KR830000869B1 - Whole Seed Treatment Method for Sorption of Solid Matter - Google Patents

Abstract

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Description

Whole Seed Treatment Method for Sorption of Solid Matter

The present invention relates to a treatment method of all seeds for sorption of solid matter to all seeds.

The present invention can be used to sorb chemicals into granule tissue (berry tissue) prior to changing the nutrients of the seeds or carrying out the accompanying additive method.

In particular, the method can be used to soak the solid material in all seeds to increase the nutritional value of the seeds used for food and feed, and to improve the safety of grain and safety of grain characteristics.

According to the present invention, the whole grains or whole seeds are brought into contact with the mixture until the mixture of the fine solid substance and the oil excipient is sorbed to the seeds so that each component of the mixture is synergistic with respect to the sorption of the whole grains or seeds. A method of treating grain or seeds characterized by the present invention is presented.

As used herein, the term "seed" refers to all grains and legumes, and includes barley, corn, cereals, millet, oats, rice, rye, rye, wheat, soybeans, peanuts and other Includes many edible beans and others in this category. The term “whole seed” refers to a substantially complete seed, whether pretreated or untreated, and includes seeds such as one form or mixed form, variety, hybrid and the like.

The method is particularly applicable to seeds because of their special and specific use. All runs were carried out using seeds containing conventional chaff, broken kernels and other crumbs to account for the effects of chemical formulation without the need for grinding.

The term " sorption " may be used interchangeably with the terms " incorporation " or " encapsulation " including both adsorption or absorption or their meaning. The term "solids" also includes mixtures of solids.

Sorption of the solid material was observed to occur by rapid sorption of both phases in the presence of an oleaginous liquid or semi-solid material. Normally, animal, vegetable and mineral oils, fats and greases are very responsive to seed tissues in small amounts or not at all in seeds, and even in normal conditions with low water content. All solids, except for solid chemicals, are solubilized in seeds in small amounts that are not measurable, or are not largely sorbed.

In the case of aqueous solutions containing soluble chemicals, the absorption site of the seed is loaded or reaction occurs at this site, which prevents more absorption.

Thus, it became clear that the relationship between oil and solids was unexpected.

The method according to the present invention will be described only by the method of practice.

All oils, fats and greases from all raw materials can be used in this method, and from now on these oil compounds will be referred to as "carriers" or "excipients". It consists of a compound. Although no special proposal is made for these compounds, oils, fats and greases having relatively high melting temperatures or higher molecular weights or other suitable arrangements are more effective excipients, but their excipients are so rare that commercially available excipients are relatively It is selected according to price and purpose of use. For example, animal fats containing products with widely varying physical and chemical properties due to their nutritional value and price, factors taking into account the importance of using large volume tonnage, and economics are mainly used and processed grains. In order to use solid chemicals such as borax as synergistic mixtures for the production of oil well drilling adjuncts which are incidentally steamed, inexpensive non-edible oils such as petroleum may be used as oily liquids.

The concept of a mesomorphic state or "liquid crystal" can be at least a partial explanation of the synergistic phenomenon. Solids or excipients do not have the ability to respond to non-equilibrium forces in the seed, but all are transported quickly within the seed, so the behavior of this mixture is quite different from the separate components. Vectors by polar and nonpolar regions of the seed structure This is caused by the metastable state of the seed resulting from the imbalance of the force and by an incidental attempt to reach maximum stability, and the proper phenomenon is in all cases that the two-phase sorption of oil and solids is faster than a single sorption of water. Moreover, due to the size of relatively large solid crystals with very low molecular weight and very large aggregates that are easily sorbed, the size or shape of the solid crystals cannot be explained based on particle size. Are not soluble in fats or oils and some solids are dissolved in small amounts in frequently used solvents. The solubility does not become a factor, nor does it occur as a chemical semi-melt factor, but in the concept of "liquid crystal", the size and shape of the crystals can change, but the characteristics of solid crystals, such as birefringence for polarization, continue to appear.

