MX375960B - Proceso para la preparacion de pirazoles. - Google Patents
Proceso para la preparacion de pirazoles.Info
- Publication number
- MX375960B MX375960B MX2017001462A MX2017001462A MX375960B MX 375960 B MX375960 B MX 375960B MX 2017001462 A MX2017001462 A MX 2017001462A MX 2017001462 A MX2017001462 A MX 2017001462A MX 375960 B MX375960 B MX 375960B
- Authority
- MX
- Mexico
- Prior art keywords
- formula
- pyrazole
- preparation
- reagent
- compounds
- Prior art date
Links
- 150000003217 pyrazoles Chemical class 0.000 title abstract 2
- 239000003153 chemical reaction reagent Substances 0.000 abstract 2
- WTKZEGDFNFYCGP-UHFFFAOYSA-N Pyrazole Chemical compound C=1C=NNC=1 WTKZEGDFNFYCGP-UHFFFAOYSA-N 0.000 abstract 1
- 150000001728 carbonyl compounds Chemical class 0.000 abstract 1
- 239000003638 chemical reducing agent Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000012847 fine chemical Substances 0.000 abstract 1
- 125000005597 hydrazone group Chemical group 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000012434 nucleophilic reagent Substances 0.000 abstract 1
- 125000002524 organometallic group Chemical group 0.000 abstract 1
- -1 pyrazole compound Chemical class 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/33—Heterocyclic compounds
- A61K31/395—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
- A61K31/41—Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having five-membered rings with two or more ring hetero atoms, at least one of which being nitrogen, e.g. tetrazole
- A61K31/415—1,2-Diazoles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
- C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
- C07D401/12—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings linked by a chain containing hetero atoms as chain links
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D403/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00
- C07D403/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings
- C07D403/12—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings linked by a chain containing hetero atoms as chain links
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D405/00—Heterocyclic compounds containing both one or more hetero rings having oxygen atoms as the only ring hetero atoms, and one or more rings having nitrogen as the only ring hetero atom
- C07D405/02—Heterocyclic compounds containing both one or more hetero rings having oxygen atoms as the only ring hetero atoms, and one or more rings having nitrogen as the only ring hetero atom containing two hetero rings
- C07D405/06—Heterocyclic compounds containing both one or more hetero rings having oxygen atoms as the only ring hetero atoms, and one or more rings having nitrogen as the only ring hetero atom containing two hetero rings linked by a carbon chain containing only aliphatic carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Engineering & Computer Science (AREA)
- Animal Behavior & Ethology (AREA)
- Pharmacology & Pharmacy (AREA)
- Public Health (AREA)
