NO934233L - Fremgangsmaate for fremstilling av et silika aerogel-lignende materiale - Google Patents
Fremgangsmaate for fremstilling av et silika aerogel-lignende materialeInfo
- Publication number
- NO934233L NO934233L NO934233A NO934233A NO934233L NO 934233 L NO934233 L NO 934233L NO 934233 A NO934233 A NO 934233A NO 934233 A NO934233 A NO 934233A NO 934233 L NO934233 L NO 934233L
- Authority
- NO
- Norway
- Prior art keywords
- alcohol
- aqueous alcohol
- solution
- silica
- room temperature
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/16—Preparation of silica xerogels
- C01B33/163—Preparation of silica xerogels by hydrolysis of organosilicon compounds, e.g. ethyl orthosilicate
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
Abstract
Fremgangsmåte for fremstilling av silika xerogel ved hydrolyse og polykondensasjon av et tetraalkoksysilan for å danne en alkogel som er et silikaskjelett omgitt av vandig alkohol, hvorefter den vandige alkohol fjernes ved fordampning. Den dannede alkogel bringes i kontakt med en løsning av et tetraalkoksysilan, kontakten opprettholdes ved eller over romtemperatur for å styrke silikaskjelettet, hvorefter gelen tørkes langsomt ved eller over romtemperatur og ved omtrentlig atmosfærisk trykk. Før alkogelen bringes i kontakt med løsningen av tetraalkoksysilan kan den vaskes med en løsning (f.eks. vandig alkohol) for å endre sammensetningen av den vandige alkohol som omgir silikaskjelettet eller endre funksjonelle grupper på overflaten av alkogelen.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NO912006A NO912006D0 (no) | 1991-05-24 | 1991-05-24 | Fremgangsmaate for fremstilling av et silika-aerogel-lignende materiale. |
PCT/NO1992/000096 WO1992020623A1 (en) | 1991-05-24 | 1992-05-22 | Process for the preparation of a silica aerogel-like material |
Publications (2)
Publication Number | Publication Date |
---|---|
NO934233D0 NO934233D0 (no) | 1993-11-23 |
NO934233L true NO934233L (no) | 1993-11-23 |
Family
ID=19894166
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NO912006A NO912006D0 (no) | 1991-05-24 | 1991-05-24 | Fremgangsmaate for fremstilling av et silika-aerogel-lignende materiale. |
NO934233A NO934233L (no) | 1991-05-24 | 1993-11-23 | Fremgangsmaate for fremstilling av et silika aerogel-lignende materiale |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NO912006A NO912006D0 (no) | 1991-05-24 | 1991-05-24 | Fremgangsmaate for fremstilling av et silika-aerogel-lignende materiale. |
Country Status (7)
Country | Link |
---|---|
EP (1) | EP0646097A1 (no) |
JP (1) | JPH06510268A (no) |
BR (1) | BR9206051A (no) |
CA (1) | CA2109715A1 (no) |
FI (1) | FI935203A (no) |
NO (2) | NO912006D0 (no) |
WO (1) | WO1992020623A1 (no) |
Families Citing this family (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4439217A1 (de) * | 1994-11-03 | 1996-05-09 | Hoechst Ag | Verfahren zur Herstellung von Aerogelen |
DE19538333A1 (de) * | 1995-10-14 | 1997-04-17 | Basf Ag | Verfahren zur unterkritischen Herstellung von Aerogelen |
US6764690B2 (en) | 1996-05-29 | 2004-07-20 | Delsitech Oy | Dissolvable oxides for biological applications |
DE19718741A1 (de) | 1997-05-02 | 1998-11-05 | Hoechst Ag | Verfahren zur Kompaktierung von Aerogelen |
DE19718740A1 (de) | 1997-05-02 | 1998-11-05 | Hoechst Ag | Verfahren zur Granulierung von Aerogelen |
DE19756633A1 (de) | 1997-12-19 | 1999-06-24 | Hoechst Ag | Verfahren zur unterkritischen Trocknung von Lyogelen zu Aerogelen |
DE19801004A1 (de) | 1998-01-14 | 1999-07-15 | Cabot Corp | Verfahren zur Herstellung von im wesentlichen kugelförmigen Lyogelen in wasserunlöslichen Silylierungsmitteln |
EP1093486B1 (de) | 1998-06-05 | 2004-08-04 | Cabot Corporation | Nanoporöse interpenetrierende organisch-anorganische netzwerke |
US6239243B1 (en) * | 1999-06-10 | 2001-05-29 | Dow Corning Corporation | Method for preparing hydrophilic silica gels with high pore volume |
ES2174680B1 (es) * | 1999-09-03 | 2004-09-16 | Consejo Superior De Investigaciones Cientificas | Materiales termohibridos inorganico-organicos de baja densidad y su procedimiento de obtencion. |
GB0025940D0 (en) * | 2000-10-24 | 2000-12-13 | Secr Defence | Solvogels & a method of manufacturing the same |
JP4170734B2 (ja) | 2002-11-13 | 2008-10-22 | 信越化学工業株式会社 | 多孔質膜形成用組成物、多孔質膜とその製造方法、層間絶縁膜及び半導体装置 |
US8034749B2 (en) | 2002-12-31 | 2011-10-11 | Baker Hughes Incorporated | Aerogels effective to reduce drilling fluid density |
DK1718564T3 (en) * | 2004-02-27 | 2019-01-21 | Delsitech Oy | PROCEDURE FOR CONTROLLABLE PREPARATION OF BIORESORABLE SOL-GEL DERIVED SIO2 |
FR2873677B1 (fr) * | 2004-07-29 | 2007-08-17 | Armines Ass Pour La Rech Et Le | Procede d'elaboration de serogels de silice hydrophobes |
PT103257B (pt) | 2005-04-05 | 2007-05-31 | Inst Superior Tecnico | Método de produção subcrítica de xerogéis e aerogéis monolíticos híbridos de sílica e látex modificado com grupos alcoxissilano |
WO2007024925A2 (en) * | 2005-08-25 | 2007-03-01 | Keller Companies, Inc. | Aerogel and method of manufacturing same |
DE102008056987A1 (de) * | 2008-11-12 | 2010-05-20 | Rwe Power Ag | Isolierkassette |
DE102009053782A1 (de) * | 2009-11-19 | 2011-06-01 | BSH Bosch und Siemens Hausgeräte GmbH | Poröses SiO2-Xerogel mit charakteristischer Porengröße, dessen trocknungsstabile Vorstufen und dessen Anwendung |
DE102009053784A1 (de) * | 2009-11-19 | 2011-05-26 | BSH Bosch und Siemens Hausgeräte GmbH | Verfahren zur Herstellung eines porösen SiO2-Xerogels mit charakteristischer Porengröße durch ein Bottom-Up-Verfahren über eine Vorstufe mit organischen Festkörperskelettstützen |
PT106781A (pt) | 2013-02-15 | 2014-08-18 | Inst Superior Tecnico | Aerogéis híbridos flexíveis preparados em condições subcríticas e processo de preparação dos mesmos |
JP6191012B2 (ja) * | 2013-12-12 | 2017-09-06 | パナソニックIpマネジメント株式会社 | 断熱材 |
WO2017147463A1 (en) | 2016-02-24 | 2017-08-31 | Massachusetts Institute Of Technology | Solar thermal aerogel receiver and materials therefor |
KR102092770B1 (ko) * | 2016-09-12 | 2020-03-24 | 주식회사 엘지화학 | 실리카 에어로겔의 제조방법 및 이에 의해 제조된 실리카 에어로겔 |
KR102092769B1 (ko) | 2016-09-12 | 2020-03-24 | 주식회사 엘지화학 | 실리카 에어로겔의 제조방법 및 이에 의해 제조된 실리카 에어로겔 |
EP3677618A4 (en) * | 2017-09-01 | 2021-05-26 | AGC Inc. | WET GEL AND XEROGEL PRODUCTION PROCESSES |
WO2019210051A1 (en) | 2018-04-25 | 2019-10-31 | Massachusetts Institute Of Technology | Energy efficient soundproofing window retrofits |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SE422045C (sv) * | 1979-04-30 | 1985-03-18 | Guy Von Dardel | Sett att framstella silikaaerogel i form av ett vesentligen sprickfritt, foretredesvis transparent block samt anvendning av detsamma i solpaneler |
US4402927A (en) * | 1980-04-22 | 1983-09-06 | Dardel Guy Von | Silica aerogel |
DE3616133A1 (de) * | 1985-09-25 | 1987-11-19 | Merck Patent Gmbh | Kugelfoermige sio(pfeil abwaerts)2(pfeil abwaerts)-partikel |
DD283701A7 (de) * | 1988-09-26 | 1990-10-24 | Veb Leuna-Werke "Walter Ulbricht",Dd | Verfahren und vorrichtung zur herstellung organisch modifizierter silikagele |
-
1991
- 1991-05-24 NO NO912006A patent/NO912006D0/no unknown
-
1992
- 1992-05-22 EP EP92910393A patent/EP0646097A1/en not_active Ceased
- 1992-05-22 CA CA002109715A patent/CA2109715A1/en not_active Abandoned
- 1992-05-22 BR BR9206051A patent/BR9206051A/pt not_active Application Discontinuation
- 1992-05-22 JP JP4510552A patent/JPH06510268A/ja active Pending
- 1992-05-22 WO PCT/NO1992/000096 patent/WO1992020623A1/en not_active Application Discontinuation
-
1993
- 1993-11-23 NO NO934233A patent/NO934233L/no unknown
- 1993-11-23 FI FI935203A patent/FI935203A/fi not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
JPH06510268A (ja) | 1994-11-17 |
FI935203A0 (fi) | 1993-11-23 |
NO934233D0 (no) | 1993-11-23 |
EP0646097A1 (en) | 1995-04-05 |
AU662147B2 (en) | 1995-08-24 |
AU1785292A (en) | 1992-12-30 |
CA2109715A1 (en) | 1992-11-26 |
WO1992020623A1 (en) | 1992-11-26 |
FI935203A (fi) | 1994-01-13 |
NO912006D0 (no) | 1991-05-24 |
BR9206051A (pt) | 1994-11-15 |
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