SG11201900068PA - Single crystal silicon plate-shaped body and production method therefor - Google Patents
Single crystal silicon plate-shaped body and production method thereforInfo
- Publication number
- SG11201900068PA SG11201900068PA SG11201900068PA SG11201900068PA SG11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA SG 11201900068P A SG11201900068P A SG 11201900068PA
- Authority
- SG
- Singapore
- Prior art keywords
- single crystal
- crystal silicon
- shaped body
- silicon plate
- ppma
- Prior art date
Links
- 229910021421 monocrystalline silicon Inorganic materials 0.000 title abstract 7
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 5
- 229910052760 oxygen Inorganic materials 0.000 abstract 5
- 239000001301 oxygen Substances 0.000 abstract 5
- 239000002244 precipitate Substances 0.000 abstract 3
- 238000010438 heat treatment Methods 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- 230000005540 biological transmission Effects 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
- C30B15/20—Controlling or regulating
- C30B15/206—Controlling or regulating the thermal history of growing the ingot
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/02—Elements
- C30B29/06—Silicon
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/60—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape characterised by shape
- C30B29/64—Flat crystals, e.g. plates, strips or discs
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10F—INORGANIC SEMICONDUCTOR DEVICES SENSITIVE TO INFRARED RADIATION, LIGHT, ELECTROMAGNETIC RADIATION OF SHORTER WAVELENGTH OR CORPUSCULAR RADIATION
- H10F71/00—Manufacture or treatment of devices covered by this subclass
- H10F71/121—The active layers comprising only Group IV materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Inorganic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
SINGLE CRYSTAL SILICON PLATE-SHAPED BODY AND PRODUCTION METHOD THEREFOR An object of the invention is to develop a single crystal silicon that becomes such a high-performance device as a solar cell or a power device in which decrease in lifetime is suppressed even if heating treatment from 800°C to 1100°C performed in a device production process is applied in a single crystal silicon plate-shaped body having a high oxygen concentration. Provided is a single crystal silicon plate-shaped body as cut out from an upper portion of a straight body portion of a CZ method single crystal silicon ingot in which an interstitial oxygen concentration in a crystal is 25 ppma to 45 ppma and a substitutional carbon concentration is 0.5 ppma or less in a radial center, wherein in the radial center, oxygen precipitates are not observed in a bulk in an image of 200,000 times by means of a transmission electron microscope, and after heating the single crystal silicon plate-shaped body at 950°C for 60 minutes, oxygen precipitates are observed in an image of the 200,000 times, and a shape of the oxygen precipitates is observed in a polyhedral structure in an image of 2,000,000 times. (Fig.1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2016134375 | 2016-07-06 | ||
PCT/JP2017/024235 WO2018008561A1 (en) | 2016-07-06 | 2017-06-30 | Single crystal silicon plate-shaped body and production method therefor |
Publications (1)
Publication Number | Publication Date |
---|---|
SG11201900068PA true SG11201900068PA (en) | 2019-02-27 |
Family
ID=60912812