- Medicinal Chemistry (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Epidemiology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Plural Heterocyclic Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Abstract
La presente invención se refiere a un proceso para la preparación de un compuesto de pirazol de la fórmula V, que comprende la ciclación de un compuesto de carbonilo a,ß-insaturado sustituido por hidrazona de la fórmula IV por medio de la reacción con un reactivo adecuado, por ej., un agente reductor, un reactivo organometálico o un reactivo nucleófilo. Los compuestos de la fórmula y son herramientas versátiles de reacción para la preparación de productos químicos finos derivados de pirazol. La presente invención también se refiere a compuestos de pirazol de las fórmulas Va, Vb, Vc, y VI.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14179249 | 2014-07-31 | ||
| PCT/EP2015/067507 WO2016016369A1 (en) | 2014-07-31 | 2015-07-30 | Process for preparing pyrazoles |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2017001462A MX2017001462A (es) | 2017-05-23 |
| MX375960B true MX375960B (es) | 2025-03-06 |
Family
ID=51257363
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2017001462A MX375960B (es) | 2014-07-31 | 2015-07-30 | Proceso para la preparacion de pirazoles. |
Country Status (19)
| Country | Link |
|---|---|
| US (2) | US10414733B2 (es) |
| EP (1) | EP3174858B1 (es) |
| JP (1) | JP6625610B2 (es) |
| KR (1) | KR102531217B1 (es) |
| CN (1) | CN106573893B (es) |
| AU (1) | AU2015295287B2 (es) |
| BR (1) | BR112016030863B1 (es) |
| CA (1) | CA2954212C (es) |
| DK (1) | DK3174858T3 (es) |
| ES (1) | ES2741831T3 (es) |
| IL (1) | IL249730B (es) |
| MX (1) | MX375960B (es) |
| PL (1) | PL3174858T3 (es) |
| PT (1) | PT3174858T (es) |
| RU (1) | RU2712192C2 (es) |
| TR (1) | TR201909606T4 (es) |
| UA (1) | UA121395C2 (es) |
| WO (1) | WO2016016369A1 (es) |
| ZA (1) | ZA201701415B (es) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105829274A (zh) | 2013-12-18 | 2016-08-03 | 巴斯夫农业公司 | 制备取代的苯氧基苯基酮的方法 |
| MX375960B (es) | 2014-07-31 | 2025-03-06 | Basf Se | Proceso para la preparacion de pirazoles. |
| WO2016062814A1 (en) | 2014-10-24 | 2016-04-28 | Basf Se | Substituted pyridine compounds having herbicidal activity |
| EP3294720B1 (en) | 2015-05-08 | 2020-12-02 | BASF Agro B.V. | A process for the preparation of terpinolene epoxide |
| CN107848922A (zh) | 2015-05-08 | 2018-03-27 | 巴斯夫农业公司 | 柠檬烯‑4‑醇的制备方法 |
| AU2016260784B2 (en) | 2015-05-11 | 2020-03-12 | Basf Se | Process for preparing 4-amino-pyridazines |
| BR112018002475A2 (pt) | 2015-08-07 | 2018-09-18 | Basf Se | método para o controle das pragas de um vegetal de milho e utilização de um ou mais componentes da árvore de ginkgo |
| AU2017216082B2 (en) * | 2016-02-02 | 2020-12-03 | Basf Se | Catalytic hydrogenation process for preparing pyrazoles |
| BR112018076043B1 (pt) | 2016-06-15 | 2023-09-26 | Basf Agro B.V | Processo de epoxidação de alqueno tetrassubstituído e uso de agente oxidante |
| MX2018015765A (es) | 2016-06-15 | 2019-08-29 | Basf Agro Bv | Proceso para la epoxidacion de un alqueno tretrasustituido. |