The weight ratio of solids to excipients varies and is influenced by several factors, but these changes are generally small, so that the particle size, as described above, should have a synergistic effect. In general, the particle size of the solid material used is a size that can pass through the US standard 60 mesh body or through a hole of 250μ, but some types of solid particles have a length of at least 250μ. Each solid has a length of at least 250μ, as well as a special mixture of solids. Each of the solids affects the synergistic ratio of solids to excipients as well as the specific mixture of solids, but usually the ratio of solids to excipients is 1: 1-6: 1 and the usual ratio is 4.5: 1. It is readily apparent that solubility can be removed based on the relatively low content of excipients required in the ratio of solids to excipients.

Generally not limited flexibility of operation has been introduced into the method. The ratio of solids and excipients to be commercially mixed will be known and will depend on the factors described above.

However, if the excipient content is insufficient, most of the solid will be absorbed quickly by the seed, but some of its solid will remain in the seed pericap. Therefore, additional excipients must be added later to achieve the same results as with sufficient excipients. Similarly, if excess excipients were used in the first addition, more solids could be added. In addition, all batches of seeds processed in such a way that the appropriate amount of excipients and solids are mixed must be mixed together.

When the "rise 2-phase" is properly quantitatively balanced, the sorption is complete and no solids or excipients remain around the seeds, so that about 35% of the mixture is sorbed based on the dry weight of the seeds, Even the accompanying grain dust is sorbed, leaving only large crushers such as stems, straw, and stones, known as fm, and other particles that are too large to be sorbed. Therefore, the apparatus used to mix the grain and the mixed components is cleaned cleanly without any trace of added physical phase.

The flexibility, simplicity and high sorption rate of synergistic mixtures are inherent in the industry, providing a method for treating large quantities of seed at extremely low prices. Accurate measuring devices for liquids and solids, mixers and screw conveyors are readily available. Many grain warehouses have such devices installed and can be installed easily and economically. The advantage of these instruments is their critical use in the large-scale food industry, including the processing of legumes and grains for feed and food.

In the process of the present invention, the seed can be treated with a variety of suitable excipients, depending on the desired purpose, and at the same time it can substantially eliminate the risk for grain dust. For example, corn can be treated with corn oil, which sows corn dust, soybeans can be treated with soybean oil. The oil is usually extracted from these seeds and, if necessary, can maintain the purity of the oil obtained from the treated seeds. When using seeds as animal feed, you should choose seeds that have the best balance of nutritional value and economy. In addition to the prevention of dust emissions, seed handles not only retain small amounts of added excipients but may also reduce or collect the amount of dust.

This method is effective for seeds with a wide range of moisture content, so it does not limit any particular moisture content or range of moisture, but for practical use seeds with natural water content are generally used. In some cases, the moisture content may be increased before or after the sorption of the solid material, particularly when solubilizing a large amount of solid material or promoting the accompanying reaction. In the absence of water on the surface of the seeds, seeds containing saturated moisture have been shown to be effective in this method. That is, the attraction of the seed to the synergistic mixture is so strong that water may be rejected from the grains so that the synergistic mixture is sorbed. On the other hand, the sorption of synergistic mixtures with actually carbohydrate seeds was found to occur regardless of the moisture level. Therefore, the obvious way to do anything is to use ordinary physical conditions.

The following specific embodiments are described for clarity.

In each of the examples described, the seeds were weighed and placed in a glass jar, weighed and added to the ingredients of the synergistic mixture, and then the glass jar was sealed with a screw bottle metal lid and shaken. In this way, the sorption of the synergistic mixture can be visually observed. Also, since metal lids and glass bottles do not absorb the mixture, it was obvious that the mixture would be absorbed by seeds. In addition to visually observing and weighing, measurements were made on total nitrogen in three examples. This incidence test is more accurate on analytical methods than on sorption.

In many examples, the treated seeds were randomly selected and cut in the transverse and longitudinal directions. like this

EXAMPLE

Therefore, the uniformity of endosperm can be visually investigated in comparison with the grain structure of the seed before processing the exposed grain structure. The endosperm of the main fodder grain is almost always non-uniform, with some of the endosperm being "corneous" or "vitreous" and the remainder usually white "floury". Thus, increasing the uniformity towards uniformity has been found to increase tissue availability for end use. In some cases, added solids or excipients in the cut seeds cannot be visually observed. For example, large amounts of salts or sorbents of urea tend to conceal the taste of added solids.

