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KR890003859A - 에너지-유도 경화성 조성물 - Google Patents

에너지-유도 경화성 조성물 Download PDF

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Publication number
KR890003859A
KR890003859A KR1019880010962A KR880010962A KR890003859A KR 890003859 A KR890003859 A KR 890003859A KR 1019880010962 A KR1019880010962 A KR 1019880010962A KR 880010962 A KR880010962 A KR 880010962A KR 890003859 A KR890003859 A KR 890003859A
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composition
ligands
sigma
mixture
polymerizable
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KR1019880010962A
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KR0134784B1 (ko
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안 브라운-웬슬레이 캐더린
제임스 데보 로버트
코시모 팔라조로 마이클
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도날드 밀러 셀
미네소타 마이닝 앤드 매뉴팩츄어링 컴패니
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/46—Polymerisation initiated by wave energy or particle radiation
    • C08F2/48—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light
    • C08F2/50—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light with sensitising agents
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F4/00—Polymerisation catalysts
    • C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
    • C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/161—Catalysts containing two or more components to be covered by at least two of the groups C08G18/166, C08G18/18 or C08G18/22
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/22—Catalysts containing metal compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
    • C08G18/637—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers characterised by the in situ polymerisation of the compounds having carbon-to-carbon double bonds in a reaction mixture of saturated polymers and isocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/68—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the catalysts used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/08—Saturated oxiranes
    • C08G65/10—Saturated oxiranes characterised by the catalysts used
    • C08G65/12—Saturated oxiranes characterised by the catalysts used containing organo-metallic compounds or metal hydrides
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S430/00—Radiation imagery chemistry: process, composition, or product thereof
    • Y10S430/1053—Imaging affecting physical property or radiation sensitive material, or producing nonplanar or printing surface - process, composition, or product: radiation sensitive composition or product or process of making binder containing
    • Y10S430/1055—Radiation sensitive composition or product or process of making
    • Y10S430/114—Initiator containing
    • Y10S430/115—Cationic or anionic
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S430/00—Radiation imagery chemistry: process, composition, or product thereof
    • Y10S430/1053—Imaging affecting physical property or radiation sensitive material, or producing nonplanar or printing surface - process, composition, or product: radiation sensitive composition or product or process of making binder containing
    • Y10S430/1055—Radiation sensitive composition or product or process of making
    • Y10S430/114—Initiator containing
    • Y10S430/122—Sulfur compound containing
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S430/00—Radiation imagery chemistry: process, composition, or product thereof
    • Y10S430/1053—Imaging affecting physical property or radiation sensitive material, or producing nonplanar or printing surface - process, composition, or product: radiation sensitive composition or product or process of making binder containing
    • Y10S430/1055—Radiation sensitive composition or product or process of making
    • Y10S430/114—Initiator containing
    • Y10S430/124—Carbonyl compound containing

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  • Chemical & Material Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Epoxy Resins (AREA)
  • Paints Or Removers (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Polymerisation Methods In General (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

내용 없음

Description

에너지-유도 경화성 조성물
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (12)

