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RU2008133052A - AUXILIARY FILTER MATERIAL BASED ON MICROCRYSTALLINE CELLULOSE - Google Patents

AUXILIARY FILTER MATERIAL BASED ON MICROCRYSTALLINE CELLULOSE Download PDF

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Publication number
RU2008133052A
RU2008133052A RU2008133052/15A RU2008133052A RU2008133052A RU 2008133052 A RU2008133052 A RU 2008133052A RU 2008133052/15 A RU2008133052/15 A RU 2008133052/15A RU 2008133052 A RU2008133052 A RU 2008133052A RU 2008133052 A RU2008133052 A RU 2008133052A
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RU
Russia
Prior art keywords
material according
silica
sorbent
polyphenols
drinks
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Application number
RU2008133052/15A
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Russian (ru)
Other versions
RU2406566C2 (en
Inventor
Андрей Леонидович Макаров (RU)
Андрей Леонидович Макаров
Борис Эдуардович Баташов (RU)
Борис Эдуардович Баташов
Original Assignee
Андрей Леонидович Макаров (RU)
Андрей Леонидович Макаров
Борис Эдуардович Баташов (RU)
Борис Эдуардович Баташов
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Priority to RU2008133052/05A priority Critical patent/RU2406566C2/en
Priority to PCT/RU2009/000382 priority patent/WO2010019077A1/en
Publication of RU2008133052A publication Critical patent/RU2008133052A/en
Application granted granted Critical
Publication of RU2406566C2 publication Critical patent/RU2406566C2/en

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/103—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/14—Diatomaceous earth
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/24—Naturally occurring macromolecular compounds, e.g. humic acids or their derivatives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/26—Synthetic macromolecular compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/26—Synthetic macromolecular compounds
    • B01J20/261—Synthetic macromolecular compounds obtained by reactions only involving carbon to carbon unsaturated bonds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/26—Synthetic macromolecular compounds
    • B01J20/262—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon to carbon unsaturated bonds, e.g. obtained by polycondensation
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/04—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material
    • C12H1/0408—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of inorganic added material
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/04—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material
    • C12H1/0416—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of organic added material
    • C12H1/0424—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of organic added material with the aid of a polymer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/44—Materials comprising a mixture of organic materials
    • B01J2220/445—Materials comprising a mixture of organic materials comprising a mixture of polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/46—Materials comprising a mixture of inorganic and organic materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/48—Sorbents characterised by the starting material used for their preparation
    • B01J2220/4812—Sorbents characterised by the starting material used for their preparation the starting material being of organic character
    • B01J2220/4825—Polysaccharides or cellulose materials, e.g. starch, chitin, sawdust, wood, straw, cotton

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Food Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)