In the table describing the examples, all weights were expressed in grams and the percentages were based on the dry weight of the seeds. The numbers in parentheses indicate the order used. The numbers following the excipients used and the water or solids represent the time that has elapsed since the addition immediately prior to the narrowing and in minutes, hours and dates with letters such as "m", "h" and "d". The lower case letters are explained in footnotes and the maximum time observed for extinction is an approximation by visual observation, which is not accurate because it is difficult to observe when seeds are active. The recorded time is usually larger than the actual time of occurrence. The protein content is determined by analyzing the nitrogen content by standard kjeldahl me-thod, multiplying this nitrogen content by a factor of 6.25, and recording the protein or equivalent protein content in the standard method of animal feed industry. have.

Footnotes to the diagram

In the case of using excipients as the first variable, (1)-(9) showed the effect of various excipients. Three excipients, namely animal fat (Example 2), oreomargarine (Example 5), and white jelly (Example 5), and white jelly (Example 7) can be roughly classified as semisolids. . Animal fats from the large-scale livestock raising industry are not uniform products but have had no difficulty in reaching grain. Two carriers, namely, white petroleum jelly, "Vaselind" (Example 7) and mineral oil (extra heavy) (Example 6) are mineral raw materials; Six excipients are obtained from vegetable raw materials, corn oil (Example 1), olive oil (Example 4), peanut oil (Example 8), cocoa butter (Example 9), soybean oil (Examples 57, 58, 59). , 60, 66, 67), cottonseed oil (Example 5) and oreomargarine (Example 5) obtained from corn oil; One excipient is anhydrous nursing (Example 3) obtained from vegetable raw materials as essential oils; Another excipient is animal fat (Example 2) obtained from animal sources.

Two excipients, namely cottonseed oil (Example 64) and soybean oil (Example 66), were not purified and the mineral oil used in Example 68 did not contain a preservative. Anise oil was sorbed before and after addition of the salt (NaCl), and corn oil was added after the salt was mixed with the grains. Sorption occurred rapidly in the presence of all excipients.

Several types of solids that appeared in a wide variety of chemical forms were sorbed as in the examples. Strongly alkaline NaOH is rapidly absorbed into the grains with normal moisture content (Example 10). After cutting the grains, the oil uniformity was significantly improved, and after 15 minutes of enveloping the solid material, the grain sample became dark. This indicates that all of the granules between the various tissues react with alkali and contain water associated with the grain tissue.

Sulfur element (Example 11), i.e. sublimated sulfur of pharmaceutical purity, was easily sorbed, and 1% sucrose (Example 12) was quickly sorbed, followed by infrared heat treatment to uniform the drainage. Improved and gave a scent. Similar results were observed when CaO and glucose were sorbed and treated with infrared heat (Example 59). The uniformity of the drainage was further improved in Example (13) in which the grains were exposed to strong infrared light for a short time after sorption of sodium formate, the reducing agent. The quality of the endosperm was somewhat improved by irradiating calcium oxide on the corn using corn oil as an excipient (Example 14), followed by infrared heat treatment. CaO or Ca (OH) ₂ was used in the cooking of corn to make tortilla flour. The essential amino acid "lysine", which is deficient in most grains for feed, was soaked in grain water using corn oil mixed with the grains in advance, and corn oil was added two times (Example 15). In Example (16), NaCl was encapsulated in grain water, followed by an increase of 20% or more of water, after which the water absorption rate was very similar to that of grains without NaCl.

Very large, complex and dissimilar molecular aggregates were sorbed in grain water using corn oil as excipient. Casein (Example 17), a milk protein, was solubilized within 1 minute, white-white corn starch (Example 18) of 8-15 micron in diameter, very quickly, and montmorillonite-type aluminum silicate clay Phosphorus bentonite (Example 19) also quickly settled in the grain. Such bentonite is commonly used in animal feed because of its inorganic content.

Examples (20) and (21) show the effect of adding various types of solid materials simultaneously with intermittent addition of excipients.

In order to explain the range of sorption in Example 20, phenol red was sorbed to the grains, then several grains were cut to expose a large portion of the endosperm and a few drops of diluted alkaline solution Was dropped in the center of exposed drainage to prevent contact. In this case, the immediate development of pink color indicates the sorption of the dye at the center of the grain structure. In the final step, CaO was sorbed to the grain.

