NO121734B - - Google Patents
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- Publication number
- NO121734B NO121734B NO168177A NO16817767A NO121734B NO 121734 B NO121734 B NO 121734B NO 168177 A NO168177 A NO 168177A NO 16817767 A NO16817767 A NO 16817767A NO 121734 B NO121734 B NO 121734B
- Authority
- NO
- Norway
- Prior art keywords
- ammonium nitrate
- hardening
- solution
- temperature
- parts
- Prior art date
Links
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 claims description 122
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 44
- 150000003839 salts Chemical class 0.000 claims description 28
- 239000002245 particle Substances 0.000 claims description 21
- 238000003860 storage Methods 0.000 claims description 11
- 239000007859 condensation product Substances 0.000 claims description 9
- WODGMMJHSAKKNF-UHFFFAOYSA-N 2-methylnaphthalene-1-sulfonic acid Chemical compound C1=CC=CC2=C(S(O)(=O)=O)C(C)=CC=C21 WODGMMJHSAKKNF-UHFFFAOYSA-N 0.000 claims description 8
- 239000011248 coating agent Substances 0.000 claims description 7
- 238000000576 coating method Methods 0.000 claims description 7
- 229920006395 saturated elastomer Polymers 0.000 claims description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 35
- 239000000243 solution Substances 0.000 description 34
- 239000013078 crystal Substances 0.000 description 31
- QPUYECUOLPXSFR-UHFFFAOYSA-N 1-methylnaphthalene Chemical class C1=CC=C2C(C)=CC=CC2=C1 QPUYECUOLPXSFR-UHFFFAOYSA-N 0.000 description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 20
- 239000000203 mixture Substances 0.000 description 19
- 239000000047 product Substances 0.000 description 19
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 18
- 238000003756 stirring Methods 0.000 description 18
- QIMMUPPBPVKWKM-UHFFFAOYSA-N 2-methylnaphthalene Chemical compound C1=CC=CC2=CC(C)=CC=C21 QIMMUPPBPVKWKM-UHFFFAOYSA-N 0.000 description 16
- 238000002425 crystallisation Methods 0.000 description 14
- 239000003607 modifier Substances 0.000 description 14
- 239000007864 aqueous solution Substances 0.000 description 13
- 239000003795 chemical substances by application Substances 0.000 description 13
- 230000008025 crystallization Effects 0.000 description 13
- 150000001875 compounds Chemical class 0.000 description 9
- AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 description 8
- 238000001816 cooling Methods 0.000 description 8
- 239000012452 mother liquor Substances 0.000 description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 239000011541 reaction mixture Substances 0.000 description 7
- 239000005909 Kieselgur Substances 0.000 description 6
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 6
- 239000000975 dye Substances 0.000 description 6
- 238000001704 evaporation Methods 0.000 description 6
- 230000008020 evaporation Effects 0.000 description 6
- 229930040373 Paraformaldehyde Natural products 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000009833 condensation Methods 0.000 description 5
- 230000005494 condensation Effects 0.000 description 5
- 230000005484 gravity Effects 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 239000000706 filtrate Substances 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 239000002244 precipitate Substances 0.000 description 4
- 239000007921 spray Substances 0.000 description 4
- 238000006277 sulfonation reaction Methods 0.000 description 4
- BXJIZCYGEBTLGO-UHFFFAOYSA-N 7-methylnaphthalene-1-sulfonic acid Chemical compound C1=CC=C(S(O)(=O)=O)C2=CC(C)=CC=C21 BXJIZCYGEBTLGO-UHFFFAOYSA-N 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 238000006482 condensation reaction Methods 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 229920002866 paraformaldehyde Polymers 0.000 description 3
- 239000012047 saturated solution Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 241000322338 Loeseliastrum Species 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- RZUBARUFLYGOGC-MTHOTQAESA-L acid fuchsin Chemical compound [Na+].[Na+].[O-]S(=O)(=O)C1=C(N)C(C)=CC(C(=C\2C=C(C(=[NH2+])C=C/2)S([O-])(=O)=O)\C=2C=C(C(N)=CC=2)S([O-])(=O)=O)=C1 RZUBARUFLYGOGC-MTHOTQAESA-L 0.000 description 2