Abstract

1. Вспомогательный фильтровальный материал, применяемый при фильтрации и/или стабилизации напитков, содержащих белки и/или полифенолы, и состоящий из микрокристаллической целлюлозы и из одного или более сорбентов белков и/или из одного или более сорбентов полифенолов. ! 2. Материал по п.1, в котором сорбентом полифенолов является сшитый полимер или сополимер N-виниллактама и предпочтительно сшитый поливинилпирролидон. ! 3. Материал по п.1, в котором сорбентом белков, является кремнезем в различных формах или производные кремнезема и предпочтительно производные кремниевой кислоты: золь (силиказоль), гидрогель (силикагель), ксерогель или обработанные кислотой силикаты щелочеземельных металлов. ! 4. Материал по п.1, в котором содержание каждого компонента составляет не менее 1 мас.% и предпочтительно не менее 5 мас.%. ! 5. Материал по п.1, в котором средний размер частиц каждого компонента находится в пределах от 1 до 500 мкм и предпочтительно в пределах от 10 до 100 мкм. ! 6. Материал по п.1 в виде гранул. ! 7. Материал по п.1, где термин напитки означает жидкости пищевого или медицинского назначения, получаемые из растительного сырья вывариванием, отжимом, экстракцией, сбраживанием и подобными методами, причем к данным жидкостям в основном относятся настои, экстракты, соки, вина и слабоалкогольные напитки, в особенности пиво и ему подобные продукты. ! 8. Способ изготовления материала по п.1, заключающийся в смешении его компонентов в воде или в водосодержащей жидкости (напитке) при высоком сдвиговом воздействии, причем содержание сухих компонентов в смеси составляет от 1 до 75% и предпочтительно от 10 до 40 мас.%. ! 9. Способ фильтрации и/или с�1. Auxiliary filter material used in the filtration and / or stabilization of beverages containing proteins and / or polyphenols, and consisting of microcrystalline cellulose and one or more protein sorbents and / or one or more polyphenol sorbents. ! 2. The material according to claim 1, in which the sorbent of polyphenols is a cross-linked polymer or a copolymer of N-vinyl lactam, and preferably cross-linked polyvinylpyrrolidone. ! 3. The material according to claim 1, in which the sorbent of proteins, is silica in various forms or derivatives of silica and preferably derivatives of silicic acid: sol (silica sol), hydrogel (silica gel), xerogel or acid-treated alkaline earth metal silicates. ! 4. The material according to claim 1, in which the content of each component is at least 1 wt.% And preferably at least 5 wt.%. ! 5. The material according to claim 1, in which the average particle size of each component is in the range from 1 to 500 microns and preferably in the range from 10 to 100 microns. ! 6. The material according to claim 1 in the form of granules. ! 7. The material according to claim 1, where the term drinks means liquids for food or medical purposes, obtained from plant materials by digestion, extraction, extraction, fermentation and similar methods, and these liquids mainly include infusions, extracts, juices, wines and low alcohol drinks , in particular beer and similar products. ! 8. The method of manufacturing the material according to claim 1, which consists in mixing its components in water or in an aqueous liquid (drink) under high shear, and the content of dry components in the mixture is from 1 to 75% and preferably from 10 to 40 wt.% . ! 9. Filtering method and / or c�

Claims (14)