In Example (21), after (NH ₄ ) ₂ SO ₃ · H ₂ O, a strongly reducing NPN compound (nonproteinaceous nitrogen compound), was sorbed to the grain, the urea was sorbed within about 5 hours, and then irradiated with infrared light. Heat treatment increased the uniformity of the drainage.

Other chemicals in aqueous solutions, such as borax (Na ₂ B ₄ O ₇ lOH ₂ O), which are often important in relation to starch availability, are unilaterally sorbed to grain seeds.

In Example (22), borax, which acts as a powerful swelling agent for starch in the presence of water, was rapidly sorbed to the seed of grain sorghum using corn oil as an excipient, and then water was sorbed to the grain at about 25%. Then heated at 65 ° C. for 12 h.

After drying to normal moisture content, the seeds were cut and found to have almost uniform drainage.

Diethylstilbestrol (DES), a synthetic hormone that is frequently used for animal therapy and feed of edible cows, was sorbed to grain water using corn oil as an excipient (Example 23). The amount of sorption affects the fattening of edible cattle, but it has also been clarified that smaller amounts can be formulated. Recently, toxic meats from animals raised by DES have led to debate between government regulators and cattle breeders. However, it is not the purpose of the present invention to describe the effects on particular feed additives such as pharmaceuticals or anything else. The present invention relates to a method for soaking a solid material into the seed within the limits of the public regulations in order to produce a desirable feed and other materials for various purposes.

Chloral hydrate, a reactant used experimentally to produce modified starch products and reported as a methane production inhibitor in ruminant feed, was so rapidly sorbed to grain water using corn oil as an excipient (examined). Example 24) At this time, the ratio of the reactor to the reactants was formulated to be suitable for secondary treatment.

Yeast cells (saccharomyces cerevisiae), a live, dried, single-food cell, were rapidly formulated into cornmeal using corn oil as a carrier (Example 25), and then water was added, followed by 12 hours at 37 ° C. Incubation during this time results in an integral amount of gas in the amount of useful sugar present in the normal grains, which can be made more obvious by simultaneously combining yeast products, suitable enzymes, or both.

Example (26) describes the easy blending of vitamin-inorganic mixtures into cereal water, although somewhat exceeding in content, and in other examples vitamin mixtures containing different solids may be used for different types of excipients. It was explained using the envelope.

In Example (27), household meat tenderizer containing papain, a protease obtained from seasonings and papaya fruit, was enclosed in grains using corn oil as an excipient, and then the moisture content of the treated grains was 25%. Heat was increased for 24 hours at 65 ° C. (the optimum temperature for papain to be active) after the increase. It can be seen that the uniformity of the endosperm was increased in the cut grains after treatment as described above, and the uniformity of the endosperm was also increased in the grains cut after drying and cooling.

By removing the inhibitory portion of the protein matrix, it can be seen that the degradation of the protein matrix can increase the availability of starch. Nutritionists have calculated the availability of starch and protein by 60-80% according to animal and compression methods, and multiplying this percentage by the total volume of grains used for animal feed is an economically important increase. You can see that.

In Example (28) Gibbrel, a commercial product containing 1.65% potassium gibberate and the remainder of the unknown filler, was sorbed to the grain water samples using corn oil as the carrier. These plant metabolites are known to promote seed germination under moderate germination conditions.

Examples (29)-(38) and (57) illustrate the effectiveness of enveloping excess chemicals in seeds, which contain products containing concentrated chemicals for feed and various other treatments. Required for the manufacture of In general, grains containing relatively large amounts of solids and carriers do not increase in volume but increase in density in proportion to the content of the additives.

Contrary to the consequences of water sorption, the increase in density indicates high sorption in the unusable areas of the seed and proves equal sorption in all seed tissues due to the inability of large sorption at the skin and embryo.

In Examples (29), (30) and (31), a method of soaking 15% calcium oxide (CaO) in the grain was described. Among the many calcium oxide compounds, lime is a representative compound and only a very small amount is dissolved in water (0.2% or less). In both examples, in example (29) a special weight mineral oil was used as the carrier and in example (30) whole amounts of CaO were added all at once to the mixture of grain-excipients.

