KR940008064B1 - Making method of hot rolling steel plate - Google Patents
Making method of hot rolling steel plate Download PDFInfo
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- KR940008064B1 KR940008064B1 KR1019910025119A KR910025119A KR940008064B1 KR 940008064 B1 KR940008064 B1 KR 940008064B1 KR 1019910025119 A KR1019910025119 A KR 1019910025119A KR 910025119 A KR910025119 A KR 910025119A KR 940008064 B1 KR940008064 B1 KR 940008064B1
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- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/02—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips
- C21D8/04—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing
- C21D8/0421—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing characterised by the working steps
- C21D8/0426—Hot rolling
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- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D6/00—Heat treatment of ferrous alloys
- C21D6/005—Heat treatment of ferrous alloys containing Mn
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/004—Very low carbon steels, i.e. having a carbon content of less than 0,01%
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/12—Ferrous alloys, e.g. steel alloys containing tungsten, tantalum, molybdenum, vanadium, or niobium
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/14—Ferrous alloys, e.g. steel alloys containing titanium or zirconium
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- Crystallography & Structural Chemistry (AREA)
- Heat Treatment Of Steel (AREA)
- Heat Treatment Of Sheet Steel (AREA)
Abstract
내용 없음.No content.
Description
제1도는 열연코일에서 재결정이 일어나는 본 발명의 열간압연 마무리 온도 및 권취온도 범위를 나타내는 그래프.1 is a graph showing a hot rolling finish temperature and a winding temperature range of the present invention in which recrystallization occurs in a hot rolled coil.
제2도는 윤활압연에 의한 전단변형 감소에 따른 두께방향 유효변형율 분포의 차이를 나타내는 그래프.2 is a graph showing the difference in the effective strain distribution in the thickness direction according to the reduction of the shear strain by lubrication rolling.
본 발명은 고가공용 열연강판의 제조방법에 관한 것으로서, 보다 상세하게는, 연속식 윤활열간압연에 의해 고가공용 열연강판을 제조하는 방법에 관한 것이다.The present invention relates to a method for manufacturing a hot rolled steel sheet for high processing, and more particularly, to a method for producing a hot rolled steel sheet for continuous processing by continuous lubricating hot rolling.
얇은 강판은 성형할 때에는 스트레칭(stretching), 딥드로잉(deepdrawing)등의 여러가지의 가공형태가 복합적으로 작용하는 것이 일반적이다. 그런데 스트레칭 가공의 경우에는 강판의 기계적 성질 중 연신율이 우수한 것이 요구되고, 딥드로잉 가공의 경우에는 γavg치가 우수한 것이 요구된다. 지금까지의 많은 연구는 열연강판에서 가공성을 향상시키기 위해 스트레칭성 또는 딥드로잉성을 각각 향상시키기 위한 것이었으며, 두 조건을 동시에 만족시키는 연구 결과는 별로 보고된 바 없다.When forming a thin steel sheet, it is common to have a combination of various processing forms such as stretching and deepdrawing. By the way, in the case of stretching processing, it is required to have excellent elongation among the mechanical properties of the steel sheet, and in the case of deep drawing processing, it is required to have excellent γavg value. To date, many studies have been conducted to improve the stretchability or the deep drawing property in order to improve the workability in hot rolled steel sheets, and few studies have been reported to satisfy both conditions simultaneously.
