KR950032032A - 펜타플루오로에탄의 정제 방법 - Google Patents
펜타플루오로에탄의 정제 방법 Download PDFInfo
- Publication number
- KR950032032A KR950032032A KR1019950003743A KR19950003743A KR950032032A KR 950032032 A KR950032032 A KR 950032032A KR 1019950003743 A KR1019950003743 A KR 1019950003743A KR 19950003743 A KR19950003743 A KR 19950003743A KR 950032032 A KR950032032 A KR 950032032A
- Authority
- KR
- South Korea
- Prior art keywords
- extractant
- pentafluoroethane
- purification
- cycloalkane
- purifying pentafluoroethane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- GTLACDSXYULKMZ-UHFFFAOYSA-N pentafluoroethane Chemical compound FC(F)C(F)(F)F GTLACDSXYULKMZ-UHFFFAOYSA-N 0.000 title claims abstract 3
- 238000000034 method Methods 0.000 title claims 4
- 238000000746 purification Methods 0.000 claims abstract description 6
- 238000000895 extractive distillation Methods 0.000 claims abstract description 4
- 150000001335 aliphatic alkanes Chemical class 0.000 claims abstract 3
- 150000001924 cycloalkanes Chemical class 0.000 claims abstract 3
- RFCAUADVODFSLZ-UHFFFAOYSA-N 1-Chloro-1,1,2,2,2-pentafluoroethane Chemical compound FC(F)(F)C(F)(F)Cl RFCAUADVODFSLZ-UHFFFAOYSA-N 0.000 claims abstract 2
- 239000004340 Chloropentafluoroethane Substances 0.000 claims abstract 2
- 235000019406 chloropentafluoroethane Nutrition 0.000 claims abstract 2
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical group CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims description 4
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims description 2
- AFABGHUZZDYHJO-UHFFFAOYSA-N dimethyl butane Natural products CCCC(C)C AFABGHUZZDYHJO-UHFFFAOYSA-N 0.000 claims 3
- RGSFGYAAUTVSQA-UHFFFAOYSA-N Cyclopentane Chemical compound C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 claims 2
- QWTDNUCVQCZILF-UHFFFAOYSA-N isopentane Chemical compound CCC(C)C QWTDNUCVQCZILF-UHFFFAOYSA-N 0.000 claims 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims 2
- 238000009835 boiling Methods 0.000 claims 1
- DMEGYFMYUHOHGS-UHFFFAOYSA-N heptamethylene Natural products C1CCCCCC1 DMEGYFMYUHOHGS-UHFFFAOYSA-N 0.000 claims 1
- 239000000203 mixture Substances 0.000 abstract description 3
- 238000001577 simple distillation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
- C07C17/386—Separation; Purification; Stabilisation; Use of additives by distillation with auxiliary compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
본 발명은 클로로펜타플루오로에탄(F115)을 함유하는 펜타플루오로에탄(F125)의 정제에 관한 것이다.
F125-F115의 혼합물의 정제는 추출제로서 C5~C8알칸 또는 시클로알칸을 사용한 추출 증류로써 실행한다.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 n-펜탄 및 추출 증류 컬럼을 사용하여 F125-F115의 혼합물로부터 F125를 분리-정제하는 것을 나타낸다. 제2도는 시클로헥산 및 단순 증류 컬럼 및 추출 증류칼럼의 조합을 사용하여 F125-F115의 혼합물로부터 F125를 분리-정제하는 것을 나타낸다.
Claims (3)
- 클로로펜타플루오로에탄(F115)을 함유하는 펜타플루오로에탄(F125)의 추출 증류에 의한 정제 방법에 있어서, 사용하는 추출제가 C5~C8직쇄 또는 측쇄의 알칸 또는 시클로알칸임을 특징으로 하는 정제 방법.
- 제1항에 있어서, 추출제가 25~85℃의 비점을 갖는 알칸 또는 시클로알칸인 정제 방법.
