SU505637A1 - The method of obtaining -acyl derivatives of the substituted imidazolidine - Google Patents
The method of obtaining -acyl derivatives of the substituted imidazolidineInfo
- Publication number
- SU505637A1 SU505637A1 SU2086702A SU2086702A SU505637A1 SU 505637 A1 SU505637 A1 SU 505637A1 SU 2086702 A SU2086702 A SU 2086702A SU 2086702 A SU2086702 A SU 2086702A SU 505637 A1 SU505637 A1 SU 505637A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- obtaining
- acyl derivatives
- alkyl
- substituted imidazolidine
- formaldehyde
- Prior art date
Links
- 150000002461 imidazolidines Chemical class 0.000 title claims 2
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 6
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 229940072033 potash Drugs 0.000 claims description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 2
- 235000015320 potassium carbonate Nutrition 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims 3
- 125000003118 aryl group Chemical group 0.000 claims 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 claims 1
- 125000003342 alkenyl group Chemical group 0.000 claims 1
- 125000003710 aryl alkyl group Chemical group 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 235000011118 potassium hydroxide Nutrition 0.000 claims 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- -1 1-tert-butylamino-2-phenyl-2-acryloylaminoethane Chemical compound 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
Landscapes
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Description
3 Пример 3. К раствору 0,6 г 1-трет-бутиламино-2-фенил - 2 - акрилоиламиноэтана в 7 мл спирта добавл ют 1,1 мл 20%-.ного водного формальдегида и 0,3 г поташа, нагревают 30 мин ири 100° С, /концентрируют в вакууме досуха, экстрагируют продукт 5x50 мл эфира, сушат экстракт сульфатом , отгон ют растворитель, перегон ют остаток в вакууме и получают 0,51 г (80,5%) 1-трет-бутил-З-аКрилоил-4-феннлимидазолидина . Свойства синтезир01ванных 1-г/9ет-бутил-3ацил-4-фенилимидазолидинов приведены в та-блице.3 Example 3. To a solution of 0.6 g of 1-tert-butylamino-2-phenyl-2-acryloylaminoethane in 7 ml of alcohol is added 1.1 ml of 20% aqueous formaldehyde and 0.3 g of potash, heated for 30 minutes Irie 100 ° C, / are concentrated in vacuo to dryness, the product is extracted with 5x50 ml of ether, the extract is dried with sulphate, the solvent is distilled off, the residue is distilled in vacuum and 0.51 g (80.5%) of 1-tert-butyl-3 is obtained aCryloyl-4-phennlimidazolidine. The properties of the synthesized 1-g / 9et-butyl-3 acyl-4-phenylimidazolidines are given in the table.
Использована окись алюмини II степени активности.Used alumina II degree of activity.
Claims (2)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU2086702A SU505637A1 (en) | 1974-12-24 | 1974-12-24 | The method of obtaining -acyl derivatives of the substituted imidazolidine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU2086702A SU505637A1 (en) | 1974-12-24 | 1974-12-24 | The method of obtaining -acyl derivatives of the substituted imidazolidine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU505637A1 true SU505637A1 (en) | 1976-03-05 |
Family
ID=20604318
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU2086702A SU505637A1 (en) | 1974-12-24 | 1974-12-24 | The method of obtaining -acyl derivatives of the substituted imidazolidine |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU505637A1 (en) |
-
1974
- 1974-12-24 SU SU2086702A patent/SU505637A1/en active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| SU498910A3 (en) | Method for preparing oxadiazolone derivatives | |
| SU628822A3 (en) | Method of producing 4'-epy-6'-oxyadriamycin hydrochloride | |
| SU505637A1 (en) | The method of obtaining -acyl derivatives of the substituted imidazolidine | |
| Bost et al. | Sulfur Studies. XIX. Alkyl Esters of Phenylthiocarbamic Acid1 | |
| SU466663A3 (en) | Method for preparing water soluble cephalosporin derivatives | |
| US2592418A (en) | Diuretic mercury compounds | |
| SU451698A1 (en) | The method of obtaining-acyl derivatives of substituted hexahydropyrimidines | |
| SU477159A1 (en) | Method for producing carboxylic acid amidophosphoryloxyethylamides | |
| US2712544A (en) | Chelating agents | |
| US3029239A (en) | Basic substituted 1-and 7-alkylxanthines or salts thereof | |
| SU496277A1 (en) | Method for preparing imidazole derivatives | |
| US3277172A (en) | Tetraphenylboron derivatives of tetracycline antibiotics | |
| US3004982A (en) | New benzimidazoles | |
| SU436057A1 (en) | METHOD OF OBTAINING ISOPROPYLIDENE DERIVATIVES OF PYRIDOXYN IN PT5FONM mmim | |
| US3280136A (en) | 5-substituted-2, 4-oxazolidinediones and magnesium chelate intermediates therefor | |
| US2832783A (en) | Preparation of piperazine adipate | |
| SU299163A1 (en) | Method of obtaining ammonium salts of b-alkoxyvinylpyrothiophosphonic acid amides | |
| SU401671A1 (en) | METHOD FOR OBTAINING ACYLTHYOURAIDOETHYLDYAMODODYTHIOPHOSPHATES | |
| SU491633A1 (en) | The method of obtaining derivatives of 1-hydroxy 1,2,5,6-tetrahydropyrimidine-3-oxide | |
| US2537004A (en) | Citric acid salts and their preparation | |
| SU570601A1 (en) | Diuretically active b-n-acylhydrazides of oxalic acid r-sulphonyl hydrozides | |
| SU455948A1 (en) | Method for producing substituted arenosulfonyloxamic acid hydrazides | |
| SU407888A1 (en) | METHOD FOR PRODUCING YN? H-BUTYL ETHER OF HYDRAZYNUGAL ACID | |
| Bradamante et al. | Activated C, H‐Acids: N‐Alkyl‐9‐fluorenimines. Preliminary communication | |
| SU568652A1 (en) | Method of obtaining tri-o-acetyl derivative a-beta-d-arabinefuranozyle of citozine or hydrochloride thereof |