통상, γavg치는 (111)집합조직의 발달과 관계가 깊다고 알려져 있는데 강판에서의 집합조직이 (111)면이 압연판 면에 평행하게 발달된 정도가 클수록 γavg치는 증가하여 딥드로잉성이 향상되나, (100)면이 압연판면에 평행하게 발달되면 딥드로잉성은 나빠진다. 그런데, 통상의 오스테나이트역 마무리 압연재의 경우에는 열간압연을 종료한 후 페라이트로의 변태가 일어나서 오스테나이트에서 발달하였던 집합조직이 변태과정 중에 크게 약화되어 딥드로잉성은 나빠진다. 따라서 통상의 열연강판의 경우 γavg치는 0.7-0.9정도이다.In general, the γavg value is known to be deeply related to the development of the (111) aggregate structure. As the degree of development of the (111) plane parallel to the rolled plate surface of the aggregate structure in the steel sheet increases the γavg value, the deep drawing property is improved. If the (100) plane is developed parallel to the rolled plate surface, the deep drawing property deteriorates. By the way, in the case of the normal austenite finish rolling material, after the hot rolling is completed, the transformation into ferrite occurs, and the aggregate structure developed in the austenite is greatly weakened during the transformation process, resulting in poor deep drawing property. Therefore, in the case of a general hot-rolled steel sheet, the γavg value is about 0.7-0.9.
최근에 이와 같은 열연강판의 딥드로잉성을 향상시키기 위해 페라이트 영역에서 열간압연을 마무리하여 γavg치를 향상시키는 방법들이 제안되고 있는데, 그 일례로서 열간압연을 페라이트 영역에서 마무리할때 그 변형율 속도를 300/초 이상으로 하여 딥드로잉성이 우수한 열연강판을 제조하는 방법(한국특허 공고번호 제91-1606호)을 들수 있다.Recently, in order to improve the deep drawing property of such hot rolled steel sheets, methods for improving γavg value by finishing hot rolling in a ferrite region have been proposed. For example, when the hot rolling is finished in a ferrite region, the strain rate is 300 /. The method of manufacturing a hot rolled steel sheet excellent in deep drawing property by more than a second (Korean Patent Publication No. 91-1606) can be mentioned.
그러나, 상기 방법에서 변형율 속도를 300/초 이상으로 하는 것은 현재 통상의 열간압연기에서 변형율 속도가 최대 100/초 정도라는 점을 감안할때 설비의 증강을 요구하게 된다.However, in the above method, the strain rate of 300 / sec or more requires the reinforcement of the equipment in view of the fact that the strain rate is about 100 / sec at most in the current hot rolling mill.
또한, 일본 특개(소)59-226149호에는 딥드로잉성이 우수한 열연강재를 제조하기 위해 윤활압연을 행하고, 강재의 화학조성을 조정하는 방법이 제시되어 있는데, 여기서도 스트레칭 가공성에 대한 내용은 제시되어 있지 않다.In addition, Japanese Unexamined Patent Publication No. 59-226149 discloses a method of lubricating and adjusting the chemical composition of steel to manufacture hot rolled steel having excellent deep drawing property. not.
또한, 하시모토등은 열연강재에서의 스트레칭성을 향상시키기 위해 페라이트 역에서 마무리 압연을 행하는 방법에 대하여 제안한 바 있었으나, 딥드로잉성에 관한 검토는 없었다(재료와 프로세스, 89-1824).In addition, Hashimoto et al. Proposed a method of performing finish rolling in a ferritic station to improve the stretchability of hot rolled steel, but did not examine the deep drawing property (materials and processes, 89-1824).
상기한 방법들은 페라이트 영역에서 열간압연을 종료하기 때문에 별도의 재결정 열처리를 행하는 공정을 채택하고 있는데, 이는 공정의 추가에 따른 제조원가의 상승을 초래하는 단점이 있다.Since the above methods terminate the hot rolling in the ferrite region, a separate recrystallization heat treatment is adopted, which has a disadvantage in that the manufacturing cost increases due to the addition of the process.
본 발명은 상기한 종래 방법의 단점들을 해결하기 위하여 제안된 것으로서, Ar3온도이하의 저온에서 윤활압연을 행하여 별도의 재결정 열처리없이 스트레칭성과 딥드로잉성이 우수한 열연강판을 직접 제조할 수 있는 방법을 제공하고자 하는데, 그 목적이 있다.The present invention has been proposed to solve the above-mentioned disadvantages of the conventional method, by performing lubrication rolling at a low temperature below the Ar 3 temperature, a method for directly manufacturing a hot rolled steel sheet having excellent stretch and deep drawing properties without a separate recrystallization heat treatment. I want to provide it, and its purpose is.