- 제1항에 있어서, 추출제를 n-펜탄, 이소펜탄, 시클로펜탄, n-헥산, 이소헥산 및 시클로헥산으로부터 선택하는 정제 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR9402114A FR2716449B1 (fr) | 1994-02-24 | 1994-02-24 | Procédé de purification du pentafluoroéthane. |
FR9402114 | 1994-02-24 |
Publications (1)
Publication Number | Publication Date |
---|---|
KR950032032A true KR950032032A (ko) | 1995-12-20 |
Family
ID=9460386
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019950003743A Withdrawn KR950032032A (ko) | 1994-02-24 | 1995-02-24 | 펜타플루오로에탄의 정제 방법 |
Country Status (7)
Country | Link |
---|---|
EP (1) | EP0669302A1 (ko) |
JP (1) | JPH07258123A (ko) |
KR (1) | KR950032032A (ko) |
CN (1) | CN1112541A (ko) |
AU (1) | AU1346395A (ko) |
CA (1) | CA2141657A1 (ko) |
FR (1) | FR2716449B1 (ko) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0778254B1 (en) * | 1994-08-17 | 2000-04-19 | Daikin Industries, Limited | Process for producing pentafluoroethane |
FR2752836B1 (fr) * | 1996-08-30 | 1998-10-30 | Atochem Elf Sa | Purification du pentafluoroethane |
FR2758137B1 (fr) * | 1997-01-06 | 1999-02-26 | Atochem Elf Sa | Procede de purification du pentafluoroethane par distillation extractive |
FR2759078B1 (fr) * | 1997-02-04 | 1999-03-05 | Atochem Elf Sa | Purification du chlorotetrafluoroethane par distillation extractive |
FR2764883B1 (fr) * | 1997-06-18 | 1999-07-16 | Atochem Elf Sa | Procede de fabrication d'hydrofluoroalcanes |
US7060165B2 (en) | 2002-02-14 | 2006-06-13 | Pcbu Services, Inc. | Processes for purification and production of fluorocarbons |
FR3035104B1 (fr) | 2015-04-14 | 2017-04-07 | Arkema France | Procede de purification du pentafluoroethane |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3819493A (en) * | 1973-04-26 | 1974-06-25 | Phillips Petroleum Co | Process for separating halogenated hydrocarbons by extractive distillation |
GB9018372D0 (en) * | 1990-08-21 | 1990-10-03 | Ici Plc | Separation process |
US5087329A (en) * | 1991-05-16 | 1992-02-11 | E. I. Du Pont De Nemours And Company | Process for separating pentafluoroethane from a mixture of halogenated hydrocarbons containing chloropentafluoroethane |
AU684757B2 (en) * | 1993-05-25 | 1998-01-08 | Showa Denko Kabushiki Kaisha | Purification process of pentafluoroethane |
-
1994
- 1994-02-24 FR FR9402114A patent/FR2716449B1/fr not_active Expired - Lifetime
-
1995
- 1995-01-23 EP EP95400125A patent/EP0669302A1/fr not_active Withdrawn
- 1995-02-01 CA CA002141657A patent/CA2141657A1/fr not_active Abandoned
- 1995-02-23 AU AU13463/95A patent/AU1346395A/en not_active Abandoned
- 1995-02-24 CN CN95100903A patent/CN1112541A/zh active Pending
- 1995-02-24 JP JP7036439A patent/JPH07258123A/ja active Pending
- 1995-02-24 KR KR1019950003743A patent/KR950032032A/ko not_active Withdrawn
Also Published As
Publication number | Publication date |
---|---|
EP0669302A1 (fr) | 1995-08-30 |
CN1112541A (zh) | 1995-11-29 |
JPH07258123A (ja) | 1995-10-09 |
FR2716449B1 (fr) | 1996-04-05 |
CA2141657A1 (fr) | 1995-08-25 |
FR2716449A1 (fr) | 1995-08-25 |
AU1346395A (en) | 1995-08-31 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19950224 |
|
PG1501 | Laying open of application | ||
PC1203 | Withdrawal of no request for examination | ||
WITN | Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid |