SU127348A1 - The method of obtaining aluminosilicone grease - Google Patents
The method of obtaining aluminosilicone greaseInfo
- Publication number
- SU127348A1 SU127348A1 SU632136A SU632136A SU127348A1 SU 127348 A1 SU127348 A1 SU 127348A1 SU 632136 A SU632136 A SU 632136A SU 632136 A SU632136 A SU 632136A SU 127348 A1 SU127348 A1 SU 127348A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- aluminosilicone
- grease
- obtaining
- temperature
- aluminum
- Prior art date
Links
Landscapes
- Lubricants (AREA)
Description
Недостаток известных смазывающих веществ, в частности силиконовых смазок, заключаетс в их значительной растворимости в органических растворител х, полимеризации и др., что затрудн ет их применение .A disadvantage of known lubricants, in particular silicone lubricants, is their significant solubility in organic solvents, polymerization, etc., which makes their application difficult.
Применение описываемого способа позвол ет получить алюмосиликоновые смазки, обладающие более хорошими показател ми в отнощении термостабильности и растворимости в органических растворител х . Способ основан на применении глицерина, тетраэтоксисилана и алюминиевой соли. Особенность способа состоит в том, что дл загущени тетраэтоксисилана используют глицериновый раствор глицерата алюмини .The application of the described method allows to obtain aluminosilicone greases having better indicators with respect to thermal stability and solubility in organic solvents. The method is based on the use of glycerol, tetraethoxysilane and aluminum salt. The peculiarity of this method is that a glycerol solution of aluminum glycerate is used to thicken tetraethoxysilane.
Способ осуществл ют следующим путем.The method is carried out in the following way.
Дл получени глицерата алюмини берут 16,75 г А12(5О4)з ISHaO и раствор ют в 100 г глицерина при нагревании в течение I-1,5 час. до температуры около 165-167°, что способствует удалению влаги из раствора. Глицерат алюмини нагревают на песчаной бане при помешивании до 110-120° и прибавл ют к нему постепенно (из капельной воронки) в течение 20-30 мин. тетраэтоксисилан при энергичном непрерывном помешивании. Смесь выдерживают при температуре около 145-150° в течение 4-5 час. и затем при 167° в течение 1 часа. Образовавшиес при этом побочные продукты (спирт, этиловый эфир и др.) удал ют из реакционной массы на другой день путем повторного нагревани ее до температуры пор дка 150°. Полученна таким образом однородна прозрачна в зка масса обладает хорошими смазывающими свойствами, незначительной растворимостью (до 1%) во многих органических растворител х и термоустойчивостью при нагревании до температуры 130°.To obtain aluminum glycerate, 16.75 g of A12 (5O4) s ISHaO are taken and dissolved in 100 g of glycerin when heated for 1-1.5 hours. to a temperature of about 165-167 °, which helps remove moisture from the solution. Aluminum glycerate is heated on a sand bath with stirring to 110-120 ° and added to it gradually (from a dropping funnel) for 20-30 minutes. tetraethoxysilane with vigorous continuous stirring. The mixture is maintained at a temperature of about 145-150 ° for 4-5 hours. and then at 167 ° for 1 hour. The resulting by-products (alcohol, ethyl ether, etc.) are removed from the reaction mass on another day by re-heating it to a temperature of about 150 °. The homogeneous, transparent viscous mass thus obtained has good lubricating properties, insignificant solubility (up to 1%) in many organic solvents, and thermal stability when heated to a temperature of 130 °.
№ 127348- 2 -No. 127348-2 -
Предмет изобретени Subject invention
Способ получени алюмосиликоновой смазки, отличающийс тем, что дл загущени тетраэтоксисилапа используетс глицериновый раствор глицерата алюмини .A method for producing an aluminosilicone lubricant, characterized in that a glycerol solution of aluminum glycerate is used to thicken tetraethoxysilap.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU632136A SU127348A1 (en) | 1959-06-26 | 1959-06-26 | The method of obtaining aluminosilicone grease |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU632136A SU127348A1 (en) | 1959-06-26 | 1959-06-26 | The method of obtaining aluminosilicone grease |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU127348A1 true SU127348A1 (en) | 1959-11-30 |
Family
ID=48398602
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU632136A SU127348A1 (en) | 1959-06-26 | 1959-06-26 | The method of obtaining aluminosilicone grease |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU127348A1 (en) |
-
1959
- 1959-06-26 SU SU632136A patent/SU127348A1/en active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Kleiderer et al. | Stereochemistry of Diphenyls. XXXI. 1 Preparation and Properties of 2, 2', 6, 6'-Tetrafluoro-3, 3'-dicarboxy-5, 5'-dichlorodiphenyl | |
| JPS5365536A (en) | Oil pan | |
| GB652754A (en) | Silicone greases and method of preparation | |
| SU127348A1 (en) | The method of obtaining aluminosilicone grease | |
| GB781519A (en) | Acetoxymethylheptamethylcyclotetrasiloxane and oils prepared therefrom | |
| KR840001968A (en) | Method for preparing 4-phenylquinazoline derivative | |
| SU131433A1 (en) | The method of obtaining high-temperature lubricants | |
| US2642395A (en) | Siloxane boundary lubricants | |
| GB433257A (en) | Improvements relating to lubricating and like oils, and greases | |
| SU143803A1 (en) | The method of obtaining polydimethylsilylene | |
| ATE2151T1 (en) | FLUORINATED GRAPHITE-BASED ENAMEL LUBRICANTS AND PROCESSES FOR THEIR PRODUCTION AND USE. | |
| ES418833A1 (en) | 1-phenyl-2-cyanovinyl(thio)-phosphoric or-phosphonic acid esters | |
| SU393267A1 (en) | METHOD FOR OBTAINING AMINOMETHYL DERIVATIVE | |
| SE7605200L (en) | METHOD OF PREPARING 2-SUBSTITUTED 1,4-BENZODIAZEPIN DERIVATIVES | |
| SU131434A1 (en) | The method of producing greases based on alkyl and arylsiliconates of various metals | |
| SU570636A1 (en) | Plastic lubricant | |
| BREED et al. | Fluorinated esters of polycarboxylic acids(Fluorinated esters of polycarboxylic acid and lubricating compositions for use at extreme temperature)[Patent] | |
| SU134267A1 (en) | The method of obtaining hypoxanthine (alpha-oxypurine) | |
| SU495339A1 (en) | Lubricating composition | |
| SU117911A1 (en) | Method for producing lubricant for mobile high vacuum compounds | |
| GB975773A (en) | Improvements in or relating to the manufacture of photographic colour images | |
| US3206443A (en) | Thickening of high temperature greases | |
| KR930700440A (en) | Method for preparing 3,4,6-trifluorophthalic acid | |
| ES409552A1 (en) | Haloalkanesulphonic acid esters and their use in compositions for killing noxious organisms | |
| IT8023093A0 (en) | PROCEDURE FOR THE PREPARATION OF LUBRICATING OIL COMPOSITIONS CONTAINING MOLYBDENUM COMPOUNDS AS ANTIOXIDANT ADDITIVES. |