| BR112018077104A2 (pt) | 2016-07-07 | 2019-04-02 | Basf Se | compostos, processo para a preparação de compostos de fórmula i, processo para a preparação de compostos de fórmula iv e uso de compostos da fórmula i |
| WO2018139560A1 (ja) | 2017-01-26 | 2018-08-02 | 三井化学アグロ株式会社 | ピリドン化合物およびそれを有効成分とする農園芸用殺菌剤 |
| CA3059702A1 (en) | 2017-04-10 | 2018-10-18 | Mitsui Chemicals Agro, Inc. | Pyridone compounds and agricultural and horticultural fungicides containing the same as active ingredients |
| WO2018190350A1 (ja) | 2017-04-10 | 2018-10-18 | 三井化学アグロ株式会社 | ピリドン化合物およびそれを有効成分とする農園芸用殺菌剤 |
| MY190386A (en) | 2017-04-11 | 2022-04-20 | Mitsui Chemicals Agro Inc | Pyridone compounds and agricultural and horticultural fungicides containing the same as active ingredients |
| JP7157738B2 (ja) | 2017-06-08 | 2022-10-20 | 三井化学アグロ株式会社 | ピリドン化合物およびそれを有効成分とする農園芸用殺菌剤 |
| JP2021506879A (ja) * | 2017-12-22 | 2021-02-22 | ソルヴェイ（ソシエテ アノニム） | ピラゾールカルボン酸誘導体及びその前駆体の製造のための方法 |
| US12114658B2 (en) | 2018-07-25 | 2024-10-15 | Mitsui Chemicals Crop & Life Solutions, Inc. | Compounds having a nitrogen-containing unsaturated six-membered ring and agricultural and horticultural fungicides containing the same as active ingredients |
| EP3894403A1 (en) | 2018-12-13 | 2021-10-20 | Intervet International B.V. | Process for preparing 1-[(3r,4s)-4-cyanotetrahydropyran-3-yl]-3-[(2-fluoro-6-methoxy-4-pyridyl)amino]p yrazole-4-carboxamide |
| EP4280398A1 (en) | 2022-05-17 | 2023-11-22 | NKT Photonics A/S | Tunable laser device with frequency stabilization and low frequency-noise |
| CN116396221B (zh) * | 2023-04-06 | 2024-09-10 | 无锡科华生物科技有限公司 | 一种1-(3-羟基-3-甲基-2-丁基)-5-甲基-1h-吡唑-4-羧酸的制备方法 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4728355A (en) | 1985-10-10 | 1988-03-01 | Fmc Corporation | Pyridazinylurea plant regulators |
| TW406075B (en) | 1994-12-13 | 2000-09-21 | Upjohn Co | Alkyl substituted piperidinyl and piperazinyl anti-AIDS compounds |
| TR199800012T1 (xx) | 1995-07-06 | 1998-04-21 | Novartis Ag | Piroloprimidinler ve preparasyon i�in tatbikler. |
| US6258822B1 (en) | 1997-08-06 | 2001-07-10 | Abbott Laboratories | Urokinase inhibitors |
| US6800758B1 (en) | 1998-06-05 | 2004-10-05 | Egis Gyogyszergyar Rt. | Process for the preparation of a 3(2H)-pyridazinone-4- substituted amino 5-chloro derivative |
| JP4829449B2 (ja) | 1999-07-28 | 2011-12-07 | アベンティス・ファーマスーティカルズ・インコーポレイテツド | 置換オキソアザヘテロシクリル化合物 |
| CA2449249A1 (en) | 2001-06-12 | 2002-12-19 | Merck & Co., Inc. | Nr2b receptor antagonists for the treatment or prevention of migraines |
| JP2007326784A (ja) | 2006-06-06 | 2007-12-20 | Sagami Chem Res Center | １−置換−５−フルオロアルキルピラゾール−４−カルボン酸エステルの製造方法 |
| US20110189167A1 (en) | 2007-04-20 | 2011-08-04 | Flynn Daniel L | Methods and Compositions for the Treatment of Myeloproliferative Diseases and other Proliferative Diseases |
| UA103006C2 (ru) | 2007-08-27 | 2013-09-10 | Басф Се | Пиразольные соединения для борьбы с бесхребетными вредителями |
| WO2009068652A1 (en) * | 2007-11-30 | 2009-06-04 | Smithkline Beecham Corporation | 2, 6-disubstituted pyridines and 2, 4-disubstituted pyrimidines as soluble guanylate cyclase activators |
