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PL423396A1 - Method for producing carbonified halloysite adsorbent for adsorption of paracetamol from water phase - Google Patents

Method for producing carbonified halloysite adsorbent for adsorption of paracetamol from water phase

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Publication number
PL423396A1
PL423396A1 PL423396A PL42339617A PL423396A1 PL 423396 A1 PL423396 A1 PL 423396A1 PL 423396 A PL423396 A PL 423396A PL 42339617 A PL42339617 A PL 42339617A PL 423396 A1 PL423396 A1 PL 423396A1
Authority
PL
Poland
Prior art keywords
halloysite
weight
paracetamol
producing
scum
Prior art date
Application number
PL423396A
Other languages
Polish (pl)
Other versions
PL234357B1 (en
Inventor
Piotr M. Słomkiewicz
Nina Rędzia
Beata Szczepanik
Original Assignee
Univ Jana Kochanowskiego W Kielcach
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Univ Jana Kochanowskiego W Kielcach filed Critical Univ Jana Kochanowskiego W Kielcach
Priority to PL423396A priority Critical patent/PL234357B1/en
Publication of PL423396A1 publication Critical patent/PL423396A1/en
Publication of PL234357B1 publication Critical patent/PL234357B1/en

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  • Carbon And Carbon Compounds (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

Przedmiotem zgłoszenia jest sposób wytwarzania uwęglonego adsorbentu haloizytowego ze zwietrzeliny haloizytowej do usuwania paracetamolu z fazy wodnej, polegający na aktywacji kwasem siarkowym(VI) o stężeniu 20% wagowych odżelazionej zwietrzeliny haloizytowej (zawartość związków żelaza poniżej 0,4% wagowych) polega na dodawaniu do 20 części wagowych wodnego roztworu melasy o stężeniu 20% wagowych 4 części wagowych aktywowanej w kwasie siarkowym(VI) odżelazionej zwietrzeliny haloizytowej i mieszaniu całości przez 24 godziny i suszeniu przez 4 godziny w temperaturze 313 K a następnie karbonizuje mieszaninę zwietrzeliny haloizytowej i melasy, w atmosferze azotu z narostem temperatury 6 K/min., w zakresie temperatur 40 - 773 K i kolejno w stałej temperaturze 773 K przez 4 godziny.The subject of the application is a method for producing carbonized halloysite adsorbent from halloysite weathered for removal of paracetamol from the aqueous phase, consisting in the activation of sulfuric acid (VI) at a concentration of 20% by weight of ferric halloysite scum (iron content below 0.4% by weight) consists in adding up to 20 parts by weight 20% by weight aqueous molasses solution 4 parts by weight activated in sulfuric (VI) acid of ferric halloysite scum and mixing for 24 hours and drying for 4 hours at 313 K and then carbonized the mixture of halloysite scum and molasses under nitrogen with a temperature rise of 6 K / min, in the temperature range of 40 - 773 K, and subsequently at a constant temperature of 773 K for 4 hours.

PL423396A 2017-11-09 2017-11-09 Method for producing carbonified halloysite adsorbent for adsorption of paracetamol from water phase PL234357B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL423396A PL234357B1 (en) 2017-11-09 2017-11-09 Method for producing carbonified halloysite adsorbent for adsorption of paracetamol from water phase

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL423396A PL234357B1 (en) 2017-11-09 2017-11-09 Method for producing carbonified halloysite adsorbent for adsorption of paracetamol from water phase

Publications (2)

Publication Number Publication Date
PL423396A1 true PL423396A1 (en) 2019-05-20
PL234357B1 PL234357B1 (en) 2020-02-28

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ID=66518991

Family Applications (1)

Application Number Title Priority Date Filing Date
PL423396A PL234357B1 (en) 2017-11-09 2017-11-09 Method for producing carbonified halloysite adsorbent for adsorption of paracetamol from water phase

Country Status (1)

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PL (1) PL234357B1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL241310B1 (en) * 2020-12-22 2022-09-05 Univ Jana Kochanowskiego W Kielcach Method for the production of a halloysite-carbon adsorbent based on a carbon precursor from cellulose dissolved in Cross-Bewan's reagent for adsorption of triclosan from the liquid phase
CN114682214A (en) * 2022-03-17 2022-07-01 中国科学院广州能源研究所 Preparation method and application of attapulgite-based charcoal composite adsorbent
PL445628A1 (en) * 2023-07-18 2024-11-18 Uniwersytet Jana Kochanowskiego W Kielcach Method of producing halloysite-carbon material for isolating naproxen from the aqueous phase by solid-phase extraction

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
ROMAN KLIMKIEWICZ, CATALYTIC ACTIVITY OF CARBONACEOUS DEPOSITS IN ZEOLITE FROM HALLOYSITE IN ALCOHOL CONVERSIONS, 2004 *
ZHENG-HONG HUANG, MESOPOROUS CARBON NANOSHEETS DERIVED FROM TUBULAR HALLOYSITE AND FURFURYL ALCOHOL WITH DIFFERENT CONCENTRATIONS, 2010 *

Also Published As

Publication number Publication date
PL234357B1 (en) 2020-02-28

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