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SG11201900068PA SG11201900068PA (en) | 2016-07-06 | 2017-06-30 | Single crystal silicon plate-shaped body and production method therefor |
Country Status (8)
Country | Link |
---|---|
US (1) | US10975496B2 (en) |
JP (1) | JP6484762B2 (en) |
KR (1) | KR102032535B1 (en) |
CN (1) | CN109477240B (en) |
DE (1) | DE112017003436T5 (en) |
SG (1) | SG11201900068PA (en) |
TW (1) | TWI732898B (en) |
WO (1) | WO2018008561A1 (en) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP6645545B1 (en) * | 2018-09-03 | 2020-02-14 | 株式会社Sumco | Method for evaluating carbon concentration of silicon sample, method for evaluating silicon wafer manufacturing process, method for manufacturing silicon wafer, and method for manufacturing silicon single crystal ingot |
JP6979007B2 (en) * | 2018-12-17 | 2021-12-08 | グローバルウェーハズ・ジャパン株式会社 | Ultra-low oxygen concentration measurement method for silicon wafers |
AU2020329758A1 (en) | 2019-08-09 | 2022-02-17 | Leading Edge Equipment Technologies, Inc. | Wafer with regions of low oxygen concentration |
EP4010519A4 (en) | 2019-08-09 | 2023-09-13 | Leading Edge Equipment Technologies, Inc. | PRODUCING A TAPE OR WAFER WITH AREAS OF LOW OXYGEN CONCENTRATION |
US20240018689A1 (en) * | 2021-09-28 | 2024-01-18 | Xi’An Eswin Material Technology Co., Ltd. | Crystal Puller for Pulling Monocrystalline Silicon Ingots |
CN115148858B (en) * | 2022-08-01 | 2024-06-11 | 安徽华晟新能源科技有限公司 | Passivation method of silicon solar cell |
US20240068122A1 (en) * | 2022-08-29 | 2024-02-29 | Globalwafers Co., Ltd. | Axial positioning of magnetic poles while producing a silicon ingot |
Family Cites Families (30)
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JPH03133121A (en) * | 1989-10-19 | 1991-06-06 | Showa Denko Kk | Silicon substrate for semiconductor device and manufacture thereof |
JPH0789789A (en) * | 1993-09-20 | 1995-04-04 | Fujitsu Ltd | Si crystal, crystal growth method and crystal growth apparatus |
US5593494A (en) * | 1995-03-14 | 1997-01-14 | Memc Electronic Materials, Inc. | Precision controlled precipitation of oxygen in silicon |
JP3006669B2 (en) | 1995-06-20 | 2000-02-07 | 信越半導体株式会社 | Method and apparatus for producing silicon single crystal having uniform crystal defects |
JPH09190954A (en) | 1996-01-10 | 1997-07-22 | Sumitomo Sitix Corp | Semiconductor substrate and method of manufacturing the same |
KR100351532B1 (en) * | 1996-07-29 | 2002-09-11 | 스미토모 긴조쿠 고교 가부시키가이샤 | Silicon epitaxial wafer and method for manufacturing the same |
US6503594B2 (en) | 1997-02-13 | 2003-01-07 | Samsung Electronics Co., Ltd. | Silicon wafers having controlled distribution of defects and slip |
JPH1143393A (en) * | 1997-07-23 | 1999-02-16 | Nippon Steel Corp | Silicon single crystal wafer and method of manufacturing the same |
JP4112654B2 (en) * | 1997-09-19 | 2008-07-02 | シルトロニック・ジャパン株式会社 | Method for manufacturing silicon wafer |
US6328795B2 (en) | 1998-06-26 | 2001-12-11 | Memc Electronic Materials, Inc. | Process for growth of defect free silicon crystals of arbitrarily large diameters |
TW505710B (en) * | 1998-11-20 | 2002-10-11 | Komatsu Denshi Kinzoku Kk | Production method for silicon single crystal and production device for single crystal ingot, and heat treating method for silicon single crystal wafer |
WO2000055397A1 (en) * | 1999-03-16 | 2000-09-21 | Shin-Etsu Handotai Co., Ltd. | Production method for silicon wafer and silicon wafer |
JP2002043318A (en) * | 2000-07-28 | 2002-02-08 | Shin Etsu Handotai Co Ltd | Method for manufacturing silicon single crystal wafer |