이하, 본 발명을 설명한다.Hereinafter, the present invention will be described.
본 발명은, 중량%로, C : 0.01% 이하, N : 0.01% 이하, Mn : 1.0% 이하, Si : 0.5% 이하, Al : 0.1% 이하, S : 0.015% 이하, Ti과 Nb의 단독 또는 복합 : 0.04∼0.06%, 잔부 Fe 및 기타 불가피하게 함유되는 불순물로 조성되는 강소재를 1150℃ 이하로 가열한 후, 열간압연 마무리 온도 : 700∼(권취온도+100)℃, 권취온도 : 650∼700℃ 및 910℃ 이하에서의 압하량 ; 진변형률로 2.2이상의 조건으로 연속식 윤활 열간압연하여 고가공용 열연강판을 제조하는 방법에 관한 것이다.The present invention, in weight%, C: 0.01% or less, N: 0.01% or less, Mn: 1.0% or less, Si: 0.5% or less, Al: 0.1% or less, S: 0.015% or less, Ti and Nb alone or Composite: 0.04% to 0.06%, remainder Fe and other steels made of impurities inevitably contained after heating to 1150 ° C or less, hot rolling finish temperature: 700 to (winding temperature + 100) ℃, winding temperature: 650 to Rolling reduction at 700 ° C and 910 ° C or lower; The present invention relates to a method for producing a hot rolled steel sheet for continuous processing by hot rolling with continuous lubrication under a true strain of 2.2 or more.
이하, 상기 강성분들의 수치한정 이유에 대하여 설명한다.Hereinafter, the reason for numerical limitation of the steel components will be described.
상기 C(탄소) 및 N(질소)는 강중에 침입형 불순원소로 존재하거나, 첨가되는 원소의 탄질화물을 형성하는 등, 그 성질이 서로 유사하며 냉연강판의 경우에는 연신율과 γavg치를 낮추는 대표적인 원소로 알려져 있다. 따라서 Ti 또는 Nb를 첨가하여 이들 원소를 탄질화물로 고정하여 가공성을 향상시키고 있는데, 열연강판의 경우에도 동일한 현상이 나타남이 보고되고 있어서 탄소 및 질소의 함량은 낮추는 것이 가공성에 유리하다.The C (carbon) and N (nitrogen) are similar to each other in the nature, such as the presence of infiltration-type impurity elements in the steel, or to form carbonitride of the added element, and in the case of cold-rolled steel sheet to lower the elongation and γavg value Known as Therefore, by adding Ti or Nb to fix these elements with carbonitrides to improve the workability, the same phenomenon is reported in the case of hot-rolled steel sheet, it is advantageous to workability to lower the content of carbon and nitrogen.
본 발명에 있어서 강중의 탄소함량 및 질소함량이 각각 0.01% 이상이면 이들을 탄질화물로 고정하는데 필요한 Ti 및 Nb 함량이 증가하여 강제적이지 못할뿐만 아니라 상기 γavg치는 향상되나 연신율이 감소되므로, 상기 탄소 및 질소의 함량은 0.01% 이하로 한정하는 것이 바람직하다.In the present invention, when the carbon content and the nitrogen content in the steel are each 0.01% or more, the Ti and Nb contents required for fixing them as carbonitrides are not compulsory due to an increase in the γavg value but the elongation is reduced, thereby reducing the carbon and nitrogen. The content of is preferably limited to 0.01% or less.
상기 Si은 일반적으로 탈산에 이용되는 원소로서 가공성 향상 효과는 별로 없지만, 그 함유량이 높으면 열연코일의 표면품질, 냉연제품의 화성처리 및 점용접성이 나빠지므로, Si의 함량은 0.5% 이하로 제한하는 것이 바람직하다.Si is generally an element used for deoxidation, but there is little effect of improving workability, but if the content is high, the surface quality of the hot rolled coil, the chemical conversion treatment and the spot weldability of the cold rolled product are deteriorated, so the content of Si is limited to 0.5% or less. It is preferable.