In Example 31, 1.3 or 1.4 g of CaO and corn oil and an increase of 0.3 and 0.4 g, respectively, were alternately added to the grains. In contrast, the change of the ratio between the solid and the carrier is not important, but the effect of the excipient is somewhat increased.

Examples (32), (33) and (58) illustrate the ability to sorb large quantities of urea, thus providing a new, simple and economical way to produce products with high equivalent protein values for feed of ruminants. have. Condensation of urea and grain aggregates can be carried out in an old way or economically, and in the prior art, it has not been possible to provide a method for encapsulating chemicals in all seeds while maintaining the original state of the seed.

In Example (32), 15% of the urea was soaked in the seed using this method, and the resulting product was analyzed to have 39.68% total equivalent protein and 11.1% final moisture content. It can be expected that the added urea will condense to some extent with the granulation at room temperature. In large quantities, the range of condensation is increased by applying heat as is normally used in the manufacture of compound feed for ruminants, and steam flaking or "micronizing" method immediately after infrared heating. The condensation observed in the rolling process), together with the envelope in the grain itself, suppresses the rate of separation of chemicals, further increasing the utilization of residual nutrients.

In Example (33), after increasing the water content of the grain to 20.5%, corn oil divided by 0.2 g and 0.3 g and urea incremented by 1.5 g were alternately added at regular intervals, followed by analysis of the protein. Was 58.96% by weight of total solids, containing 15.95% water, and 70.15% of equivalent protein by dry weight. The equivalent protein in this Example (33) is higher than the concentrate of the oilseed protein and this example also clearly shows the flexibility of the method.

Examples (34) and (35) illustrate the rapid addition of glucose (Example 34) and sucrose (Example 35) suitable as energy sources readily available for food or feed, and using microorganisms such as yeast cells. Explain that you can.

In Example (36), NH ₄ H ₂ PO ₄ , which is commonly used as a source of NPN and phosphorus, was formulated into grain water using corn oil as an excipient, with 3.75% of excipients and 15.0% of solids in a dry weight ratio of 60 seconds. It was formulated within and most of the two-phase system disappeared within 15 seconds after addition of the solids.

Based on total solids and final moisture content, the total equivalent protein content was determined to be 17.53% and the phosphorus content was calculated to be 3.02%.

At dry dry ratios of grains, 15% of sodium chloride (Example 37) sorbed to grain water, which greatly exceeded the amount that could be sorbed to the skin layer from an aqueous solution of any concentration, and consequently sorbed water very quickly. The sorption of water is then slightly suppressed in the presence of large amounts of synergistic two-phase systems, but is further supported by the sorption action of nonpolar sites.

Example (38) illustrates the ease of sorbing trace mineral concentrates into grain water using corn oil as an excipient, with about 15% of the amount used being about 300 of the trace minerals required for ruminants in the blended feed. Represents a pear.

In Example (39), sufficient amounts of urea and corn oil were absorbed by corn seed to increase the total equivalent protein level varying from 10.5-12% depending on the age of the animal to about 11%, the average value of cattle feed. .

In Examples (40) and (41), dried northern beans, mainly called "gangnam beans," were used, and 0.4 g of calcium oxide was enveloped in soybeans using corn oil as a carrier. Thereafter, in Example 40, the beans were cooked by conventional boiling, and the cooking time was compared with the untreated beans, and these beans were found to be harder and more digestible.

In Example (41), the same treatment as in Example (40) was used to shorten the cooking time, except for 30 seconds of infrared heat treatment after the chemical treatment, and these beans were found to be harder and more digestible. .

Very similar results were observed when the dried stained pinto bean (Example 42) was treated with CaO and corn oil and then heated in infrared. The beans were retained in shape and desirable firmness, had a short cooking time and were better digested compared to untreated stained Gangnam beans.

Example (43) shows the efficacy of blending the necessary nutrients deficient in grains in the whole seedlings to produce a complete feed for edible cows. .

In Example 44, 2% NaCl was blended into the seed structure of raw peanut using corn oil as an excipient.

Examples (45)-(53) illustrate the efficacy of enveloping large quantities of various solids in different types of seeds, including barley, corn, whole grain maize, oats, rice, rye, rye wheat, wheat, and soybeans. will be. In this example, animal fat was used as an excipient because of its practicality and economic feasibility, and the composition of the solid additive was the same, and the water content in each embodiment was adjusted to the same level (14%), but the sorption time of the ascending mixture of animal fat and the solid substance Was varied from several seconds to 30 seconds according to each embodiment.