1. Вспомогательный фильтровальный материал, применяемый при фильтрации и/или стабилизации напитков, содержащих белки и/или полифенолы, и состоящий из микрокристаллической целлюлозы и из одного или более сорбентов белков и/или из одного или более сорбентов полифенолов.1. Auxiliary filter material used in the filtration and / or stabilization of beverages containing proteins and / or polyphenols, and consisting of microcrystalline cellulose and one or more protein sorbents and / or one or more polyphenol sorbents. 2. Материал по п.1, в котором сорбентом полифенолов является сшитый полимер или сополимер N-виниллактама и предпочтительно сшитый поливинилпирролидон.2. The material according to claim 1, in which the sorbent of polyphenols is a cross-linked polymer or a copolymer of N-vinyl lactam, and preferably cross-linked polyvinylpyrrolidone. 3. Материал по п.1, в котором сорбентом белков, является кремнезем в различных формах или производные кремнезема и предпочтительно производные кремниевой кислоты: золь (силиказоль), гидрогель (силикагель), ксерогель или обработанные кислотой силикаты щелочеземельных металлов.3. The material according to claim 1, in which the sorbent of proteins, is silica in various forms or derivatives of silica and preferably derivatives of silicic acid: sol (silica sol), hydrogel (silica gel), xerogel or acid-treated alkaline earth metal silicates. 4. Материал по п.1, в котором содержание каждого компонента составляет не менее 1 мас.% и предпочтительно не менее 5 мас.%.4. The material according to claim 1, in which the content of each component is at least 1 wt.% And preferably at least 5 wt.%. 5. Материал по п.1, в котором средний размер частиц каждого компонента находится в пределах от 1 до 500 мкм и предпочтительно в пределах от 10 до 100 мкм.5. The material according to claim 1, in which the average particle size of each component is in the range from 1 to 500 microns and preferably in the range from 10 to 100 microns. 6. Материал по п.1 в виде гранул.6. The material according to claim 1 in the form of granules. 7. Материал по п.1, где термин напитки означает жидкости пищевого или медицинского назначения, получаемые из растительного сырья вывариванием, отжимом, экстракцией, сбраживанием и подобными методами, причем к данным жидкостям в основном относятся настои, экстракты, соки, вина и слабоалкогольные напитки, в особенности пиво и ему подобные продукты.7. The material according to claim 1, where the term drinks means liquids for food or medical purposes, obtained from plant materials by digestion, extraction, extraction, fermentation and similar methods, and these liquids mainly include infusions, extracts, juices, wines and low alcohol drinks , in particular beer and similar products. 8. Способ изготовления материала по п.1, заключающийся в смешении его компонентов в воде или в водосодержащей жидкости (напитке) при высоком сдвиговом воздействии, причем содержание сухих компонентов в смеси составляет от 1 до 75% и предпочтительно от 10 до 40 мас.%.8. The method of manufacturing the material according to claim 1, which consists in mixing its components in water or in an aqueous liquid (drink) under high shear, and the content of dry components in the mixture is from 1 to 75% and preferably from 10 to 40 wt.% . 9. Способ фильтрации и/или стабилизации напитков, отличающийся тем, что применяется материал по п.1.9. A method of filtering and / or stabilizing drinks, characterized in that the material according to claim 1 is used. 10. Способ по п.9, отличающийся тем, что используются мембранные фильтры.10. The method according to claim 9, characterized in that membrane filters are used. 11. Способ по п.9, отличающийся тем, что используются фильтры намывного типа.11. The method according to claim 9, characterized in that the alluvial type filters are used. 12. Способ по п.11, отличающийся тем, что материал по п.1 применяется в дополнение к основному фильтровальному материалу, в частности к кизельгуру.12. The method according to claim 11, characterized in that the material according to claim 1 is applied in addition to the main filter material, in particular to kieselguhr. 13. Способ по п.9, отличающийся тем, что после фильтрации и/или стабилизации проводится вспомогательная стабилизация напитка сорбентом полифенолов.13. The method according to claim 9, characterized in that after filtration and / or stabilization, auxiliary stabilization of the drink is carried out with a sorbent of polyphenols. 14. Способ по п.13, отличающийся тем, что в качестве сорбента полифенолов применяют материал по п.1. 14. The method according to item 13, wherein the material according to claim 1 is used as the polyphenol sorbent.
RU2008133052/05A 2008-08-11 2008-08-11 Material for increasing colloidal stability of drinks RU2406566C2 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
RU2008133052/05A RU2406566C2 (en) 2008-08-11 2008-08-11 Material for increasing colloidal stability of drinks
PCT/RU2009/000382 WO2010019077A1 (en) 2008-08-11 2009-08-04 The filter aid based on microcrystalline cellulose and method of its preparation

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Application Number Priority Date Filing Date Title
RU2008133052/05A RU2406566C2 (en) 2008-08-11 2008-08-11 Material for increasing colloidal stability of drinks

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RU2406566C2 RU2406566C2 (en) 2010-12-20

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EP2737942B1 (en) * 2011-07-29 2020-01-01 Toray Industries, Inc. Filter aid and method of manufacturing thereof
RU2608647C1 (en) * 2016-04-11 2017-01-23 Федеральное государственное бюджетное образовательное учреждение высшего образования "Кемеровский технологический институт пищевой промышленности (университет)" Method of stabilising beer
CN107955189B (en) * 2017-12-21 2021-02-26 陈明秦 Preparation method of hydrogel
WO2021077290A1 (en) * 2019-10-22 2021-04-29 浙江大学 Nanopore starch-based adsorbent and preparation method therefor
CN110922301B (en) * 2019-11-19 2021-12-17 山东福田药业有限公司 Method for extracting sugar alcohol from chewing gum waste
US11135567B1 (en) * 2020-06-26 2021-10-05 The Florida International University Board Of Trustees Microcrystalline cellulose particle supported sol-gel sorbents and methods of manufacturing the same
CN114470969A (en) * 2020-11-12 2022-05-13 四川远大蜀阳药业有限责任公司 A kind of depth filter medium and its use

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RU2406566C2 (en) 2010-12-20

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