상기 Mn은 강도향상효과를 나타내는 원소이나, 그 함유량이 높으면 페라이트 온도영역을 저하시켜 열간압연이 페라이트 영역에서 행해질 때 변형저항을 증가시켜 실제조업이 곤란하게 되는 문제점이 있으므로 그 함량은 1.0% 이하로 제한하는 것이 바람직하다.The Mn is an element exhibiting an effect of improving strength, but if the content thereof is high, the ferrite temperature range is lowered, so that the deformation resistance is increased when hot rolling is performed in the ferrite region. It is desirable to limit.
상기 Al은 냉연강재의 탈산원소로 주로 이용되는 원소이며, 질소를 AIN으로 고정하는 역활을 하지만, 본 발명 강에 있어서는 질소의 고정은 Al 대신 Ti로 하는 것을 목적으로 하기 때문에 Al의 함량이 많으면 경제적으로 불리할 뿐만 아니라 Al2O3와 같은 개재물이 증가하여 표면 품질이 나빠지므로, Al의 함량은 0.1% 이하로 제한하는 것이 바람직하다.Al is an element mainly used as a deoxidation element of cold rolled steel, and serves to fix nitrogen as AIN. However, in the present invention steel, since nitrogen is fixed to Ti instead of Al, it is economical if the content of Al is high. In addition to the disadvantages, since the inclusions such as Al 2 O 3 is increased to deteriorate the surface quality, it is preferable to limit the content of Al to 0.1% or less.
상기 S는 Ti로 고정되는 원소로서, 그 함량이 높으면 이에 상응하여 Ti의 함량이 높아지기 때문에 연신율이 저하되고, 경제적으로 불리하므로, 그 함량은 0.015% 이하로 한정하는 것이 바람직하다.S is an element fixed to Ti, and if the content is high, the content of Ti is increased correspondingly, so the elongation is lowered and it is economically disadvantageous. Therefore, the content is preferably limited to 0.015% or less.
상기 Ti 또는 Nb은 탄질화물을 형성하여 고용탄소 또는 고용질소의 함량을 낮추어 가공성을 향상시키는 역할을 하는데, 본 발명에 있어서는 Ti 단독 또는 Nb 단독 또는 이들을 복합하여 첨가하는 것으로서, 상기 Ti과 Nb의 단독 또는 복합첨가량이 0.04% 이하인 경우에는 충분히 탄질화물을 형성하지 못하고, 그 첨가량이 너무 많으면, 탄질화물을 형성하는 양을 제외하고도 상당량이 고용상태로 존재하게 되며, 이러한 고용 Ti와 Nb은 딥드로잉성에는 문제가 없으나, 연신율을 저하시키기 때문에 스트레칭성을 나쁘게 하므로 본 발명에서는 Ti 및 Nb 함량의 단독 또는 복합첨가량을 0.04∼0.06%로 제한하는 것이 바람직하다.The Ti or Nb forms a carbonitride to lower the content of solid solution carbon or solid solution nitrogen to improve workability. In the present invention, Ti alone or Nb alone or a combination thereof is added, and the Ti and Nb alone Alternatively, when the compounding amount is 0.04% or less, the carbonitride may not be formed sufficiently. If the amount of addition is too large, a considerable amount of the carbonitride may be present in solid solution, except for the formation of carbonitride. Although there is no problem in the property, since the elongation is lowered, the stretching property is deteriorated. Therefore, in the present invention, it is preferable to limit the amount of Ti and Nb content alone or in combination to 0.04 to 0.06%.
이하, 열간압연 조건의 한정 이유에 대하여 설명한다.Hereinafter, the reason for limitation of hot rolling conditions is demonstrated.
열간압연된 페라이트가 재결정되는 현상은 압연시에 가해진 변형에너지를 구동적으로 하여 재결정립이 생성되어 성장하는 과정이므로 변형량이 많을수록 변형후 유지온도가 높을수록 압연온도가 낮을수록 재결정이 용이하다.The re-crystallization of the hot-rolled ferrite is a process in which recrystallized grains are formed and grown by driving the strain energy applied during rolling, so that the larger the amount of deformation, the higher the holding temperature after deformation, and the lower the rolling temperature, the easier the recrystallization.
상기 압연 마무리 온도가 너무 높으면 압연시에 가해지는 변형에너지가 압연과 동시에 동적 회복에 의해 소멸되는 양이 많아서 재결정에 필요한 만큼의 충분한 변형에너지가 남지 않으므로 그 상한은(권취온도+100)℃의 온도로 한정하는 것이 바람직하다.If the rolling finish temperature is too high, the amount of strain energy applied at the time of rolling is extinguished by dynamic recovery at the same time as rolling, so that sufficient strain energy does not remain as necessary for recrystallization, so the upper limit is (winding temperature +100) ° C. It is preferable to limit to.
반면에, 압연 마무리 온도가 낮을수록 축적되는 변형에너지 양은 증가하여 재결정에 유리하지만, 그 하한은 실제 열연공장에서 마무리 압연 후 권취공정까지의 냉각과정에서 적어도 5℃의 온도 강하가 있다는 점을 고려할때 권취온도의 하한이 650℃이므로 이에 따른 마무리 압연 온도의 하한은 700℃로 한정한다.On the other hand, as the rolling finish temperature is lower, the amount of strain energy accumulated increases, which is advantageous for recrystallization. However, the lower limit thereof is at least 5 ° C in the cooling process from the finish rolling to the winding process in the hot rolling mill. Since the lower limit of a coiling temperature is 650 degreeC, the minimum of this finishing rolling temperature is limited to 700 degreeC.
한편, 상기 권취온도가 너무 낮으면 변형에너지가 충분하더라도 확산속도가 늦어서 재결정이 일어나지 못하므로 그 하한은 650℃로 한정하는 것이 바람직하고, 권취온도가 너무 높으면 재결정이 일어나기 전에 정적회복에 의해 소멸되는 변형에너지의 양이 많아서 결정립은 이상 조대립으로 발달하므로 권취온도의 상한은 700℃로 한정하는 것이 바람직하다.On the other hand, if the coiling temperature is too low, even if the strain energy is sufficient, the diffusion rate is slow and recrystallization does not occur, so the lower limit is preferably limited to 650 ℃, if the coiling temperature is too high is extinguished by static recovery before recrystallization occurs Since the amount of strain energy is large and crystal grains develop into coarse grains, the upper limit of the winding temperature is preferably limited to 700 ° C.
상기 온도조건 범위에서 열간압연을 행할때 축적되는 변형에너지는 가해지는 변형율에 의해 결정되며, 이때 변형율이 증가할수록 재결정은 일어나기 쉽게 되므로, 페라이트 변태가 시작되는 온도인 910℃ 이하에서의 압하량은 진변형율로 2.2이상이 되도록 제한하는 것이 바람직하다.The strain energy accumulated during hot rolling in the above temperature condition range is determined by the strain applied, and as the strain increases, recrystallization is likely to occur, so the rolling reduction at 910 ° C. or lower, which is the temperature at which ferrite transformation starts, is true. It is desirable to limit the strain to 2.2 or more.
