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RU96121629A - COATING SYSTEM OF NEUTRAL HIGH-QUALITY GLASS WITH LOW RADIATIVE ABILITY, MANUFACTURED FROM IT, INSULATING GLASS BLOCKS, AND METHOD OF THEIR MANUFACTURE - Google Patents

COATING SYSTEM OF NEUTRAL HIGH-QUALITY GLASS WITH LOW RADIATIVE ABILITY, MANUFACTURED FROM IT, INSULATING GLASS BLOCKS, AND METHOD OF THEIR MANUFACTURE

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Publication number
RU96121629A
RU96121629A RU96121629/03A RU96121629A RU96121629A RU 96121629 A RU96121629 A RU 96121629A RU 96121629/03 A RU96121629/03 A RU 96121629/03A RU 96121629 A RU96121629 A RU 96121629A RU 96121629 A RU96121629 A RU 96121629A
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RU
Russia
Prior art keywords
glass
sheets
coated
insulating
film system
Prior art date
Application number
RU96121629/03A
Other languages
Russian (ru)
Other versions
RU2124483C1 (en
Inventor
Клаус В. Хартинг
Стивен Л. Ларсон
Филип Дж. Лингл
Original Assignee
Гардиян Индастриз Корп.,
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Publication date
Application filed by Гардиян Индастриз Корп., filed Critical Гардиян Индастриз Корп.,
Application granted granted Critical
Publication of RU2124483C1 publication Critical patent/RU2124483C1/en
Publication of RU96121629A publication Critical patent/RU96121629A/en

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Claims (1)

1. Покрытое напылением стеклянное изделие, состоящее из стеклянной подложки, имеющей на ее плоской поверхности, кнаружи от стекла, пленочную систему, включающую в себя: а) слой, содержащий Si3N4 и нержавеющую сталь, причем нержавеющая сталь составляет в количественном отношении 0,5 - 15% по весу от упомянутого слоя; б) слой никеля или нихрома; в) слой серебра; г) слой никеля или нихрома; и д) слой, содержащий Si3N4 и нержавеющую сталь, причем нержавеющая сталь составляет в количественном отношении 0,5 - 15% по весу от упомянутого слоя, при этом если упомянутая стеклянная подложка имеет толщину от 2 до 6 мм, то упомянутая покрытая стеклянная подложка имеет излучательную способность по нормали (Еn) около 0,06 или меньше, излучательную способность в полусферу (Еh) около 0,07 или меньше, листовое сопротивление (Rs) около 5,0 ом/кв, или меньше и имеет практически нейтральный цвет отраженного видимого излучения при взгляде со стороны стекла.1. A glass-coated product consisting of a glass substrate having on its flat surface, outwards from the glass, a film system comprising: a) a layer containing Si 3 N 4 and stainless steel, stainless steel being in quantitative terms 0 , 5 - 15% by weight of the above layer; b) a layer of nickel or nichrome; c) a layer of silver; d) a layer of nickel or nichrome; and d) a layer containing Si 3 N 4 and stainless steel, with stainless steel in a quantitative ratio of 0.5 to 15% by weight of said layer, while if said glass substrate has a thickness of from 2 to 6 mm, then said coated the glass substrate has a normal emissivity (E n ) of about 0.06 or less, a hemisphere emissivity (E h ) of about 0.07 or less, a sheet resistance (R s ) of about 5.0 ohm / sq, or less and has almost neutral color of the reflected visible radiation when viewed from the side of the glass. 2. Покрытое напылением стеклянное изделие по п. 1, в котором упомянутая покрытая стеклянная подложка имеет коэффициент пропускания в видимом диапазоне по меньшей мере около 70%. 2. The coated glass product of claim 1, wherein said coated glass substrate has a transmittance in the visible range of at least about 70%. 3. Покрытое напылением стеклянное изделие по п. 1, в котором упомянутое стеклянное изделие способно подвергаться тепловой обработке. 3. The coated glass product according to claim 1, wherein said glass product is capable of being heat-treated. 4. Покрытое напылением стеклянное изделие по п. 1, в котором упомянутая пленочная система дополнительно включает в себя подслой, состоящий из TiO2, и слои имеют следующие толщины
слой - толщина
Figure 00000001