| WO2009135808A2 (de) * | 2008-05-05 | 2009-11-12 | Basf Se | Verfahren zur herstellung von 1,3,4-substituierten pyrazolverbindungen |
| EA018198B1 (ru) | 2008-06-12 | 2013-06-28 | Янссен Фармацевтика Нв | Диаминопиридиновые, пиримидиновые и пиридазиновые модуляторы гистаминового рецептора h |
| ES2710701T3 (es) | 2008-09-24 | 2019-04-26 | Basf Se | Compuestos de pirazol para el control de plagas de invertebrados |
| UA103633C2 (ru) | 2008-09-24 | 2013-11-11 | Басф Се | Пиразольные соединения для борьбы с бесхребетными вредителями |
| US20100113465A1 (en) | 2008-10-30 | 2010-05-06 | Pfizer Inc. | 7-azaspiro[3.5]nonane-7-carboxamide compounds |
| EP2236505A1 (de) | 2009-04-03 | 2010-10-06 | Bayer CropScience AG | Acylierte Aminopyridine und - pyridazine als Insektizide |
| AR076984A1 (es) * | 2009-06-08 | 2011-07-20 | Merck Serono Sa | Derivados de pirazol oxadiazol |
| JP5752691B2 (ja) | 2009-09-29 | 2015-07-22 | グラクソ グループ リミテッドＧｌａｘｏ Ｇｒｏｕｐ Ｌｉｍｉｔｅｄ | 新規化合物 |
| EP2555773A1 (de) | 2010-04-08 | 2013-02-13 | Boehringer Ingelheim International GmbH | Arzneimittelkombinationen enthaltend pde4-inhibitoren und ep4-rezeptor-antagonisten |
| EP2468736A1 (en) | 2010-12-23 | 2012-06-27 | LEK Pharmaceuticals d.d. | Synthesis of intermediates for preparing anacetrapib and derivates thereof |
| WO2012098387A1 (en) | 2011-01-18 | 2012-07-26 | Centro Nacional De Investigaciones Oncológicas (Cnio) | 6, 7-ring-fused triazolo [4, 3 - b] pyridazine derivatives as pim inhibitors |
| KR102123083B1 (ko) | 2011-04-12 | 2020-06-16 | 써메디컬, 인코포레이티드 | 유체 증강 절제 치료법에서 원격 온도 관찰 방법 및 장치 |
| AU2012244846B2 (en) | 2011-04-21 | 2016-07-07 | Basf Se | Novel pesticidal pyrazole compounds |
| WO2013004984A1 (en) | 2011-07-07 | 2013-01-10 | Centro Nacional De Investigaciones Oncologicas (Cnio) | Tricyclic compounds for use as kinase inhibitors |
| EP2828262A4 (en) | 2012-03-19 | 2015-09-23 | Forum Pharmaceuticals Inc | IMIDAZOTRIAZINONVERBINDUNGEN |
| JO3407B1 (ar) | 2012-05-31 | 2019-10-20 | Eisai R&D Man Co Ltd | مركبات رباعي هيدرو بيرازولو بيريميدين |
| EP2671873A1 (en) | 2012-06-06 | 2013-12-11 | Solvay Sa | Method for the cyclization of hydrazinoacrylic acid derivatives |
| ES2800288T3 (es) * | 2012-06-20 | 2020-12-29 | Basf Se | Mezclas plaguicidas que comprenden un compuesto de pirazol |
| US9604961B2 (en) * | 2012-12-06 | 2017-03-28 | Celgene Quanticel Research, Inc. | Histone demethylase inhibitors |
| UA112028C2 (uk) | 2012-12-14 | 2016-07-11 | Пфайзер Лімітед | Похідні імідазопіридазину як модулятори гамка-рецептора |
| WO2015114106A1 (en) | 2014-01-31 | 2015-08-06 | Basf Se | Pyrazoles for controlling invertebrate pests |
| WO2015162133A1 (en) | 2014-04-22 | 2015-10-29 | Basf Se | C3-c4-cycloalkenyl-comprising pyrazoles for controlling invertebrate pests |
| WO2015169734A1 (en) | 2014-05-05 | 2015-11-12 | Basf Se | Pyrazoles for controlling invertebrate pests |
| WO2015189080A1 (en) | 2014-06-12 | 2015-12-17 | Basf Se | Pesticidally active mixtures |
| MX375960B (es) | 2014-07-31 | 2025-03-06 | Basf Se | Proceso para la preparacion de pirazoles. |