상기한 열연조건을 다시 정리해보면, 열연코일의 미세조직을 재결정시키기 위해서는 페라이트역에서의 진변형율을 2.2이상 가하여 압연할때 제1도에 나타난 바와 같이 압연조건의 범위를 권취온도는 650℃ 이상 700℃ 이하로 하고, 권취온도가 650℃인 경우에는 열간압연 마무리 온도를 700℃ 이상 750℃ 이하의 범위로 제어해 주어야 하고, 권취온도가 700℃인 경우에는 열간압연 온도범위를 700℃ 이상 800℃ 이하의 범위로 제어해 주어야 하고, 권취온도가 650℃에서 700℃ 사이인 경우에는 열간압연 마무리 온도를 700℃ 이상(권취온도+100)℃ 이하로 제어해 주어야 한다.To summarize the above hot rolling conditions, in order to recrystallize the microstructure of the hot rolled coil, when rolling with a true strain rate of 2.2 or more in the ferrite region, as shown in FIG. 1, the winding temperature ranges from 650 ° C to 700. When the coiling temperature is lower than or equal to 650 ° C and the winding temperature is 650 ° C, the hot rolling finish temperature must be controlled in the range of 700 ° C or higher and 750 ° C or lower. When the winding temperature is 700 ° C, the hot rolling temperature range is 700 ° C or higher and 800 ° C. It should be controlled within the following range, and in case the winding temperature is between 650 ℃ and 700 ℃, hot rolling finish temperature should be controlled to 700 ℃ or more (coiling temperature + 100) ℃.
이때의 재결정 미세조직은 마치 냉연 후 소둔된 미세조직을 열간압연 과정에서 얻어진 것과 유사하고, 그 가공성 또는 집합조직의 발달경향은 냉연재에서와 유사하다고 생각할 수 있다.At this time, the recrystallized microstructure is similar to that obtained in the hot rolling process of the annealing microstructure after cold rolling, and the processability or development tendency of the aggregate structure can be considered to be similar to that of the cold rolling material.
본 발명에 적용되는 윤활압연 방식으로는 당업계에서 사용되고 있는 어떠한 윤활압연 방식이라도 가능하며, 이 윤활압연방식은 물과 함께 윤활유를 압연롤에 뿌려주면서 열간압연을 행하는 방식이다.The lubrication rolling method applied to the present invention may be any lubrication rolling method used in the art, and this lubrication rolling method is a method of performing hot rolling while spraying lubricating oil together with water onto a rolling roll.
본 발명에 의해 제조된 열연코일은 열간압연 상태에서 미세조직이 재결정되었기 때문에 별도의 재결정 열처리가 필요없이 가공성이 우수하고, 또한 압연시의 변형속도가 통상의 변형속도 범위이내이기 때문에 별도의 설비보강 없이도 적용가능하며, 또한 가열온도가 낮아서 통상적인 슬라브 제조공정 외에도 박슬라브 주조공정(Thin Slab Casting) 또는 직송압연기술(Hot Direct Rolling)과도 연결지워 사용할 수 있는 장점이 있으며, 통상의 슬라브 제조공정에서는 에너지 절감효과가 크고, 스케일로스(scale loss)가 적어서 실수율이 높다.The hot rolled coil manufactured by the present invention is excellent in workability without the need for a separate recrystallization heat treatment because the microstructure is recrystallized in the hot rolling state, and the additional equipment reinforcement because the deformation rate during rolling is within the normal deformation rate range. It can be applied without and also has the advantage that it can be used in connection with thin slab casting or hot direct rolling in addition to the conventional slab manufacturing process due to the low heating temperature. High energy savings, low scale loss, high error rate.
본 발명에 따라 열간압연된 열연강판의 가공성이 향상되는 이유는 다음과 같다.The reason why the workability of the hot rolled hot rolled steel sheet according to the present invention is improved is as follows.
통상의 오스테나이트 영역에서 열간압연을 마무리한 코일에 비해서는 열간압연을 페라이트 영역에서 마무리하였기 때문에 집합조직의 제어가 용이하여 딥드로잉성을 향상시킬 수 있다. 이때 딥드로잉성의 향상은 냉연강판에서와 동일한 기구로 이루어진다고 생각되며, 고용탄소 및 고용질소의 함량감소가 중요한데, 오스테나이트에서의 탄소 및 질소 고용도에 비해 페라이트에서의 고용도가 낮기 때문에 페라이트에서의 열간압연은 보다 효과적으로 고용탄소 및 고용질소의 함량을 낮추는 효과가 있을 뿐만 아니라 고용탄소 함량이 감소되면, 연신율이 증가되는 효과가 동시에 나타나는데 이는 가공성을 더욱 좋게하는 효과가 있다.Compared to a coil in which hot rolling is finished in the normal austenite region, hot rolling is finished in the ferrite region, so that the texture of the texture can be easily controlled and the deep drawing property can be improved. In this case, it is thought that the improvement of deep drawing is made with the same mechanism as that of cold rolled steel sheet, and it is important to reduce the content of solid solution carbon and solid solution nitrogen, and because the solid solubility in ferrite is low compared to that of carbon and nitrogen in austenite, The hot rolling of not only effectively lowers the content of solid solution carbon and solid solution nitrogen, but also decreases the content of solid solution carbon, so that the effect of increasing the elongation is simultaneously produced, which has the effect of improving workability.
더우기, 본 발명에 있어서는 Ti 및 Nb를 단독 또는 복합첨가하므로서 이들이 탄질화물을 형성하여 고용탄소 및 고용질소의 함량을 낮추므로서 가공성을 더욱 향상시키게 된다.Moreover, in the present invention, by adding Ti and Nb alone or in combination, they form carbonitrides to further improve workability by lowering the content of solid solution carbon and solid solution nitrogen.
이하, 실시예를 통하여 본 발명을 보다 구체적으로 설명한다.Hereinafter, the present invention will be described in more detail with reference to Examples.
[실시예 1]Example 1
하기표 1과 같이 조성되는 강소재를 950℃로 가열한 후, 마무리 압연 온도 : 750℃, 권취온도 : 700℃ 및 910℃ 이하에서의 압하량 : 진변형율로 2.2가 되는 조건으로 윤활 및 비윤활 열간압연을 행한 다음, 열간압연시의 윤활여부에 따른 스트레칭성 및 딥드로잉성의 영향을 조사하기 위해 항복강도, 인장강도, 연신율 및 γavg값을 측정하고, 그 측정결과를 하기표 2에 나타내었다.After heating the steel material to be prepared as shown in Table 1 to 950 ℃, finish rolling temperature: 750 ℃, winding temperature: 700 ℃ and rolling pressure at 910 ℃ or less: lubrication and non-lubrication under the condition that the true strain is 2.2 After hot rolling, yield strength, tensile strength, elongation, and γavg were measured to investigate the effects of stretching and deep drawing on the lubrication during hot rolling. The results are shown in Table 2 below.
[표 1]TABLE 1
[표 2]TABLE 2
상기표 2에 나타난 바와 같이, 발명재(a)와 비교재(1)은 스트레칭성을 나타내는 연신율에 있어서 거의 동일한 값을 나타내고 있는데, 이로부터 스트레칭성은 열간압연시의 윤활여부와는 무관하다는 것을 알수 있다.As shown in Table 2, the inventive material (a) and the comparative material (1) showed almost the same value in the elongation exhibiting the stretchability, from which it can be seen that the stretchability is independent of lubrication during hot rolling. have.
반면에, 발명재(a)는 비교재(1)에 비하여 딥드로잉성을 나타내는 γavg값에 있어서 더 큰 값을 나타내고 있는데, 이로부터 윤활압연을 하는 경우가 윤활압연을 하지 않는 경우보다 딥드로잉성에 있어 우수하다는 것을 알 수 있다.On the other hand, the inventive material (a) shows a larger value in the? Avg value indicating deep drawing property than the comparative material (1), whereby lubrication rolling is more effective on deep drawing than when lubrication rolling is not performed. It can be seen that it is excellent.
이와 같이 윤활압연을 하므로서 딥드로잉성이 향상되는 것은 열간압연시의 롤과 소재와의 마찰에 기인되는 현상으로서, 이를, 윤활압연에 의한 전단변형 감소에 따른 두께 방향유효 변형율 분포의 차이를 나타내는 제2도를 통해 구체적으로 설명하면 다음과 같다.The improvement of the deep drawing property by lubrication rolling is caused by the friction between the roll and the material during hot rolling, and this is a product which shows the difference in the thickness direction effective strain distribution according to the reduction of shear deformation by lubrication rolling. If specifically described through 2 degrees are as follows.
제2도에 나타난 바와 같이, 윤활압연재[발명재(a)]에서는 표층부와 중심부의 변형율 분포가 균일하게 되지만, 윤활을 행하지 않은 압연재[비교재(1)]에서는 마찰때문에 표층부에 전단변형이 집중되는 효과가 있음을 알수 있는데, 이러한 전단변형의 집중은 표충부에서 (110)집합조직의 발달을 조장하고, (111)집합조직의 발달을 억제하여 딥드로잉성을 나쁘게 한다.As shown in FIG. 2, in the lubricated rolled material (invention material (a)), the strain distribution between the surface layer portion and the center portion is uniform, while in the rolled material (comparative material (1)) without lubrication, shear deformation in the surface layer portion due to friction. It can be seen that there is a concentrated effect, such a concentration of shear deformation encourages the development of (110) aggregates in the worms, and inhibits the development of (111) aggregates, worsening deep drawing.
그리고, 이러한 윤활압연의 효과는 강판의 화학조성과는 무관함을 알수 있다.In addition, it can be seen that the effect of the lubrication rolling has nothing to do with the chemical composition of the steel sheet.
[실시예 2]Example 2
하기표 3과 같이 조성되는 강소재를 950℃로 가열한 후 마무리 압연 온도 : 750℃, 권취온도 : 700℃ 및 910℃ 이하에서 압하율 : 진변형률로 2.2가 되는 조건으로 윤활연간압연을 행한 다음, 연신율 및 γavg치를 측정하고, 그 측정결과를 하기표 4에 나타내었다.After heating the steel material as shown in Table 3 to 950 ℃ and finish rolling temperature: 750 ℃, winding temperature: 700 ℃ and 910 ℃ or less rolling rate: lubricated rolled to a condition that is 2.2 as true strain rate , Elongation and γavg value were measured, and the measurement results are shown in Table 4 below.
[표 3]TABLE 3
[표 4]TABLE 4
[표 5]TABLE 5
상기한 표 5에 나타난 바와 같이, 강소재의 가열온도를 1150℃ 이하로하여 열간압연한 발명재(d∼f)는 강소재의 가열온도를 1250℃로 하여 열간압연한 비교재(5)에 비하여 연신율 및 γavg값이 크게 나타나고 있는 바, 스트레칭성 및 딥드로잉성에 있어서 보다 우수함을 알수 있다.As shown in Table 5 above, the invention materials (d to f) hot-rolled at a heating temperature of the steel material to 1150 ° C. or lower were applied to the comparative material (5) hot-rolled at a heating temperature of the steel material to 1250 ° C. Elongation and γavg values are larger than those of the present invention, indicating that stretching and deep drawing properties are excellent.
상술한 바와 같이, 본 발명은 딥드로잉성과 스트레칭성을 동시에 향상시켜 통상의 가공형태에서 나타나는 복합적인 가공양상에서 가공이 용이한 소재를 제고하고, 또한, 열연판 재결정 열처리를 생략할 수 있으므로 공정단축에 의한 원가절감효과를 가져올 수 있고, 통상의 방법인 오스테나이트 영역에서 열간압연을 마무리 하는 경우에 비해 압연온도가 낮기 때문에 슬라브의 가열온도를 낮출수 있으므로 에너지 절감효과가 매우 크고, 가열시의 스케일 생성량이 적어서 열연코일의 실수율을 향상시킬 수 있는 효과가 있는 것이다.As described above, the present invention improves both the deep drawing and the stretchability at the same time, thereby improving the material that is easy to process in the complex processing pattern shown in the conventional processing form, and also eliminating the hot-rolled sheet recrystallization heat treatment process. It is possible to bring about cost reduction effect and the heating temperature of slab can be lowered because the rolling temperature is lower than that of hot rolling in austenite area, which is a common method. Since the amount of production is small, there is an effect that can improve the error rate of the hot rolled coil.
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