подслой - 100 - 400
а - 20 - 120
б - 7 - 50
в - 75 - 225
г - 7 - 30
д - 50 - 600
5. Покрытое напылением стеклянное изделие по п. 4, в котором упомянутая стеклянная подложка имеет излучательную способность по нормали (En) около 0,05 или меньше, излучательную способность в полусферу (Еh) около 0,06 или меньше, листовое сопротивление (Rs) около 5,0 ом/кв, или меньше.4. The coated glass product of claim 1, wherein said film system further includes an underlayer consisting of TiO 2 and layers have the following thickness
layer - thickness
Figure 00000001

sublayer - 100 - 400
a - 20 - 120
b - 7 - 50
in - 75 - 225
g - 7 - 30
d - 50 - 600
5. The coated glass product of claim 4, wherein said glass substrate has an emissivity normal (E n ) of about 0.05 or less, a hemisphere emissivity (E h ) of about 0.06 or less, sheet resistance ( R s ) about 5.0 ohms / sq, or less. 6. Покрытое напылением стеклянное изделие по п. 5, состоящее по существу из упомянутых подслоя и слоев (а) - (д), в котором упомянутая нержавеющая сталь в упомянутых слоях (а) и (д) составляет около 6% по весу упомянутого слоя. 6. The coated glass product according to claim 5, consisting essentially of said underlayer and layers (a) - (d), in which said stainless steel in said layers (a) and (d) is about 6% by weight of said layer . 7. Покрытое напылением стеклянное изделие по п. 6, в котором слои имеют следующие толщины
слой - толщина
Figure 00000002

подслой - 200-250
а - 40-60
б - 7-30
в - 150-180
г - 7-15
д - 400-500
8. Покрытое напылением стеклянное изделие по п. 7, в котором упомянутые слои (б) и (г) содержат нитрид хрома и упомянутая нержавеющая сталь содержит нитрид хрома.7. Spray-coated glass product according to claim 6, in which the layers have the following thickness
layer - thickness
Figure 00000002

sublayer - 200-250
a - 40-60
b - 7-30
in - 150-180
g - 7-15
d - 400-500
8. The glass-coated glass product of claim 7, wherein said layers (b) and (d) comprise chromium nitride and said stainless steel contains chromium nitride. 9. Покрытое напылением стеклянное изделие по п. 8, в котором слои имеют следующие толщины:
слой - толщина
Figure 00000003

подслой - 225
а - 50
б - 20
в - 165
г - 7
д - 450
и в котором стеклянная подложка с упомянутой пленочной системой на ней имеет следующие характеристики
со стороны стекла
RgY около - 11,0
аh - около 2,3
bh - около-8,8
со стороны пленки
RFY - около 6,0
аh - около 5,4
bh - около17,5
где RY есть коэффициент отражения, а аh, bh есть цветовые координаты, измеренные в единицах Хантера, с эталонным источником света в 1 свечу, под углом наблюдения 10°, и в котором упомянутая пленочная система является механически и химически стойкой и имеет коэффициент пропускания в видимом диапазоне около 76%.9. The coated glass product of claim. 8, in which the layers have the following thickness:
layer - thickness
Figure 00000003

sublayer - 225
a - 50
b - 20
in - 165
g - 7
d - 450
and in which the glass substrate with said film system on it has the following characteristics
on the glass side
RgY around - 11.0
and h - about 2.3
b h - about 8.8
from the side of the film
R F Y - about 6.0
h is about 5.4
b h - about 17.5
where RY is the reflection coefficient, and h , b h are color coordinates, measured in Hunter units, with a reference light source in 1 candle, at an observation angle of 10 °, and in which the mentioned film system is mechanically and chemically resistant and has a transmittance in the visible range of about 76%. 10. Покрытое напылением стеклянное изделие по п. 9, в котором упомянутая пленочная система является обрабатываемой теплом. 10. The coated glass product of claim 9, wherein said film system is heat treated. 11. Покрытое напылением стеклянное изделие по п. 1, в котором упомянутая пленочная система состоит из упомянутых слоев (а) - (д) и упомянутые слои имеют следующие толщины
слой - толщина
Figure 00000004

а - 200-600
б - 7-50
в - 115-190
г - 7-30
д - 50-600
12. Покрытое напылением стеклянное изделие по п. 11, в котором слои имеют следующие толщины
слой - толщина
Figure 00000005