Given the low-protein grains of corn and sorghum, ruminants do not normally need these nutrients because they have the ability to synthesize B-vitamins or vitamin E, but for all concentrated cattle feeds. Necessary nutrients turned out.

These products are manufactured by adding nutrients deficient by cattle breeders or as required. In addition, there is an advantage, including the uniformity of the feed components that can not be separated by forming a complete NPN secretion and layering for animal feed.

Examples (54) and (55) illustrate the benefits of sorption of chemicals suitable for added steam treatment. In Example (54), 1.4 g of Na ₂ SO ₃ (equivalent to 0.395% of sulfur dioxide) was encapsulated in grain water according to the methods of US Pat. Nos. 3,725,081 and 3,911,147 prior to sorption of sulfur dioxide. It is an object to sorb chemical reducing agents to polar and nonpolar sites. Then, steamed at 150 psig for 4 minutes, dried and milled. 77.23% of this product was dissolved in cold water and showed improvement compared to the same treated grains except that Na ₂ SO ₃ and oil were not enclosed.

In Example (55), 1% calcium formate and 0.28% mineral oil excipients were soaked in grain water and then steamed at 150 psig for 4 minutes. As a result, 71.28% of the product is dissolved in cold water and has excellent adhesive properties such as feed pellet binder, wall plate adhesive, and charcoal briquuette adhesive.

In Example (56), 0.4 g of corn oil and 2 g of urea were sorbed simultaneously to cooked grains to illustrate the benefits of combining solids with pretreated seed, ie, gelatinized corn. This sorption shows that even if gelatinized, the internal vector force causing the absorption of the synergistic mixture remains as it is, and as expected, most of the internal primary vector forces are destroyed to denature the examples (54) and ( The samples in 55 did not sorb the synergistic mixture.

Examples (60)-(69) clearly show an example of the present disease in which various kinds of seed dusts are sorbed using various types of suitable oil excipients. The examples listed above were selected from a variety of experimental examples including commodity seeds, dust and dust mixtures from various types of seeds and oily excipients and mixtures of such excipients. In most cases, dust (passing 60 mesh bodies, the American standard) was filtered out of the grains and then added again to ensure a known amount of dust. In all cases, "dust" actually contains a significant amount of particles of less than 37μ. In all the examples described the content of added dust was found to be actually greater than the amount normally found in seed foods (the amount which causes serious problems as the amount of dust obtained in normal handling).

Example (60) illustrates the effect of treatment under extremely unsuitable conditions. 3% of the dust (2.66% based on the grain weight present in that state) is 15-50 times more than what is normally found below, depending on the type of raw material and the age and condition of the grain.

In this example, the sample treated with the ratio of solid matter (dust) to excipient in the ascending mixing door is 3: 1 was milled with flour and baked in an independent laboratory. Absorption of treated wheat (tempering), mill extraction (grain yield) and most baking properties (bread volume and bread particles and structure) are associated with untreated wheat ("control"). Compared to normal, high content of synergistic mixture was sorbed in the grain oil, which adversely affected the color, ash content and odor of flour, and the odor caused by dust.

In Example (61), after mixing with 1/3 of the total amount of dust added with wheat, fine grain dust and excipient were mixed well so that the two-phase mixture of the synergistic mixture was quickly sorbed at the same time. Assuming that new dust was produced by the addition treatment, 1/3 of the dust was mixed with wheat seeds, and the remaining 1/3 of the dust was mixed with the grain for the same reason.

The total amount of added dust is about three times the amount normally obtained, and in each case the large glass bottle was shaken so that the absorption of dust occurred quickly. The atmosphere of the vial was very cloudy and opaque before the addition of mineral oil excipients, but no dust was visible after all of the synergistic mixture had been added. The normal product was obtained when the flour obtained by milling the wheat was compared with the untreated grain.

In Example (62), the mill was specially carburized to have a water content of 1.49% to demonstrate that the treatment efficiency was independent of the water content of the grain. The sorption rate of two-phase corn oil and wheat dust was not higher than that of wheat with normal moisture content.