| EP3255990B1 (en) | 2015-02-11 | 2020-06-24 | Basf Se | Pesticidal mixture comprising a pyrazole compound, an insecticide and a fungicide |
| WO2016128240A1 (en) | 2015-02-11 | 2016-08-18 | Basf Se | Pesticidal mixture comprising a pyrazole compound and two fungicides |
| WO2016128239A1 (en) | 2015-02-11 | 2016-08-18 | Basf Se | Pesticidal mixture comprising a pyrazole compound and a biopesticide |
| AU2016260784B2 (en) | 2015-05-11 | 2020-03-12 | Basf Se | Process for preparing 4-amino-pyridazines |
| AU2017216082B2 (en) | 2016-02-02 | 2020-12-03 | Basf Se | Catalytic hydrogenation process for preparing pyrazoles |
-
2015
- 2015-07-30 MX MX2017001462A patent/MX375960B/es active IP Right Grant
- 2015-07-30 WO PCT/EP2015/067507 patent/WO2016016369A1/en not_active Ceased
- 2015-07-30 RU RU2017106265A patent/RU2712192C2/ru active
- 2015-07-30 DK DK15750664.3T patent/DK3174858T3/da active
- 2015-07-30 JP JP2017505088A patent/JP6625610B2/ja active Active
- 2015-07-30 EP EP15750664.3A patent/EP3174858B1/en active Active
- 2015-07-30 UA UAA201701767A patent/UA121395C2/uk unknown
- 2015-07-30 ES ES15750664T patent/ES2741831T3/es active Active
- 2015-07-30 PL PL15750664T patent/PL3174858T3/pl unknown
- 2015-07-30 US US15/329,104 patent/US10414733B2/en active Active
- 2015-07-30 TR TR2019/09606T patent/TR201909606T4/tr unknown
- 2015-07-30 KR KR1020177005786A patent/KR102531217B1/ko active Active
- 2015-07-30 PT PT15750664T patent/PT3174858T/pt unknown
- 2015-07-30 CA CA2954212A patent/CA2954212C/en active Active
- 2015-07-30 CN CN201580041109.2A patent/CN106573893B/zh active Active
- 2015-07-30 AU AU2015295287A patent/AU2015295287B2/en active Active
- 2015-07-30 BR BR112016030863-8A patent/BR112016030863B1/pt active IP Right Grant
-
2016
- 2016-12-22 IL IL249730A patent/IL249730B/en active IP Right Grant
-
2017
- 2017-02-24 ZA ZA2017/01415A patent/ZA201701415B/en unknown
-
2019
- 2019-03-05 US US16/292,773 patent/US10513498B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| PT3174858T (pt) | 2019-07-23 |
| AU2015295287A1 (en) | 2017-02-16 |
| EP3174858A1 (en) | 2017-06-07 |
| RU2017106265A3 (es) | 2019-02-25 |
| TR201909606T4 (tr) | 2019-07-22 |
| BR112016030863B1 (pt) | 2021-05-04 |
| ZA201701415B (en) | 2019-06-26 |
| DK3174858T3 (da) | 2019-07-15 |
| RU2017106265A (ru) | 2018-08-30 |
| US10414733B2 (en) | 2019-09-17 |
| CN106573893B (zh) | 2020-06-09 |
| RU2712192C2 (ru) | 2020-01-24 |
| MX2017001462A (es) | 2017-05-23 |
| IL249730B (en) | 2019-12-31 |
| WO2016016369A1 (en) | 2016-02-04 |
| CN106573893A (zh) | 2017-04-19 |
| US20180086715A9 (en) | 2018-03-29 |
| UA121395C2 (uk) | 2020-05-25 |
| EP3174858B1 (en) | 2019-04-17 |
| PL3174858T3 (pl) | 2019-10-31 |
| JP6625610B2 (ja) | 2019-12-25 |
| IL249730A0 (en) | 2017-02-28 |
| JP2017522342A (ja) | 2017-08-10 |
| US20170210712A1 (en) | 2017-07-27 |
| KR102531217B1 (ko) | 2023-05-10 |
| ES2741831T3 (es) | 2020-02-12 |
| US10513498B2 (en) | 2019-12-24 |
| CA2954212C (en) | 2023-09-19 |
| AU2015295287B2 (en) | 2019-07-04 |
| KR20170036094A (ko) | 2017-03-31 |
| CA2954212A1 (en) | 2016-02-04 |
| US20190194141A1 (en) | 2019-06-27 |
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