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KR927003488A - 술폰화제 및 술폰화법 - Google Patents

술폰화제 및 술폰화법 Download PDF

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Publication number
KR927003488A
KR927003488A KR1019920701398A KR920701398A KR927003488A KR 927003488 A KR927003488 A KR 927003488A KR 1019920701398 A KR1019920701398 A KR 1019920701398A KR 920701398 A KR920701398 A KR 920701398A KR 927003488 A KR927003488 A KR 927003488A
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KR
South Korea
Prior art keywords
sulfonating agent
sulfonic acid
sulfonation method
trimethylbenzene
compound
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KR1019920701398A
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English (en)
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KR0185224B1 (ko
Inventor
에이지 오가따
노리오 야나세
다까유끼 기따하라
Original Assignee
고니시 기히꼬
고니시가가꾸고오교 가부시끼가이샤
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Publication of KR927003488A publication Critical patent/KR927003488A/ko
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Publication of KR0185224B1 publication Critical patent/KR0185224B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B45/00—Formation or introduction of functional groups containing sulfur
    • C07B45/02—Formation or introduction of functional groups containing sulfur of sulfo or sulfonyldioxy groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F8/00—Chemical modification by after-treatment
    • C08F8/34—Introducing sulfur atoms or sulfur-containing groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/02—Ortho- or ortho- and peri-condensed systems
    • C07C2603/04—Ortho- or ortho- and peri-condensed systems containing three rings
    • C07C2603/22—Ortho- or ortho- and peri-condensed systems containing three rings containing only six-membered rings
    • C07C2603/24—Anthracenes; Hydrogenated anthracenes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

내용 없음

Description

술폰화제 및 술폰화법
[도면의 간단한 설명]
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (17)

  1. 일반식(I)로 나타내지는 술폰화제.
    (상기 식중에서, R1기는 같거나 다르며 각각 1 내지 3 탄소원자를 갖는 저급 알킬기이고, n은 3,4 또는 5의 정수, m은 1 또는 2의 정수이며 n+m≤6 이다.)
  2. 제1항에 있어서, R1이 메틸 또는 에틸인 술폰화제.
  3. 제2항에 있어서, R1이 메틸인 술폰화제.
  4. 제1항 또는 2항에 있어서, n이 3인 술폰화제.
  5. 제1항 내지 제3항의 어느 한 항에 있어서, m이 1인 술폰화제.
  6. 제1항에 있어서, 1,3,5-트리메틸벤젠-2-술폰산, 1,2,4,5-테트라메틸벤젠-3-술폰산, 1,2,3,5-테트라메틸벤젠-4-술폰산, 1,2,3,4,5-펜타메틸벤젠-6-술폰산, 1,3,5-트리메틸벤젠-2,4-디술폰산 및 1,3,5-트리에틸벤젠-2-술폰산으로 이루어진 군에서 선택된 화합물인 술폰화제.
  7. 제6항에 있어서, 1,3,5-트리메틸벤젠-2-술폰산인 술폰화제.
  8. 술폰화제로 작용하며 하기 일반식으로 나타내지는 화합물로 방향족 화합물을 술폰화시킴을 특징으로 하는 방향족 화합물 술폰화법.
    (상기 식에서, R1기는 같거나 다르며 각각 1 내지 3 탄소윈자를 갖는 저급 알킬기이고, n은 3,4 또는 5의 정수, m은 1 또는 2의 정수이고 n+m≤6 이다.)
  9. 제8항에 있어서. R1이 메틸 또는 에틸인 술폰화법.
  10. 제9항에 있어서, R1이 메틸인 술폰화법.
  11. 제8항 또는 제9항에 있어서, n이 3인 술폰화법.
  12. 제8항 내지 제10항의 어느 한 항에 있어서, m이 1인 술폰화법.
  13. 제8항에 있어서, 술폰화제가 1,3,5-트리메틸벤젠-2-술폰산, 1,2,4,5-테트라메틸벤젠-3-술폰산, 1,2,3,5-테트라메틸벤젠-4-술폰산, 1,2,3,4,5-펜타메틸벤젠-6-술폰산, 1,3,5-트리메틸벤젠-2,4-디술폰산 및 1,3,5-트리에틸벤젠-2-술폰산으로 이루어진 군에서 선택된 하나 이상의 화합물인 술폰화법.
  14. 제13항에 있어서, 술폰화제가 1.3,5-트리메틸벤젠-2-술폰산인 술폰화법.
  15. 제8항에 있어서, 방향족 화합물이 방향족 아민 화합물인 술폰화법.
  16. 제8항에 있어서, 방향족 화합물이 아미노로 치환되지 않은 방향족 화합물인 술폰화법.
  17. 제8항에 있어서, 방향족 화합물이 방향족 고분자량 화합물인 술폰화법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019920701398A 1990-10-12 1991-10-09 술폰화제 및 술폰화법 KR0185224B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP90-273725 1990-10-12
JP27372590 1990-10-12
PCT/JP1991/001372 WO1992006935A1 (en) 1990-10-12 1991-10-09 Sulfonating agent and process

Publications (2)

Publication Number Publication Date
KR927003488A true KR927003488A (ko) 1992-12-18
KR0185224B1 KR0185224B1 (ko) 1999-05-15

Family

ID=17531694

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019920701398A KR0185224B1 (ko) 1990-10-12 1991-10-09 술폰화제 및 술폰화법

Country Status (7)

Country Link
US (1) US5596128A (ko)
EP (1) EP0505582B1 (ko)
KR (1) KR0185224B1 (ko)
CA (1) CA2070663C (ko)
DE (1) DE69121188T2 (ko)
TW (1) TW198708B (ko)
WO (1) WO1992006935A1 (ko)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6048904A (en) * 1998-12-01 2000-04-11 Exxon Research And Engineering Co. Branched alkyl-aromatic sulfonic acid dispersants for solublizing asphaltenes in petroleum oils
ATE444328T1 (de) * 2002-10-08 2009-10-15 Toyo Boseki Sulfonsuuregruppenhaltige polyarylenether- verbindung, diese enthaltende zusammensetzung und verfahren zu deren herstellung
EP1810997B1 (en) 2004-11-10 2011-03-09 Toyo Boseki Kabushiki Kaisha Proton-conducting polymer composition and method for preparation thereof, catalyst ink containing said proton-conducting polymer composition and fuel cell including said catalyst
JPWO2006137473A1 (ja) * 2005-06-24 2009-01-22 日産化学工業株式会社 芳香族スルホン酸化合物の製造法
BRPI0711690B1 (pt) 2006-06-15 2018-05-08 Dow Global Technologies Inc composição e artigo
JP4836080B2 (ja) * 2007-01-09 2011-12-14 小西化学工業株式会社 スルホン化排出液の処理方法及びスルホン化排出液のリサイクル方法
WO2013094586A1 (ja) * 2011-12-22 2013-06-27 小西化学工業株式会社 芳香族ポリマーのスルホン化物の製造方法
CN103936636B (zh) * 2013-01-23 2016-05-25 中国科学院大连化学物理研究所 一种甲苯磺化制备对甲苯磺酸的方法
CN103274971B (zh) * 2013-06-19 2014-08-06 太仓沪试试剂有限公司 一种5-磺基水杨酸的纯化方法
CN104447420B (zh) * 2014-10-29 2016-08-24 宁夏共享化工有限公司 一种铸造砂型喷墨打印树脂用磺酸固化剂的生产方法
CN105968033B (zh) * 2016-05-12 2018-02-16 浙江正大新材料科技有限公司 一种3,4‑二氯苯胺‑6‑磺酸的生产方法
CN106146356B (zh) * 2016-07-01 2018-07-20 宁夏紫光川庆化工有限公司 连续生产1-萘磺酸的方法
CN106831500A (zh) * 2017-01-19 2017-06-13 南通海之阳膜化工有限公司 一种g盐及其副产物r盐的制备方法
CN108863856B (zh) * 2018-06-15 2021-06-01 永华化学股份有限公司 一种分析纯试剂5-磺基水杨酸提纯方法

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3222393A (en) * 1962-05-07 1965-12-07 Union Oil Co 1,2,3,4-tetraalkyl benzene sulfonic acid production
GB1434020A (en) * 1972-10-30 1976-04-28 Koebner A Sulphonation of aromatic compounds in the presence of solvents

Also Published As

Publication number Publication date
EP0505582A4 (en) 1993-03-31
CA2070663C (en) 2002-05-07
TW198708B (ko) 1993-01-21
US5596128A (en) 1997-01-21
DE69121188D1 (de) 1996-09-05
WO1992006935A1 (en) 1992-04-30
KR0185224B1 (ko) 1999-05-15
EP0505582A1 (en) 1992-09-30
EP0505582B1 (en) 1996-07-31
CA2070663A1 (en) 1992-04-13
DE69121188T2 (de) 1997-01-02

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