NO773911L - Fremgangsmaate for fremstilling av etylenglykoler - Google Patents
Fremgangsmaate for fremstilling av etylenglykolerInfo
- Publication number
- NO773911L NO773911L NO773911A NO773911A NO773911L NO 773911 L NO773911 L NO 773911L NO 773911 A NO773911 A NO 773911A NO 773911 A NO773911 A NO 773911A NO 773911 L NO773911 L NO 773911L
- Authority
- NO
- Norway
- Prior art keywords
- ethylene oxide
- procedure
- stated
- glycol
- alkali metal
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 18
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 title description 6
- 239000005977 Ethylene Substances 0.000 title description 6
- 238000002360 preparation method Methods 0.000 title description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical class OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 50
- 238000004519 manufacturing process Methods 0.000 claims abstract description 19
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims description 27
- 239000007788 liquid Substances 0.000 claims description 19
- 238000006703 hydration reaction Methods 0.000 claims description 14
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 14
- 230000036571 hydration Effects 0.000 claims description 12
- 238000010521 absorption reaction Methods 0.000 claims description 9
- 229910000033 sodium borohydride Inorganic materials 0.000 claims description 9
- 239000012279 sodium borohydride Substances 0.000 claims description 9
- 229910052783 alkali metal Inorganic materials 0.000 claims description 7
- 150000001340 alkali metals Chemical class 0.000 claims description 7
- 150000001875 compounds Chemical class 0.000 claims description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 6
- 229910052760 oxygen Inorganic materials 0.000 claims description 6
- 239000001301 oxygen Substances 0.000 claims description 6
- 238000011282 treatment Methods 0.000 claims description 5
- 230000001502 supplementing effect Effects 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 18
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 150000002334 glycols Chemical class 0.000 description 7
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 5
- 238000000746 purification Methods 0.000 description 5
- 238000007380 fibre production Methods 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 235000011121 sodium hydroxide Nutrition 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 239000003344 environmental pollutant Substances 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 231100000719 pollutant Toxicity 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 1
- 230000008033 biological extinction Effects 0.000 description 1
- UORVGPXVDQYIDP-UHFFFAOYSA-N borane Chemical class B UORVGPXVDQYIDP-UHFFFAOYSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
- C07C29/10—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
- C07C29/103—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
- C07C29/10—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
- C07C29/103—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers
- C07C29/106—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers of oxiranes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/18—Polyhydroxylic acyclic alcohols
- C07C31/20—Dihydroxylic alcohols
