NO311423B1 - Kontinuerlig fremgangsmåte for behandling av kondensater av ammoniakk og urea - Google Patents
Kontinuerlig fremgangsmåte for behandling av kondensater av ammoniakk og urea Download PDFInfo
- Publication number
- NO311423B1 NO311423B1 NO19931779A NO931779A NO311423B1 NO 311423 B1 NO311423 B1 NO 311423B1 NO 19931779 A NO19931779 A NO 19931779A NO 931779 A NO931779 A NO 931779A NO 311423 B1 NO311423 B1 NO 311423B1
- Authority
- NO
- Norway
- Prior art keywords
- ammonia
- stream
- zone
- approx
- condensate
- Prior art date
Links
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title claims description 202
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 title claims description 124
- 229910021529 ammonia Inorganic materials 0.000 title claims description 101
- 239000004202 carbamide Substances 0.000 title claims description 64
- 238000010924 continuous production Methods 0.000 title description 2
- 238000000034 method Methods 0.000 claims description 135
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 100
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 72
- 230000007062 hydrolysis Effects 0.000 claims description 52
- 238000006460 hydrolysis reaction Methods 0.000 claims description 52
- 239000001569 carbon dioxide Substances 0.000 claims description 50
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 50
- 230000015572 biosynthetic process Effects 0.000 claims description 47
- 238000003786 synthesis reaction Methods 0.000 claims description 47
- 239000007788 liquid Substances 0.000 claims description 32
- 238000004519 manufacturing process Methods 0.000 claims description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 229910001868 water Inorganic materials 0.000 claims description 16
- 239000004215 Carbon black (E152) Substances 0.000 claims description 9
- 229930195733 hydrocarbon Natural products 0.000 claims description 9
- 150000002430 hydrocarbons Chemical class 0.000 claims description 9
- 150000001298 alcohols Chemical class 0.000 claims description 6
- 150000001412 amines Chemical class 0.000 claims description 6
- 238000011437 continuous method Methods 0.000 claims description 4
- 238000000629 steam reforming Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- 238000004064 recycling Methods 0.000 claims description 2
- 239000006227 byproduct Substances 0.000 description 10
- 239000000470 constituent Substances 0.000 description 7
- 239000007789 gas Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000003054 catalyst Substances 0.000 description 3
- 239000000356 contaminant Substances 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 239000008246 gaseous mixture Substances 0.000 description 3
- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 3
- 238000012856 packing Methods 0.000 description 3
- 238000002407 reforming Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- 239000002737 fuel gas Substances 0.000 description 2
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000002351 wastewater Substances 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000003795 desorption Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 235000020030 perry Nutrition 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/04—Preparation of ammonia by synthesis in the gas phase
- C01C1/0405—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
- C01C1/0488—Processes integrated with preparations of other compounds, e.g. methanol, urea or with processes for power generation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
- C01B3/025—Preparation or purification of gas mixtures for ammonia synthesis
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/10—Separation of ammonia from ammonia liquors, e.g. gas liquors
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
- C07C273/10—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds combined with the synthesis of ammonia
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/821,209 US5223238A (en) | 1992-01-16 | 1992-01-16 | Method for treating ammonia and urea condensates |
CA002094542A CA2094542C (en) | 1992-01-16 | 1993-04-21 | Method for treating ammonia and urea condensates |
EP93107098A EP0622335B1 (de) | 1992-01-16 | 1993-04-30 | Verfahren zur Behandlung von Abwässern aus der Ammoniak und Harnstoffsynthese |
BR9301811A BR9301811A (pt) | 1992-01-16 | 1993-05-11 | Processo contínuo, em instalação para a produção de amônia e uréia em que um primeiro e um segundo condensados de processamento são produzidos, para tratar simulaneamente os condensados de processamento em um único vaso. |
JP11322593A JP3394559B2 (ja) | 1992-01-16 | 1993-05-14 | アンモニア及び尿素凝縮物の処理方法 |
NO19931779A NO311423B1 (no) | 1992-01-16 | 1993-05-14 | Kontinuerlig fremgangsmåte for behandling av kondensater av ammoniakk og urea |
Applications Claiming Priority (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/821,209 US5223238A (en) | 1992-01-16 | 1992-01-16 | Method for treating ammonia and urea condensates |
CA002094542A CA2094542C (en) | 1992-01-16 | 1993-04-21 | Method for treating ammonia and urea condensates |
EP93107098A EP0622335B1 (de) | 1992-01-16 | 1993-04-30 | Verfahren zur Behandlung von Abwässern aus der Ammoniak und Harnstoffsynthese |