1)적어도 하나의 에틸렌-불포화 단량체, 2)적어도 하나의 에폭시 단량체, 및 3) 폴리우레탄전구체, 유기금속 화합물 및 오늄열을 포함하는 경화제 및 용매로 구성되는 그룹으로부터 선택된 중합전구체의 한 부류를 포함하는 것을 특징으로하는중합형 조성물.
제1항에 있어서, 상기 조성물은 광중합성인 것을 특징으로 하는 조성물.
제1항에 있어서, 상기 중합전구체의 부류는 적어도 하나의 에틸렌-불포화 단량체 또는 폴리우레탄 전구체이며, 상기 조성물은 열 중합성인 것을 특징으로 하는 조성물.
제1항에 있어서, 상기 유기금속 화합물이 하기 구조식을 지니는 것을 특징으로하는 조성물.
L1,L2,L3M
상기식에서, L1은 0이거나, 혹은 치환 및 비치환된 아크릴과 사이클 불포화 화합물 및 그룹, 그리고 치환 및 비치환된 카르복실 방향족과 헤테로 사이클 방향족 화합물로 부터 선택된 동일하거나, 다른 리간드의 파이( )전자를 기여하는 1내지 12개의 리간드를 나타내며, 이들 각각은 원자가 껍질 M에 2내지 24개의 파이 전자를 기여할 수 있고, L2는 0이거나, 혹은 모노-,디-,및 트리-덴테이트(dentate)리간드로 부터 선택되는 시그마( )-전자의 짝수를 기여하는 동일하거나, 다른 1내지 24개의 리간드이며, 이들 각각은 원자가 껍질M에 2,4또는 6개의 시그마-전자를 제공하고, L3는 0이거나, 혹은 동일하거나, 다른 1내지 12개의 리간드이며, 이들 각각은 원자가 껍질 M에 한개의 시그마 전자만 제공하고 : 리간드 L1,L2,및 L3는 가교 또는 비-가교리드간 이고, M은 주기표 원소 IVB, VB, VIIB및 VIIIB족으로 부터 선택되는 동일하거나, 다른 1내지 4개의 금속 원자인데 : 이조건부로, 상기 유기금속 화합물은 적어도 하나의 금속-금속 시그마 결합 및 L3를 함유해야하며 및 L1, L2, L3및 M은 안정한 형상을 것을 선택해야 한다.
제1항에 있어서, 상기 오늄염이 하기구조식(II)를 가지는 것을 특징으로하는 조성물.
AX (II)
상기식에서, A는 요오드늄 설포늄 또는 디아조늄 양이온, 및 X는 유기 설포네이트 대이온 또는 할로겐화 금속 또는 준금속대이온이다.
제1항에 있어서, 상기 에틸렌 불포화 단량체가 아크릴레이트, 아크릴아미드 및 비닐 화합물로 구성된 그룹으로 부터 선택되는 것을 특징으로하는 조성물.
제1항에 있어서, 상기 폴리우레탄 전구체가 폴리이소시아네이트 및 적어도 2개의 이소시아네이트-반응 수소원자를 지닌 화합물의 혼합물로 구성되며, 상기 이소시아네이트기 ; 이소시아네이트- 반응수소원자의 비율은 1:2 내지 2:1의 범위인 것을 특징으로하는 조성물.
(a)제1내지 제7항에 따른 중합성 혼합물을 준비하고, 및 (b)상기 혼합물을 퉁합시키거나 또는 상기 혼합물에 에너지를 가해 중합시키는 단계를 포함하는 것을 특징으로 하는 방법.
제1항 내지 7항중 어느 한 항에 따라서 중합성 조성물의 한 표면위에 피복된 기판을 포함하는 것을 특징으로 하는 적층구조물.
제9항에 있어서, 상기 구조물은 영상 구조인 것을 특징으로 하는 적층구조물.
제1항 내지 제7항중 어느 한 항에 따라서 경화되는 것을 특징으로 하는 중합성 조성물.
제11항에 따라서 얻어지는 것을 특징으로하는 성형제품.
※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019880010962A 1987-08-28 1988-08-27 에너지 유도된 경화성 조성물 KR0134784B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US090,791 1987-08-28
US07/090,791 US4952612A (en) 1987-08-28 1987-08-28 Energy-induced curable compositions

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KR890003859A true KR890003859A (ko) 1989-04-18
KR0134784B1 KR0134784B1 (ko) 1998-04-20

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US (1) US4952612A (ko)
EP (1) EP0306161A3 (ko)
JP (1) JPS6470516A (ko)
KR (1) KR0134784B1 (ko)
AU (1) AU610618B2 (ko)
CA (1) CA1335620C (ko)
ZA (1) ZA885645B (ko)

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