- C07C31/202—Ethylene glycol
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT29386/76A IT1063805B (it) | 1976-11-17 | 1976-11-17 | Procedimento per la produzione di glicoli etilenici ad alta purezza |
Publications (1)
Publication Number | Publication Date |
---|---|
NO773911L true NO773911L (no) | 1978-05-19 |
Family
ID=11226884
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NO773911A NO773911L (no) | 1976-11-17 | 1977-11-15 | Fremgangsmaate for fremstilling av etylenglykoler |
Country Status (26)
Country | Link |
---|---|
US (1) | US4358625A (fr) |
JP (1) | JPS5363304A (fr) |
AR (1) | AR217090A1 (fr) |
AT (1) | AT359054B (fr) |
AU (1) | AU514202B2 (fr) |
BE (1) | BE860929A (fr) |
BR (1) | BR7707598A (fr) |
CS (1) | CS196408B2 (fr) |
DD (1) | DD133791A5 (fr) |
DE (1) | DE2751383B2 (fr) |
DK (1) | DK500077A (fr) |
ES (1) | ES464378A1 (fr) |
FR (1) | FR2371405A1 (fr) |
GB (1) | GB1560135A (fr) |
HU (1) | HU175533B (fr) |
IN (1) | IN146447B (fr) |
IT (1) | IT1063805B (fr) |
LU (1) | LU78518A1 (fr) |
NL (1) | NL7712471A (fr) |
NO (1) | NO773911L (fr) |
PL (1) | PL109691B1 (fr) |
RO (1) | RO71280A (fr) |
SE (1) | SE7712960L (fr) |
TR (1) | TR19507A (fr) |
YU (1) | YU270477A (fr) |
ZA (1) | ZA776810B (fr) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2831210B2 (de) * | 1978-07-15 | 1980-05-08 | Chemische Werke Huels Ag, 4370 Marl | Verfahren zur Reinigung von Ethyldiglykol und von Dipropylenglykol |
DE3001727A1 (de) * | 1980-01-18 | 1981-07-23 | Hoechst Ag, 6000 Frankfurt | Verfahren zur herstellung von hochreinem monoethylenglykol |
EP0226799B1 (fr) * | 1985-11-18 | 1992-01-02 | MITSUI TOATSU CHEMICALS, Inc. | Procédé pour la fabrication d'éthylène glycol et/ou de propylène glycol |
US4830712A (en) * | 1987-09-29 | 1989-05-16 | Union Carbide Corporation | Process for refining ethylene glycol |
US5196601A (en) * | 1989-12-26 | 1993-03-23 | Kao Corporation | Process for producing alcohol or amine |
DE4304465C2 (de) * | 1993-02-15 | 1995-01-05 | Schilling Chemie Gmbh U Produk | Verfahren zur Entfernung in Wasser gelösten Sauerstoffs, insbesondere in wasserführenden, geschlossenen Systemen |
JP4740432B2 (ja) * | 1999-07-14 | 2011-08-03 | 株式会社日本触媒 | エチレングリコールの精製方法 |
US6187973B1 (en) | 2000-04-06 | 2001-02-13 | Scientific Design Company, Inc. | Glycol purification |
US6242655B1 (en) * | 2000-07-11 | 2001-06-05 | Scientific Design Company, Inc. | Glycol purification |
TW200838838A (en) * | 2006-12-22 | 2008-10-01 | Dow Technology Investments Llc | Process for reducing side-reactions during alkylene glycol and poly-alkylene glycol manufacturing |
DE102009038398A1 (de) * | 2009-08-24 | 2011-03-03 | Uhde Gmbh | Verfahren und Vorrichtung zur Herstellung von Alkylenoxiden und von Alkylenglykolen |
MY182437A (en) * | 2013-10-23 | 2021-01-25 | Basf Se | Method for the preparation of 1, 4-butane diol having an apha color index of less than 30 |
CN107285997B (zh) | 2016-03-30 | 2022-04-22 | 长春美禾科技发展有限公司 | 一种改善乙二醇紫外透过率的方法 |
CN111662162B (zh) * | 2020-05-23 | 2022-08-12 | 安阳化学工业集团有限责任公司 | 一种提高煤制乙二醇紫外透光率所用的添加剂及其利用添加剂制备聚酯级乙二醇的方法 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1025852B (de) | 1954-11-19 | 1958-03-13 | Basf Ag | Verfahren zur Gewinnung reiner Glykole |
US2867651A (en) * | 1955-10-24 | 1959-01-06 | Standard Oil Co | Purification of alcohols and production of esters in the presence of borohydrides |