а - 400-500
б - 7-30
в - 140-170
г - 7-15
д - 400-600
13. Покрытое напылением стеклянное изделие по п. 12, в котором упомянутая пленочная система является химически и механически стойкой.11. The coated glass product of claim 1, wherein said film system consists of said layers (a) - (d) and said layers have the following thickness
layer - thickness
Figure 00000004

a - 200-600
b - 7-50
in - 115-190
g - 7-30
d - 50-600
12. The glass-coated product according to claim 11, wherein the layers have the following thicknesses
layer - thickness
Figure 00000005

a - 400-500
b - 7-30
in - 140-170
g - 7-15
d - 400-600
13. The coated glass product according to claim 12, wherein said film system is chemically and mechanically resistant. 14. Покрытое напылением стеклянное изделие по п. 13, в которой упомянутые слои имеют следующие толщины
слой - толщина
Figure 00000006

а - 450
б - 20
в - 155
г - 7
д - 550
и в котором упомянутая стеклянная подложка с упомянутой пленочной системой на ней имеет коэффициент пропускания в видимом диапазоне больше, чем 70%.14. A coated glass product according to claim 13, wherein said layers have the following thicknesses
layer - thickness
Figure 00000006

a - 450
b - 20
in - 155
g - 7
d - 550
and in which said glass substrate with said film system on it has a transmittance in the visible range greater than 70%. 15. Покрытое напылением стеклянное изделие по п. 14, в котором упомянутая стеклянная подложка с упомянутой пленочной системой на ней имеет следующие характеристики:
со стороны стекла
RGY - около 10,2
ah - около 0,4
bh - около -4,7
со стороны пленки
RFY - около 4,6
ah - около 6,5
bh - около-15,8
где RY есть коэффициент отражения, а ah, bh есть цветовые координаты, измеренные в единицах Хантера, с эталонным источником света в 1 свечу, под углом наблюдения 10°.15. A coated glass product according to claim 14, wherein said glass substrate with said film system on it has the following characteristics:
on the glass side
R G Y - about 10.2
a h - about 0.4
b h - about -4.7
from the side of the film
R F Y - about 4.6
a h - about 6.5
b h - about 15.8
where RY is the reflection coefficient, and a h , b h is the color coordinates, measured in Hunter units, with a reference light source of 1 candle, at an observation angle of 10 °. 16. Покрытое напылением стеклянное изделие по п. 15, в котором упомянутая пленочная система является обрабатываемой теплом. 16. A coated glass article according to claim 15, wherein said film system is heat to be processed. 17. Покрытое напылением стеклянное изделие по п. 16, в котором упомянутая нержавеющая сталь в слоях (а) и (д) составляет около 6% по весу упомянутого слоя. 17. The coated glass product of claim 16, wherein said stainless steel in layers (a) and (e) is about 6% by weight of said layer. 18. Покрытое напылением стеклянное изделие по п. 17, в котором упомянутые слои (б) и (г) содержат нитрид хрома и упомянутая нержавеющая сталь содержит нитрид хрома. 18. A coated glass product according to claim 17, wherein said layers (b) and (d) contain chromium nitride and said stainless steel contains chromium nitride. 19. Покрытое напылением стеклянное изделие по п. 1, в котором упомянутая нержавеющая сталь является нержавеющей сталью #316.
20. Покрытое напылением стеклянное изделие по п. 1, в котором упомянутая стеклянная подложка с упомянутой пленочной системой на ней имеет следующие характеристики
С со стороны стекла
RGY от 8 до 18
ah от -3 до +3
bh от 0 до -15
со стороны пленки
RFY от 4 до 15
ah от 0 до +8
bh от -5 до -20
где RY есть коэффициент отражения, а ah, bh есть цветовые координаты, измеренные в единицах Хантера, с эталонным источником света в 1 свечу, под углом наблюдения 10°.19. A coated glass article according to claim 1, wherein said stainless steel is # 316 stainless steel.
20. The glass-coated glass product of claim 1, wherein said glass substrate with said film system on it has the following characteristics
From the side of the glass
R G Y from 8 to 18
a h from -3 to +3
b h from 0 to -15
from the side of the film
R F Y from 4 to 15
a h from 0 to +8
b h from -5 to -20
where RY is the reflection coefficient, and a h , b h is the color coordinates, measured in Hunter units, with a reference light source of 1 candle, at an observation angle of 10 °. 21. Покрытое напылением стеклянное изделие по п. 20, в котором характеристики со стороны стекла и со стороны пленки составляют
со стороны стекла
RGY от 9 до 15
ah от -1 до +3
bh от -4 до -10
со стороны пленки
RFY от 4 до 10
ah от +3 до +7