Before adding the excipient corn oil, grain water dust (1/2 of the whole) was mixed with grain water (Example 63) and the residual amount was mixed after the ascending mixture was sorbed. Since the excipients were predispersed, the sorption proceeded very quickly.

In Example (64) wheat dust was used with raw grain water and crude cottonseed oil to illustrate the incompatibility of the particular dust raw material with any particular type of seed. Grain grinders are usually treated not only as dusty mixtures but also as seed mixtures of some kind.

In Example 65, a synergistic mixture of corn dust and corn was used with corn, which is suitable when the intended use also includes the production of corn oil. When preparing animal feeds using large quantities of corn, an oily excipient such as soybean oil, which is not refined in Example 66, may be suitably used.

Virtually all soy is treated with two primary products: soy foods and soybean oil. As shown in Example (67), the soybean dust was mixed with soybean and then mixed with unrefined soybean oil to allow the synergistic mixture to be rapidly absorbed, and then the soybean dust was added twice in the same amount and mixed with the soybean. Atmospheric dust was not observed. Although the content of oil excipients added by such experiments is very small in most cases, soybean suppliers and processors can protect the purity of oil products as needed.

After mixing with one-third of all the rice dust added (Example 68), all the food grade mineral oils were mixed, and the two-phase quickly soaked in the rice. As a result of the addition of the same amount of the remaining dust twice, assuming that new dust has formed, as in the above-described examples, all the dust additives sorption very quickly as shown in the table of the examples.

Animal fat at 65 ° C. was used as an excipient for the mixture of barley seed and barley dust in Example (69), and the sorption rate and efficiency of the synergistic mixture were similar to those in the other examples.

All of the oily excipients described herein can work with seed dust or other solid materials as described.

In general, the ratio of solids (dust) to oil excipients required to sorb all of the synergistic mixture at the same time is about 3: 1 to 4.5: 1, but smaller when using less excipients than necessary for the total sorption of the two-phase Dust control occurs by selective sorption of the particles. Since larger particles do not cause explosive conditions, it is found that the treatment effect is excellent when treated at a ratio of 6: 1-10: 1 in the practical use of the method. The amount of dust is very small compared to the weight of the grain, so the amount of excipients used is very small.

In order to control the dust dust, it is appropriate to use, for example, 250-500 p.pm (0.025-0.050% of the dry grain weight) excipients. However, when mixed with untreated grain, very small amounts of excipients are used to sorb the dust, an additional excipient must be supplied to the grain.

By the present invention, which finds that the synergistic mixture of the solid material and the oil excipient is sorbed to the whole seed, it is clearly demonstrated by the above-described description and the example that a new treatment method is provided. The present method provides a method for sorbing large amounts of solids in virtually unlimited formulations, giving nearly similar component efficacy of seed tissues and also preventing degradation into their original components. Also in selected embodiments, half of the reaction to the dye, the sorption after the reaction, and the subsequent addition process involves the total structure of all seed tissues in the sorption adhering of the synergistic mixture, such as by the high content of sorbed solids, baking tests, etc. I found out. He also explained that the sorption of solids with varying chemical compositions and physical arrangements has the effect of increasing the nutritional value of all seeds.

The present invention provides a method that omits the use of many seeds that depend on seed grinding, a method that can use the natural seed structure in the present and future grain sale process as well as various seed products containing a more nutritious energy source. Provides a way to manufacture In addition, a quick and accurate example of this method provides seed treatment with reactive chemicals, catalysts, live cells (yeasts), etc., at a very low cost, by further treatment and furthermore, for the production of complete non-invertebrate blends. It provides a method for sorption of solid matter in tissues. It also absorbs dust, eliminates the explosion hazard of grain depots, reduces the risk of fire, and provides a very effective and economical way to significantly improve the ambient conditions for handlers and the general public. Therefore, those skilled in the art will immediately know that all products by the method of the present invention have been enhanced in properties by concomitant use or treatment.

Claims (1)

The solids and oil-based excipients that pass through the US60 mesh sieve are mixed in a weight ratio of 1: 1-9: 1 to form a mixture in which the components are synergistic against sorption of whole grains or seeds, and then the mixtures are whole grains. A method of treatment of seed seed for sorbing a solid material, characterized in that the mixture components are sorbed to whole grains or seed seeds by contacting the granules or seed seeds.