GB912797A (en) | 1960-04-22 | 1962-12-12 | Union Carbide Corp | Improvements in and relating to a process for refining alcohols |
US3860520A (en) * | 1967-08-22 | 1975-01-14 | Continental Oil Co | Odor reduction in alcohols |
US3597452A (en) * | 1968-02-19 | 1971-08-03 | Jefferson Chem Co Inc | Treatment of ethylene oxide process cycle water with an amine residue |
US3970711A (en) * | 1971-07-19 | 1976-07-20 | Ppg Industries, Inc. | Method of producing glycols |
US3904656A (en) * | 1973-02-13 | 1975-09-09 | Ppg Industries Inc | Process for preparing monoethylene glycol and ethylene oxide |
-
1976
- 1976-11-17 IT IT29386/76A patent/IT1063805B/it active
-
1977
- 1977-11-10 DK DK500077A patent/DK500077A/da unknown
- 1977-11-11 BR BR7707598A patent/BR7707598A/pt unknown
- 1977-11-11 YU YU02704/77A patent/YU270477A/xx unknown
- 1977-11-11 NL NL7712471A patent/NL7712471A/xx not_active Application Discontinuation
- 1977-11-15 LU LU78518A patent/LU78518A1/xx unknown
- 1977-11-15 IN IN1605/CAL/77A patent/IN146447B/en unknown
- 1977-11-15 DD DD7700202095A patent/DD133791A5/xx unknown
- 1977-11-15 PL PL1977202145A patent/PL109691B1/pl unknown
- 1977-11-15 ZA ZA00776810A patent/ZA776810B/xx unknown
- 1977-11-15 NO NO773911A patent/NO773911L/no unknown
- 1977-11-16 RO RO7792137A patent/RO71280A/fr unknown
- 1977-11-16 AU AU30693/77A patent/AU514202B2/en not_active Expired
- 1977-11-16 HU HU77SA3073A patent/HU175533B/hu unknown
- 1977-11-16 SE SE7712960A patent/SE7712960L/xx not_active Application Discontinuation
- 1977-11-16 FR FR7734511A patent/FR2371405A1/fr active Granted
- 1977-11-16 CS CS777549A patent/CS196408B2/cs unknown
- 1977-11-16 GB GB47766/77A patent/GB1560135A/en not_active Expired
- 1977-11-16 AT AT818177A patent/AT359054B/de not_active IP Right Cessation
- 1977-11-17 DE DE2751383A patent/DE2751383B2/de not_active Withdrawn
- 1977-11-17 JP JP13731677A patent/JPS5363304A/ja active Pending
- 1977-11-17 BE BE182703A patent/BE860929A/fr unknown
- 1977-11-17 TR TR19507A patent/TR19507A/xx unknown
- 1977-11-17 ES ES464378A patent/ES464378A1/es not_active Expired
- 1977-11-17 AR AR270011A patent/AR217090A1/es active
-
1979
- 1979-03-09 US US06/019,109 patent/US4358625A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
FR2371405A1 (fr) | 1978-06-16 |
BE860929A (fr) | 1978-05-17 |
DD133791A5 (de) | 1979-01-24 |
IN146447B (fr) | 1979-06-02 |
PL109691B1 (en) | 1980-06-30 |
PL202145A1 (pl) | 1978-12-04 |
HU175533B (hu) | 1980-08-28 |
AR217090A1 (es) | 1980-02-29 |
IT1063805B (it) | 1985-02-18 |
US4358625A (en) | 1982-11-09 |
JPS5363304A (en) | 1978-06-06 |
DK500077A (da) | 1978-05-18 |
BR7707598A (pt) | 1978-06-20 |
ES464378A1 (es) | 1978-09-01 |
ATA818177A (de) | 1980-03-15 |
RO71280A (fr) | 1982-02-26 |
SE7712960L (sv) | 1978-05-18 |
AU3069377A (en) | 1979-05-24 |
CS196408B2 (en) | 1980-03-31 |
TR19507A (tr) | 1979-03-29 |
FR2371405B1 (fr) | 1980-08-22 |
NL7712471A (nl) | 1978-05-19 |
AU514202B2 (en) | 1981-01-29 |
LU78518A1 (fr) | 1978-03-20 |
YU270477A (en) | 1982-05-31 |
DE2751383B2 (de) | 1980-03-06 |
AT359054B (de) | 1980-10-27 |
GB1560135A (en) | 1980-01-30 |
ZA776810B (en) | 1978-09-27 |
DE2751383A1 (de) | 1978-05-18 |
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