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RU96123869A - METHOD FOR PRODUCING DIETHYLMETOXYBORANE - Google Patents

METHOD FOR PRODUCING DIETHYLMETOXYBORANE

Info

Publication number
RU96123869A
RU96123869A RU96123869/04A RU96123869A RU96123869A RU 96123869 A RU96123869 A RU 96123869A RU 96123869/04 A RU96123869/04 A RU 96123869/04A RU 96123869 A RU96123869 A RU 96123869A RU 96123869 A RU96123869 A RU 96123869A
Authority
RU
Russia
Prior art keywords
producing
diethylmetoxyborane
triethylborane
pivalic acid
diethylmethoxyborane
Prior art date
Application number
RU96123869/04A
Other languages
Russian (ru)
Other versions
RU2102397C1 (en
Inventor
Е.А. Желудов
Б.А. Селяков
О.В. Сучкова
М.А. Ульянцев
Original Assignee
Открытое акционерное общество "Авиабор"
Дзержинский опытный завод авиационных материалов
Filing date
Publication date
Application filed by Открытое акционерное общество "Авиабор", Дзержинский опытный завод авиационных материалов filed Critical Открытое акционерное общество "Авиабор"
Priority to RU96123869A priority Critical patent/RU2102397C1/en
Priority claimed from RU96123869A external-priority patent/RU2102397C1/en
Application granted granted Critical
Publication of RU2102397C1 publication Critical patent/RU2102397C1/en
Publication of RU96123869A publication Critical patent/RU96123869A/en

Links

Claims (1)

Способ получения диэтилметоксиборана, включающий взаимодействие триэтилборана с метиловым спиртом в присутствии пивалевой кислоты, отличающийся тем, что процесс ведут при молярном соотношении триэтилборана, метанола и пивалевой кислоты, равном 1 : (1,005 - 1,01) : (0,005 - 0,01) и температуре 2 - 10oС, полученную реакционную массу выдерживают при 18 - 22oС с последующим выделением целевого продукта ректификацией.A method of producing diethylmethoxyborane, including the interaction of triethylborane with methyl alcohol in the presence of pivalic acid, characterized in that the process is carried out at a molar ratio of triethylborane, methanol and pivalic acid equal to 1: (1.005 - 1.01): (0.005 - 0.01) and a temperature of 2 - 10 o C, the resulting reaction mass is maintained at 18 - 22 o C, followed by isolation of the target product by distillation.
RU96123869A 1996-12-24 1996-12-24 Method for producing diethylmethoxy borane RU2102397C1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU96123869A RU2102397C1 (en) 1996-12-24 1996-12-24 Method for producing diethylmethoxy borane

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU96123869A RU2102397C1 (en) 1996-12-24 1996-12-24 Method for producing diethylmethoxy borane

Publications (2)

Publication Number Publication Date
RU2102397C1 RU2102397C1 (en) 1998-01-20
RU96123869A true RU96123869A (en) 1998-02-10

Family

ID=20188284

Family Applications (1)

Application Number Title Priority Date Filing Date
RU96123869A RU2102397C1 (en) 1996-12-24 1996-12-24 Method for producing diethylmethoxy borane

Country Status (1)

Country Link
RU (1) RU2102397C1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103483366B (en) * 2013-09-05 2017-02-08 润泽制药(苏州)有限公司 Preparation method of methoxy diethyl borane
CN117402184B (en) * 2023-12-15 2024-04-26 山东国邦药业有限公司 Preparation method of diethyl methoxyborane
CN119264170A (en) * 2024-12-12 2025-01-07 山东国邦药业有限公司 A kind of preparation method of diethylmethoxyborane

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