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SG10201401683RA - Method for manufacturing high purity sulfuric acid - Google Patents

Method for manufacturing high purity sulfuric acid

Info

Publication number
SG10201401683RA
SG10201401683RA SG10201401683RA SG10201401683RA SG10201401683RA SG 10201401683R A SG10201401683R A SG 10201401683RA SG 10201401683R A SG10201401683R A SG 10201401683RA SG 10201401683R A SG10201401683R A SG 10201401683RA SG 10201401683R A SG10201401683R A SG 10201401683RA
Authority
SG
Singapore
Prior art keywords
sulfuric acid
high purity
manufacturing high
purity sulfuric
sulfur trioxide
Prior art date
Application number
SG10201401683RA
Inventor
Douglas Dove Curtis
Chang Goang-Cheng
Kung Yuen-Ming
Chan Hung-Wen
Hsu Wei-Hsuan
Original Assignee
Asia Union Electronic Chemical Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Asia Union Electronic Chemical Corp filed Critical Asia Union Electronic Chemical Corp
Publication of SG10201401683RA publication Critical patent/SG10201401683RA/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/90—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/88—Concentration of sulfuric acid
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00—Sulfur; Compounds thereof
    • C01B17/69—Sulfur trioxide; Sulfuric acid
    • C01B17/90—Separation; Purification
    • C01B17/901—Recovery from spent acids containing metallic ions, e.g. hydrolysis acids, pickling acids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/148—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step in combination with at least one evaporator

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Cleaning Or Drying Semiconductors (AREA)
  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

28 OF THE DISCLOSURE A method for manufacturing high purity sulfuric acid is provided. A mixed solution subsequently undergoes a first preheating step, a second preheating step, a distilling step and an evaporating step to remove peroxide, water, oxygen and insoluble impurities, so as to obtain the first gas containing sulfur trioxide, sulfuric acid and hydrogen oxide. And then, the sulfur trioxide is absorbed by a sulfuric acid solution, thereby forming the high purity sulfuric acid. Fig. 1
SG10201401683RA 2013-05-01 2014-04-22 Method for manufacturing high purity sulfuric acid SG10201401683RA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
TW102115629 2013-05-01
TW102138283A TWI481550B (en) 2013-05-01 2013-10-23 Method for manufacturing high purity sulfuric acid

Publications (1)

Publication Number Publication Date
SG10201401683RA true SG10201401683RA (en) 2014-12-30

Family

ID=51802681

Family Applications (1)

Application Number Title Priority Date Filing Date
SG10201401683RA SG10201401683RA (en) 2013-05-01 2014-04-22 Method for manufacturing high purity sulfuric acid

Country Status (7)

Country Link
US (2) US9926198B2 (en)
JP (1) JP6231427B2 (en)
KR (1) KR101598401B1 (en)
CN (1) CN104129762A (en)
MY (1) MY169334A (en)
SG (1) SG10201401683RA (en)
TW (1) TWI481550B (en)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105293449B (en) * 2015-10-30 2018-05-18 上海新阳半导体材料股份有限公司 A kind of method that sulfuric acid is recycled in spent acid from semiconductor cleaning process
CN105621374B (en) * 2016-02-16 2018-02-02 江苏达诺尔科技股份有限公司 A kind of preparation method of ultra-pure sulfuric acid
KR101675947B1 (en) 2016-05-03 2016-11-16 현대피.에프산업 (주) Device for producing high purity sulfuric acid
CN108483411A (en) * 2018-04-09 2018-09-04 四川高绿平环境科技有限公司 The processing unit and its processing method of hydrogen peroxide in a kind of removing sulfuric acid waste
CN109534302A (en) * 2018-11-13 2019-03-29 乳源东阳光电化厂 A kind of method and its application for removing dimethyl sulfate in sulfuric acid
CN110155955B (en) * 2019-04-01 2021-07-23 岷山环能高科股份公司 Production method for preparing electronic-grade sulfuric acid by using non-ferrous smelting flue gas
US11345594B2 (en) * 2019-12-13 2022-05-31 Veolia North America Regeneration Services, Llc Regeneration of acid containing peroxy acids of sulfur
RU200426U1 (en) * 2020-03-02 2020-10-23 Общество с ограниченной ответственностью «Аналит Продактс» CONTAINER FOR PURIFICATION OF LIQUIDS IN THE COMPOSITION OF A PLANT FOR OBTAINING SPECIALLY PURE SUBSTANCES
CN112079337B (en) * 2020-09-19 2023-08-15 韶关高科祥高新材料有限公司 Production method of electronic grade high-purity ultra-clean sulfuric acid
CN111994881A (en) * 2020-10-08 2020-11-27 江苏电科环保有限公司 Sulfuric acid recovery method and system
CN113336198B (en) * 2021-08-05 2021-10-15 清大国华环境集团股份有限公司 Method and system for recycling waste sulfuric acid in integrated circuit industry
US20240189772A1 (en) * 2022-12-07 2024-06-13 Sar Technology Inc. Method for recycling electronic-grade and industrial-grade sulfuric acid
KR102688740B1 (en) * 2023-10-30 2024-07-26 에스케이에코플랜트(주) Method for recovering high purity sulfuric acid from used solution containing hydrogen peroxide and various metallic impurities and apparatus thereof
KR102784880B1 (en) * 2024-06-14 2025-03-20 엘에스엠앤엠 주식회사 Pure Sulfuric Acid Production System

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1233368B (en) * 1962-08-13 1967-02-02 Heraeus Schott Quarzschmelze Process for the continuous distillation of sulfuric acid in apparatus made of ceramic materials
US3856673A (en) * 1973-04-02 1974-12-24 Air Prod & Chem Purification of spent sulfuric acid
CH641126A5 (en) * 1979-06-13 1984-02-15 Bertrams Ag Process and system for regenerating sulphuric acid
US5164049A (en) * 1986-10-06 1992-11-17 Athens Corporation Method for making ultrapure sulfuric acid
JP3257074B2 (en) * 1992-10-16 2002-02-18 富士通株式会社 Sulfuric acid regeneration equipment
JP3474280B2 (en) * 1994-09-02 2003-12-08 日曹エンジニアリング株式会社 Purification method of sulfuric acid
JPH08175810A (en) * 1994-12-22 1996-07-09 Nippon Sanso Kk Purification apparatus for waste sulfuric acid
JP3507317B2 (en) * 1996-12-20 2004-03-15 富士通株式会社 Distillation apparatus and distillation method
JP3375050B2 (en) * 1997-03-31 2003-02-10 富士通株式会社 Waste sulfuric acid continuous purification device and purification method
DE19963509A1 (en) * 1999-12-28 2001-07-05 Merck Patent Gmbh Process for the production of high-purity sulfuric acid
CN100335405C (en) * 2005-06-16 2007-09-05 武汉青江化工股份有限公司 Analytical pure sulfuric acid production process
CN202829582U (en) * 2012-09-27 2013-03-27 武汉市永发化工制造有限公司 Reagent sulfuric acid purifying and heating device

Also Published As

Publication number Publication date
TW201442944A (en) 2014-11-16
TWI481550B (en) 2015-04-21
KR101598401B1 (en) 2016-02-29
JP2014218423A (en) 2014-11-20
US10351427B2 (en) 2019-07-16
KR20140130632A (en) 2014-11-11
MY169334A (en) 2019-03-21
JP6231427B2 (en) 2017-11-15
US20180162731A1 (en) 2018-06-14
US20140326593A1 (en) 2014-11-06
US9926198B2 (en) 2018-03-27
CN104129762A (en) 2014-11-05

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