- DVARTQFDIMZBAA-UHFFFAOYSA-O ammonium nitrate Chemical class [NH4+].[O-][N+]([O-])=O DVARTQFDIMZBAA-UHFFFAOYSA-O 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 159000000007 calcium salts Chemical class 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000002360 explosive Substances 0.000 description 2
- 238000010907 mechanical stirring Methods 0.000 description 2
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 2
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical class C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 description 2
- 239000000123 paper Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- ZTDJDNLZVGJTBW-UHFFFAOYSA-N 4-methylnaphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(C)=CC=C(S(O)(=O)=O)C2=C1 ZTDJDNLZVGJTBW-UHFFFAOYSA-N 0.000 description 1
- KXADICOPIZKQKI-UHFFFAOYSA-N 4-methylnaphthalene-2-sulfonic acid Chemical compound C1=CC=C2C(C)=CC(S(O)(=O)=O)=CC2=C1 KXADICOPIZKQKI-UHFFFAOYSA-N 0.000 description 1
- BATOZQRGECFVTF-UHFFFAOYSA-N 5-methylnaphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(C)=CC=CC2=C1S(O)(=O)=O BATOZQRGECFVTF-UHFFFAOYSA-N 0.000 description 1
- FYYMFSCGGOJKPN-UHFFFAOYSA-N 5-methylnaphthalene-2-sulfonic acid Chemical compound OS(=O)(=O)C1=CC=C2C(C)=CC=CC2=C1 FYYMFSCGGOJKPN-UHFFFAOYSA-N 0.000 description 1
- UGDHIURSEUVFCE-UHFFFAOYSA-N 6-methylnaphthalene-2-sulfonic acid Chemical compound C1=C(S(O)(=O)=O)C=CC2=CC(C)=CC=C21 UGDHIURSEUVFCE-UHFFFAOYSA-N 0.000 description 1
- LUGQQBPUAULKPK-UHFFFAOYSA-N 7-methylnaphthalene-2-sulfonic acid Chemical compound C1=CC(S(O)(=O)=O)=CC2=CC(C)=CC=C21 LUGQQBPUAULKPK-UHFFFAOYSA-N 0.000 description 1
- HMFSQLOMPHLGEJ-UHFFFAOYSA-N 8-methylnaphthalene-2-sulfonic acid Chemical compound C1=C(S(O)(=O)=O)C=C2C(C)=CC=CC2=C1 HMFSQLOMPHLGEJ-UHFFFAOYSA-N 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 239000003377 acid catalyst Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- 159000000009 barium salts Chemical class 0.000 description 1
- -1 carbinol anhydride Chemical class 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000012045 crude solution Substances 0.000 description 1
- 239000011549 crystallization solution Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Natural products OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- IPSIPYMEZZPCPY-UHFFFAOYSA-N new fuchsin Chemical class [Cl-].C1=CC(=[NH2+])C(C)=CC1=C(C=1C=C(C)C(N)=CC=1)C1=CC=C(N)C(C)=C1 IPSIPYMEZZPCPY-UHFFFAOYSA-N 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000010583 slow cooling Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000012258 stirred mixture Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
- H01M50/10—Primary casings; Jackets or wrappings
- H01M50/172—Arrangements of electric connectors penetrating the casing
- H01M50/174—Arrangements of electric connectors penetrating the casing adapted for the shape of the cells
- H01M50/182—Arrangements of electric connectors penetrating the casing adapted for the shape of the cells for cells with a collector centrally disposed in the active mass, e.g. Leclanché cells
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M6/00—Primary cells; Manufacture thereof
- H01M6/04—Cells with aqueous electrolyte
- H01M6/06—Dry cells, i.e. cells wherein the electrolyte is rendered non-fluid
- H01M6/08—Dry cells, i.e. cells wherein the electrolyte is rendered non-fluid with cup-shaped electrodes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Sealing Battery Cases Or Jackets (AREA)
- Hybrid Cells (AREA)
- Primary Cells (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- General Preparation And Processing Of Foods (AREA)
- Secondary Cells (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR984121A FR1451975A (fr) | 1964-08-04 | 1964-08-04 | élément électrochimique étanche perfectionné |
| FR62098A FR91355E (fr) | 1964-08-04 | 1966-05-18 | élément électrochimique étanche perfectionné |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO121734B true NO121734B (xx) | 1971-04-05 |
Family
ID=26170745
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO159137A NO119092B (xx) | 1964-08-04 | 1965-07-29 | |
| NO168177A NO121734B (xx) | 1964-08-04 | 1967-05-16 |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO159137A NO119092B (xx) | 1964-08-04 | 1965-07-29 |
Country Status (13)