bh от -10 до -20.21. A coated glass product according to claim 20, wherein the characteristics on the glass side and on the film side are
on the glass side
R G Y from 9 to 15
a h from -1 to +3
b h from -4 to -10
from the side of the film
R F Y from 4 to 10
a h from +3 to +7
b h from -10 to -20. 22. Покрытое напылением стеклянное изделие по п. 1, в котором упомянутый коэффициент пропускания в видимом диапазоне упомянутой покрытой стеклянной подложки составляет 74 - 76%. 22. The glass-coated glass product of claim 1, wherein said transmittance in the visible range of said coated glass substrate is 74-76%. 23. Изоляционный стеклянный блок, состоящий по меньшей мере из двух практически параллельных разнесенных листов стекла, в котором по меньшей мере один лист стекла является покрытым напылением листом стекла по п. 1. 23. Insulating glass unit consisting of at least two practically parallel spaced glass sheets, in which at least one glass sheet is a coated glass sheet according to claim 1. 24. Изоляционный стеклянный блок по п. 23, в котором упомянутые два листа стекла совместно герметизированы по их краям для образования тем самым между ними изолирующей камеры, и в котором упомянутая пленочная система расположена на поверхности одного из упомянутых стеклянных листов внутри упомянутой изолирующей камеры, а коэффициент отражения и цветовые характеристики при взгляде снаружи составляют
RGY от 14 до 20
ah от -2 до +2
bh от 0 до -10,
при взгляде изнутри составляют:
RFY от 11 до 18
аh от 0 до +4
bh от 0 до -10,
а коэффициент пропускания в видимом диапазоне составляет по меньшей мере 61 %.24. The insulating glass unit of claim 23, wherein said two sheets of glass are jointly sealed at their edges to thereby form an insulating chamber between them, and wherein said film system is located on the surface of one of said glass sheets inside said insulating chamber, and reflection coefficient and color characteristics when viewed from the outside are
R G Y from 14 to 20
a h from -2 to +2
b h from 0 to -10,
when viewed from the inside are:
R F Y from 11 to 18
h from 0 to +4
b h from 0 to -10,
and the transmittance in the visible range is at least 61%. 25. Изоляционный стеклянный блок по п. 24, в котором упомянутый блок представляет собой изолирующее стеклянное окно, дверь или стену, и коэффициент пропускания в видимом диапазоне составляет по меньшей мере 63%. 25. Insulating glass unit according to claim 24, in which said unit is an insulating glass window, door or wall, and the transmittance in the visible range is at least 63%. 26. Изоляционный стеклянный блок, содержащий по меньшей мере два практически параллельных разнесенных листа стекла, совместно герметизированных по их краям для образования тем самым между ними изолирующей камеры, в котором по меньшей мере из упомянутых стеклянных листов является покрытым напылением листом стекла по п. 4. причем упомянутая пленочная система расположена внутри упомянутой изолирующей камеры. 26. An insulating glass block comprising at least two substantially parallel spaced sheets of glass, jointly sealed at their edges, thereby forming an insulating chamber between them, in which at least of the said glass sheets is a sprayed glass sheet according to claim 4. moreover, said film system is located inside said insulating chamber. 27. Изоляционный стеклянный блок, содержащий по меньшей мере два практически параллельных разнесенных листа стекла, совместно герметизированных по их краям для образования тем самым между ними изолирующей камеры, в котором по меньшей мере из упомянутых стеклянных листов является покрытым напылением листом стекла по п. 8, причем упомянутая пленочная система расположена внутри упомянутой изолирующей камеры. 27. An insulating glass block comprising at least two substantially parallel spaced glass sheets, jointly sealed at their edges, thereby forming an insulating chamber between them, in which at least of the said glass sheets is a sprayed glass sheet according to claim 8, moreover, said film system is located inside said insulating chamber. 28. Изоляционный стеклянный блок, содержащий по меньшей мере два практически параллельных разнесенных листа стекла, совместно герметизированных теплом по их краям и образующих между собой практически свободную от воздуха изолирующую камеру, в котором по меньшей мере один из упомянутых стеклянных листов является покрытым напылением листом стекла по п. 10, причем упомянутая пленочная система расположена внутри упомянутой изолирующей камеры. 