BR9301811A BR9301811A (pt) | 1992-01-16 | 1993-05-11 | Processo contínuo, em instalação para a produção de amônia e uréia em que um primeiro e um segundo condensados de processamento são produzidos, para tratar simulaneamente os condensados de processamento em um único vaso. |
JP11322593A JP3394559B2 (ja) | 1992-01-16 | 1993-05-14 | アンモニア及び尿素凝縮物の処理方法 |
NO19931779A NO311423B1 (no) | 1992-01-16 | 1993-05-14 | Kontinuerlig fremgangsmåte for behandling av kondensater av ammoniakk og urea |
Publications (3)
Publication Number | Publication Date |
---|---|
NO931779D0 NO931779D0 (no) | 1993-05-14 |
NO931779L NO931779L (no) | 1994-11-15 |
NO311423B1 true NO311423B1 (no) | 2001-11-26 |
Family
ID=27543189
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NO19931779A NO311423B1 (no) | 1992-01-16 | 1993-05-14 | Kontinuerlig fremgangsmåte for behandling av kondensater av ammoniakk og urea |
Country Status (6)
Country | Link |
---|---|
US (1) | US5223238A (de) |
EP (1) | EP0622335B1 (de) |
JP (1) | JP3394559B2 (de) |
BR (1) | BR9301811A (de) |
CA (1) | CA2094542C (de) |
NO (1) | NO311423B1 (de) |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0538848A1 (de) * | 1991-10-23 | 1993-04-28 | Urea Casale S.A. | Verfahren und Einrichtung für die Hydrolyse von Restharnstoff im Wasser aus Harnstoff-Syntheseanlagen |
CA2141886E (en) | 1994-05-11 | 1999-10-12 | Federico Zardi | Reactor for two-phase reactions, in particular for urea synthesis at high pressure and temperature |
CA2146070C (en) * | 1995-03-15 | 2002-01-29 | Kees Jonckers | Improved reactor for the synthesis of urea |
US5523483A (en) * | 1995-06-16 | 1996-06-04 | The M. W. Kellogg Company | Integrated urea/ammonia process |
JP4112056B2 (ja) * | 1997-12-18 | 2008-07-02 | 東洋エンジニアリング株式会社 | 改良された尿素の合成方法および装置 |
JP4975205B2 (ja) * | 2000-04-28 | 2012-07-11 | 日揮株式会社 | ガス状混合物からのアンモニア回収方法 |
US6511644B1 (en) | 2000-08-28 | 2003-01-28 | The Chemithon Corporation | Method for removing contaminants in reactors |
US6761868B2 (en) * | 2001-05-16 | 2004-07-13 | The Chemithon Corporation | Process for quantitatively converting urea to ammonia on demand |
US6887449B2 (en) | 2002-11-21 | 2005-05-03 | The Chemithon Corporation | Method of quantitatively producing ammonia from urea |
NL1028497C2 (nl) * | 2005-03-09 | 2006-09-12 | Dsm Ip Assets Bv | Werkwijze voor de bereiding van een ureum-bevattende waterige stroom. |
CN100400430C (zh) * | 2006-05-18 | 2008-07-09 | 刘国胜 | 尿素工艺冷凝液节能净化回收工艺 |
US20080016768A1 (en) | 2006-07-18 | 2008-01-24 | Togna Keith A | Chemically-modified mixed fuels, methods of production and used thereof |
US7687041B2 (en) * | 2008-02-27 | 2010-03-30 | Kellogg Brown & Root Llc | Apparatus and methods for urea production |
TW201032887A (en) * | 2009-01-13 | 2010-09-16 | Saipem Spa | Process for the recovery of ammonia from a gaseous stream |
EA025490B1 (ru) * | 2010-02-12 | 2016-12-30 | Стамикарбон Б.В. | Способ удаления аммиака в секции формования мочевины |
US8262787B2 (en) * | 2010-06-09 | 2012-09-11 | Uop Llc | Configuration of contacting zones in vapor liquid contacting apparatuses |
CN102167412B (zh) * | 2011-04-08 | 2013-01-30 | 吉林化工学院化工分离技术开发中心 | 一种高效复合式尿素废液深度水解解吸塔 |
EP3095760A1 (de) * | 2015-05-21 | 2016-11-23 | Casale SA | Verfahren zur erhöhung der kapazität einer ammoniakanlage |
CN108911950B (zh) * | 2018-06-22 | 2021-03-30 | 河北威远生物化工有限公司 | 一种分离废水中醇和碳酸铵的设备和方法 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS50133995A (de) * | 1974-04-11 | 1975-10-23 | ||
US4341640A (en) * | 1976-09-27 | 1982-07-27 | Standard Oil Company | Urea hydrolysis |
NL8100989A (nl) * | 1981-02-28 | 1982-09-16 | Unie Van Kunstmestfab Bv | Werkwijze voor het verwijderen van ureum, ammoniak en kooldioxide uit verdunde waterige oplossingen. |
NL8102391A (nl) * | 1981-05-15 | 1982-12-01 | Unie Van Kunstmestfab Bv | Werkwijze voor het winnen van waardevolle bestanddelen uit de afvalstromen verkregen bij de ureumbereiding. |
NL8204583A (nl) * | 1982-11-25 | 1984-06-18 | Unie Van Kunstmestfab Bv | Werkwijze voor het verwijderen van ureum, ammoniak en kooldioxide uit verdunde waterige oplossingen. |
US4552979A (en) * | 1984-08-27 | 1985-11-12 | James Chemical Engineering Inc. | Process for treatment of urea plant process condensate |
IT1232670B (it) * | 1989-09-15 | 1992-03-02 | Snam Progetti | Procedimento per la purificazione delle acque reflue prodotte dagli impianti di produzione dell'urea. |
-
1992
- 1992-01-16 US US07/821,209 patent/US5223238A/en not_active Expired - Lifetime
-
1993
- 1993-04-21 CA CA002094542A patent/CA2094542C/en not_active Expired - Lifetime
- 1993-04-30 EP EP93107098A patent/EP0622335B1/de not_active Expired - Lifetime
- 1993-05-11 BR BR9301811A patent/BR9301811A/pt not_active IP Right Cessation
- 1993-05-14 NO NO19931779A patent/NO311423B1/no not_active IP Right Cessation
- 1993-05-14 JP JP11322593A patent/JP3394559B2/ja not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
JPH06329614A (ja) | 1994-11-29 |
CA2094542C (en) | 2003-06-10 |
BR9301811A (pt) | 1994-11-29 |
JP3394559B2 (ja) | 2003-04-07 |
EP0622335B1 (de) | 1997-10-01 |
US5223238A (en) | 1993-06-29 |
NO931779D0 (no) | 1993-05-14 |
CA2094542A1 (en) | 1994-10-22 |
EP0622335A1 (de) | 1994-11-02 |
NO931779L (no) | 1994-11-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
MM1K | Lapsed by not paying the annual fees |