
Всесоюзный научно-исследовательский институт фитопатологии
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Всесоюзный научно-исследовательский институт фитопатологии filed Critical Всесоюзный научно-исследовательский институт фитопатологии
Priority to SU7502120931A priority Critical patent/SU566847A1/en
Application granted granted Critical
Publication of SU566847A1 publication Critical patent/SU566847A1/en

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Description

перегонкой, т. кип. 125-128°С/1 мм рт. ст.; «2 1,5010; df 1,3366. MRo 52,3, вычислено 52,6. Выход 82,5%. Найдено, %: С1аш-. 14,61; S 13,28: Вычислено, %: С1анг. 14,95; S 13,50. В услови х примера 1 получают другие вё щества, представленные в таблице.distillation, t. Kip. 125-128 ° C / 1 mm Hg. v .; “2 1,5010; df 1.3366. MRo 52.3, calculated 52.6. Yield 82.5%. Found,%: C1ash-. 14.61; S 13.28: Calculated,%: S1ang. 14.95; S 13.50. Under the conditions of Example 1, the other substances presented in the table are obtained.

Пример 2. Получение 7-хлорпропил-5-4хлорфенил-хлортиофосфата .Example 2. Getting 7-chloropropyl-5-4 chlorophenyl-chlorothiophosphate.

К 0,05 г-моль треххлористого фосфора в 20 мл хлороформа при 0°С прибавл ют 0,05 г-моль 1,3-пропиленгликол , а затем в тех же услови х раствор 0,05 г-моль 4-хлорфенилсульфенилхлорида . Смесь перемешивают 2 ч при комнатной температуре, растворитель и летучие вещества удал ют в вакууме и в остатке получают продукт в виде малоподвижной жидкости.To 0.05 gm mol of phosphorus trichloride in 20 ml of chloroform at 0 ° C was added 0.05 gm mol of 1,3-propylene glycol, and then under the same conditions a solution of 0.05 gm mol of 4-chlorophenylsulfenyl chloride. The mixture is stirred for 2 hours at room temperature, the solvent and volatiles are removed in vacuo, and the residue is obtained as a sedentary liquid.

Выход 97%, п 1,5808, df 1,4507. MRo 73,0, вычислено 72,3. Найдено, %: С1анг. 11,26; S 10,38. Вычислено, %: С1анг. ПД1; S 10,01.The yield is 97%, p 1,5808, df 1,4507. MRo 73.0, calculated 72.3. Found,%: S1ang. 11.26; S 10.38. Calculated,%: S1ang. PD1; S 10.01.

Claims (1)

1. Авторское свидетельство СССР №202937, кл. С 07F 9/20, 1966.1. USSR author's certificate No. 202937, cl. From 07F 9/20, 1966.
SU7502120931A 1975-04-04 1975-04-04 Method of preparing chloralkyl-s-organochlorthio- SU566847A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU7502120931A SU566847A1 (en) 1975-04-04 1975-04-04 Method of preparing chloralkyl-s-organochlorthio-

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU7502120931A SU566847A1 (en) 1975-04-04 1975-04-04 Method of preparing chloralkyl-s-organochlorthio-

Publications (1)

Publication Number Publication Date
SU566847A1 true SU566847A1 (en) 1977-07-30

Family

ID=20615119

Family Applications (1)

Application Number Title Priority Date Filing Date
SU7502120931A SU566847A1 (en) 1975-04-04 1975-04-04 Method of preparing chloralkyl-s-organochlorthio-

Country Status (1)

Country Link
SU (1) SU566847A1 (en)

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