JP2002184779A (en) * | 2000-12-13 | 2002-06-28 | Shin Etsu Handotai Co Ltd | Annealed wafer and method of manufacturing the same |
US6846539B2 (en) * | 2001-01-26 | 2005-01-25 | Memc Electronic Materials, Inc. | Low defect density silicon having a vacancy-dominated core substantially free of oxidation induced stacking faults |
EP1456875A2 (en) | 2001-12-21 | 2004-09-15 | MEMC Electronic Materials, Inc. | Ideal oxygen precipitating silicon wafers with nitrogen/carbon stabilized oxygen precipitate nucleation centers and process for making the same |
US7201800B2 (en) * | 2001-12-21 | 2007-04-10 | Memc Electronic Materials, Inc. | Process for making silicon wafers with stabilized oxygen precipitate nucleation centers |
WO2003088346A1 (en) * | 2002-04-10 | 2003-10-23 | Memc Electronic Materials, Inc. | Process for controlling denuded zone depth in an ideal oxygen precipitating silicon wafer |
KR100573473B1 (en) | 2004-05-10 | 2006-04-24 | 주식회사 실트론 | Silicon Wafer and Manufacturing Method Thereof |
US7700394B2 (en) * | 2004-06-30 | 2010-04-20 | Sumco Corporation | Method for manufacturing silicon wafer method |
CN1269186C (en) * | 2004-11-22 | 2006-08-09 | 浙江大学 | Carbon doped silicon sheet with internal impurity absorbing function and production thereof |
KR100939299B1 (en) * | 2005-07-27 | 2010-01-28 | 가부시키가이샤 사무코 | Silicon Wafer and Manufacturing Method Thereof |
JP2007194232A (en) * | 2006-01-17 | 2007-08-02 | Shin Etsu Handotai Co Ltd | Process for producing silicon single crystal wafer |
JP5151777B2 (en) * | 2008-07-30 | 2013-02-27 | 株式会社Sumco | Method for manufacturing silicon epitaxial wafer and silicon epitaxial wafer |
KR20100036155A (en) * | 2008-09-29 | 2010-04-07 | 매그나칩 반도체 유한회사 | Silicon wafer and fabrication method thereof |
JP5088338B2 (en) * | 2009-03-10 | 2012-12-05 | 信越半導体株式会社 | Method of pulling silicon single crystal |
JP2011228459A (en) | 2010-04-19 | 2011-11-10 | Sumco Corp | Silicon wafer and method of manufacturing the same |
JP5984448B2 (en) * | 2012-03-26 | 2016-09-06 | グローバルウェーハズ・ジャパン株式会社 | Silicon wafer |
JP5885305B2 (en) * | 2013-08-07 | 2016-03-15 | グローバルウェーハズ・ジャパン株式会社 | Silicon wafer and manufacturing method thereof |
CN104726931A (en) * | 2015-03-30 | 2015-06-24 | 江苏盎华光伏工程技术研究中心有限公司 | Single crystal furnace with annealing device and control method for single crystal furnace |
-
2017
- 2017-06-30 DE DE112017003436.1T patent/DE112017003436T5/en not_active Withdrawn
- 2017-06-30 JP JP2018526343A patent/JP6484762B2/en active Active
- 2017-06-30 KR KR1020187037710A patent/KR102032535B1/en not_active Expired - Fee Related
- 2017-06-30 WO PCT/JP2017/024235 patent/WO2018008561A1/en active Application Filing
- 2017-06-30 CN CN201780041617.XA patent/CN109477240B/en not_active Expired - Fee Related
- 2017-06-30 SG SG11201900068PA patent/SG11201900068PA/en unknown
- 2017-06-30 US US16/315,216 patent/US10975496B2/en active Active
- 2017-07-04 TW TW106122354A patent/TWI732898B/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
TW201816201A (en) | 2018-05-01 |
TWI732898B (en) | 2021-07-11 |
CN109477240B (en) | 2019-12-27 |
DE112017003436T5 (en) | 2019-03-21 |
CN109477240A (en) | 2019-03-15 |
JP6484762B2 (en) | 2019-03-13 |
KR20190007502A (en) | 2019-01-22 |
KR102032535B1 (en) | 2019-10-15 |
US20190161888A1 (en) | 2019-05-30 |
WO2018008561A1 (en) | 2018-01-11 |
US10975496B2 (en) | 2021-04-13 |
JPWO2018008561A1 (en) | 2018-11-29 |
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