28. An insulating glass block containing at least two practically parallel spaced sheets of glass, jointly sealed with heat at their edges and forming an insulating chamber practically free of air between them, in which at least one of the said glass sheets is covered with a spraying glass sheet 10, and the above-mentioned film system is located inside the said insulating chamber. 29. Изоляционный стеклянный блок, содержащий по меньшей мере два практически параллельных разнесенных листа стекла, совместно герметизированных по их краям для образования тем самым между ними изолирующей камеры, в котором по меньшей мере из упомянутых стеклянных листов является покрытым напылением листом стекла по п.11, причем упомянутая пленочная система расположена внутри упомянутой изолирующей камеры. 29. An insulating glass unit comprising at least two substantially parallel spaced glass sheets, jointly sealed at their edges, thereby forming an insulating chamber between them, in which at least one of the said glass sheets is a sprayed glass sheet according to claim 11, moreover, said film system is located inside said insulating chamber. 30. Изоляционный стеклянный блок, содержащий по меньшей мере два практически параллельных разнесенных листа стекла, совместно герметизированных по их краям для образования тем самым между ними изолирующей камеры, в котором по меньшей мере из упомянутых стеклянных листов является покрытым напылением листом стекла по п. 13, причем упомянутая пленочная система расположена внутри упомянутой изолирующей камеры. 30. An insulating glass block comprising at least two substantially parallel spaced glass sheets, jointly sealed at their edges, thereby forming an insulating chamber between them, in which at least of the said glass sheets is a sprayed glass sheet according to claim 13, moreover, said film system is located inside said insulating chamber. 31. Изоляционный стеклянный блок, содержащий по меньшей мере два практически параллельных разнесенных листа стекла, совместно герметизированных теплом по их краям и образующих между собой практически свободную от воздуха изолирующую камеру, в котором по меньшей мере один из упомянутых стеклянных листов является покрытым напылением листом стекла по п. 18, причем упомянутая пленочная система расположена внутри упомянутой изолирующей камеры. 31. An insulating glass block containing at least two practically parallel spaced sheets of glass, jointly sealed with heat at their edges and forming an insulating chamber, which is practically free from air, in which at least one of the said glass sheets is covered by spraying a glass sheet 18, and said film system is located inside said insulating chamber. 32. В способе изготовления изоляционного стеклянного блока, содержащего по меньшей мере два листа стекла, герметизированных по их краям друг с другом для образования тем самым между ними по меньшей мере одной изолирующей камеры, упомянутый способ включает в себя операции разнесения упомянутых стеклянных листов друг от друга, нагрева упомянутых листов при повышенной температуре и припайки краев упомянутых листов друг к другу при повышенной или еще более высокой температуре, усовершенствование содержит использование, по меньшей мере в качестве одного из упомянутых стеклянных листов, упомянутого покрытого напылением стеклянного изделия по п. 3, расположенного так, что упомянутая пленочная система на нем находится внутри упомянутой изолирующей камеры. 32. In a method of manufacturing an insulating glass block containing at least two sheets of glass sealed at their edges with each other, thereby forming between at least one insulating chamber between them, said method includes separating said glass sheets from one another , heating said sheets at elevated temperatures and soldering the edges of said sheets to each other at elevated or even higher temperatures, the improvement includes using ETS of one of said glass sheets, said sputter-coated glass article according to claim. 3 disposed so that said film system thereon is within said insulating chamber. 33. В способе по п. 32, в котором по меньшей мере один из упомянутых стеклянных листов является покрытым напылением стеклянным изделием по п. 10. 33. In the method according to claim 32, wherein at least one of said glass sheets is a spray-coated glass article according to claim 10. 34. В способе по п. 32, в котором по меньшей мере один из упомянутых стеклянных листов является покрытым напылением стеклянным изделием по п. 16. 34. In the method according to claim 32, wherein at least one of said glass sheets is a spray-coated glass article according to claim 16.
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