| Country | Link |
|---|---|
| US (2) | US3342644A (xx) |
| BE (2) | BE667463A (xx) |
| CH (1) | CH475655A (xx) |
| CY (1) | CY407A (xx) |
| DE (2) | DE1496242B1 (xx) |
| DK (2) | DK115559B (xx) |
| FR (1) | FR91355E (xx) |
| GB (2) | GB1069015A (xx) |
| IL (1) | IL27852A (xx) |
| LU (2) | LU49207A1 (xx) |
| NL (2) | NL144440C (xx) |
| NO (2) | NO119092B (xx) |
| OA (1) | OA120E (xx) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL136425C (xx) * | 1966-07-11 | |||
| JPS4921504B1 (xx) * | 1970-09-29 | 1974-06-01 | ||
| US3850776A (en) * | 1971-12-07 | 1974-11-26 | E Karobath | Apparatus for joining a tubular thermoplastic container jacket, by means of ultrasonics to a thermoplastic end cap to form a liquid-tight seal |
| US4079173A (en) * | 1974-10-17 | 1978-03-14 | Pun Ching W | Leak resistant dry cells |
| FR2357076A1 (fr) * | 1976-06-30 | 1978-01-27 | Cipel | Generateur electrochimique cylindrique |
| US4606983A (en) * | 1985-02-25 | 1986-08-19 | Duracell Inc. | Anchored terminal conductor |
| GB8815181D0 (en) * | 1988-06-25 | 1988-08-03 | Tucke Fasteners Ltd | Electrical storage cell |
| US4879191A (en) * | 1989-03-23 | 1989-11-07 | Globe-Union Inc. | Crimp terminal for a battery |
| US5273845A (en) * | 1992-08-18 | 1993-12-28 | Acme Electric Corporation | Terminal structure and seal |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB531237A (en) * | 1940-02-06 | 1940-12-31 | Ray O Vac Co | Improvements relating to electrical primary cells |
| US2396693A (en) * | 1942-04-18 | 1946-03-19 | Nat Carbon Co Inc | Dry cell and process for manufacturing the same |
| US2552091A (en) * | 1945-12-22 | 1951-05-08 | Union Carbide & Carbon Corp | Dry cell |
| US2642471A (en) * | 1951-06-07 | 1953-06-16 | Olin Ind Inc | Dry cell |
| NL196993A (xx) * | 1954-05-06 | |||
| FR77948E (fr) * | 1959-07-17 | 1962-05-11 | Accumulateurs Fixes | élément électro-chimique étanche et son procédé de fabrication |
| NL122193C (xx) * | 1959-07-17 | |||
| US3168420A (en) * | 1960-06-24 | 1965-02-02 | Accumulateurs Fixes | Leak-resistant electrochemical cell and process for manufacturing the same |
-
1965
- 1965-01-28 US US428714A patent/US3342644A/en not_active Expired - Lifetime
- 1965-07-27 BE BE667463A patent/BE667463A/xx unknown
- 1965-07-29 NO NO159137A patent/NO119092B/no unknown
- 1965-07-29 LU LU49207D patent/LU49207A1/xx unknown
- 1965-08-02 DE DE19651496242 patent/DE1496242B1/de active Pending
- 1965-08-03 DK DK398665AA patent/DK115559B/da unknown
- 1965-08-04 NL NL656510106A patent/NL144440C/xx active
- 1965-08-04 GB GB33451/65A patent/GB1069015A/en not_active Expired
-
1966
- 1966-05-18 FR FR62098A patent/FR91355E/fr not_active Expired
-
1967
- 1967-04-19 DE DE19671671923 patent/DE1671923C3/de not_active Expired
- 1967-04-23 IL IL27852A patent/IL27852A/en unknown
- 1967-05-06 OA OA52930A patent/OA120E/xx unknown
- 1967-05-10 BE BE698279A patent/BE698279A/xx not_active Expired
- 1967-05-10 US US637552A patent/US3433681A/en not_active Expired - Lifetime
- 1967-05-11 LU LU53653D patent/LU53653A1/xx unknown
- 1967-05-12 CH CH672067A patent/CH475655A/fr not_active IP Right Cessation
- 1967-05-16 NO NO168177A patent/NO121734B/no unknown
- 1967-05-17 DK DK257467AA patent/DK122489B/da unknown
- 1967-05-17 NL NL6706863A patent/NL6706863A/xx unknown
- 1967-05-18 GB GB23100/67A patent/GB1175725A/en not_active Expired
- 1967-10-06 CY CY40767A patent/CY407A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| LU53653A1 (xx) | 1969-02-10 |
| DE1671923C3 (de) | 1976-05-20 |
| GB1175725A (en) | 1969-12-23 |
| IL27852A (en) | 1970-09-17 |
| GB1069015A (en) | 1967-05-17 |
| BE698279A (xx) | 1967-11-10 |
| LU49207A1 (xx) | 1967-01-30 |
| NL6706863A (xx) | 1967-11-20 |
| NL144440C (nl) | 1974-12-16 |
| FR91355E (fr) | 1968-05-31 |
| DK115559B (da) | 1969-10-20 |
| DK122489B (da) | 1972-03-06 |
| US3433681A (en) | 1969-03-18 |
| OA120E (xx) | 1970-12-15 |
| DE1496242B1 (de) | 1969-10-02 |
| NO119092B (xx) | 1970-03-23 |
| DE1671923B2 (de) | 1975-10-09 |
| DE1671923A1 (de) | 1971-10-21 |
| US3342644A (en) | 1967-09-19 |
| NL6510106A (xx) | 1966-02-07 |
| CH475655A (fr) | 1969-07-15 |
| CY407A (en) | 1967-10-06 |
| BE667463A (xx) | 1966-01-27 |
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