SU480014A1 - Method for determining moisture in substances - Google Patents
Method for determining moisture in substancesInfo
- Publication number
- SU480014A1 SU480014A1 SU1809972A SU1809972A SU480014A1 SU 480014 A1 SU480014 A1 SU 480014A1 SU 1809972 A SU1809972 A SU 1809972A SU 1809972 A SU1809972 A SU 1809972A SU 480014 A1 SU480014 A1 SU 480014A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- substances
- determining moisture
- moisture
- determining
- acetone
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 3
- 239000000126 substance Substances 0.000 title description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
- 239000013543 active substance Substances 0.000 description 2
- RFVVBBUVWAIIBT-UHFFFAOYSA-N beryllium nitrate Chemical compound [Be+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O RFVVBBUVWAIIBT-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- SMQUZDBALVYZAC-UHFFFAOYSA-N salicylaldehyde Chemical compound OC1=CC=CC=C1C=O SMQUZDBALVYZAC-UHFFFAOYSA-N 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 229910052790 beryllium Inorganic materials 0.000 description 1
- ATBAMAFKBVZNFJ-UHFFFAOYSA-N beryllium atom Chemical compound [Be] ATBAMAFKBVZNFJ-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004020 luminiscence type Methods 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
Description
л ет 0,025-0,05 об. %. Предложенный способ дает возможность определ ть содержание влаги с точностью +5% в интервале от 0,025 до 5%.l et 0.025-0.05 about. % The proposed method makes it possible to determine the moisture content with an accuracy of + 5% in the range from 0.025 to 5%.
Пример. К 2 лл анализируемого органического вещества добавл ют 3 мл люминесцирующего раствора нитрата берилли с салициловым альдегидом и довод т до 100 мл осушенным ацетоном. Интен сивность измер ют через 1 час на флуориметре при 366 млгк нри 20° С и сравнивают с контрольным опытом. В контрольном опыте используют раствор, состо щий из 2 мл осущеиной исследуемой жидкости и 3 мл люминесцирующего раствора .Example. To 2 liters of the analyzed organic matter is added 3 ml of a luminescent solution of beryllium nitrate with salicylic aldehyde and brought to 100 ml with dried acetone. The intensity is measured after 1 hour on a fluorimeter at 366 mlgc at 20 ° C and compared with the control experiment. In the control experiment, a solution consisting of 2 ml of osuschein test liquid and 3 ml of a luminescent solution is used.
При определении влаги в сол х соли растирают , воду экстрагируют ацетоном н провод т определение, как описано выше.When determining the moisture in the salts, the salts are triturated, the water is extracted with acetone, and the determination is carried out as described above.
Предмет изобретени Subject invention
Способ определени влаги в веществах по гашению люминесценции оптически активного вещества, отличающийс тем, что, с целью повыщени точности определени и увеличени числа анализируемых соединений, в качестве оптически активного вещества используют комплексное соединение нитрата берилли с салициловым альдегидом в осушенном ацетоне .The method of determining the moisture in substances for quenching the luminescence of an optically active substance, characterized in that, in order to increase the accuracy of determination and increase the number of analyzed compounds, the complex compound of beryllium with salicylic aldehyde in dried acetone is used as an optically active substance.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1809972A SU480014A1 (en) | 1972-07-17 | 1972-07-17 | Method for determining moisture in substances |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1809972A SU480014A1 (en) | 1972-07-17 | 1972-07-17 | Method for determining moisture in substances |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU480014A1 true SU480014A1 (en) | 1975-08-05 |
Family
ID=20521730
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1809972A SU480014A1 (en) | 1972-07-17 | 1972-07-17 | Method for determining moisture in substances |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU480014A1 (en) |
-
1972
- 1972-07-17 SU SU1809972A patent/SU480014A1/en active
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