KR20160140291A - Functional Jeotkal, Salted and Fermented Seafood, and its manufacturing method - Google Patents
Functional Jeotkal, Salted and Fermented Seafood, and its manufacturing method Download PDFInfo
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- KR20160140291A KR20160140291A KR1020150085472A KR20150085472A KR20160140291A KR 20160140291 A KR20160140291 A KR 20160140291A KR 1020150085472 A KR1020150085472 A KR 1020150085472A KR 20150085472 A KR20150085472 A KR 20150085472A KR 20160140291 A KR20160140291 A KR 20160140291A
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
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- Chemical & Material Sciences (AREA)
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- Meat, Egg Or Seafood Products (AREA)
Abstract
본 발명은 인체에 유해한 나트륨성분의 소금의 사용을 줄이고, 나트륨의 함량이 현저히 적고 항균효능이 있는 붉나무 추출물을 소금 대신 투입하여 젓갈을 제조함으로써 저염 젓갈로서 보존 효력이 향상된 기능성 젓갈 및 그 제조방법을 제공하기 위한 것으로, 젓갈용 생선을 선별하고 5%~20% 소금물에 세척하여 물기를 빼는 제1단계; 상기 세척된 생선을 붉나무 추출액에 침지하여 가염하는 제2단계; 상기 가염된 생선을 건져내 물기를 제거한 후 숙성하는 제3단계; 및 상기 숙성 후 양념으로 조미하여 원적외선으로 살균시켜 포장하는 것을 특징으로 하는 기능성 젓갈의 제조방법에 의해 달성될 수 있다.
본 발명에 따른 기능성 젓갈의 제조방법에 의하면, 다량의 소금 대신 나트륨 함량이 적고 항균효능이 있는 붉나무 추출물에 젓갈 원료를 침지하고 가염하여 젓갈을 제조하므로 나트륨의 함량을 낮출 수 있고, 보존기간이 향상되어 젓갈의 유통기간이 늘어나는 효과가 있다. The present invention relates to a functional fermented seafood having reduced preservation efficacy as low salt fermented seafood by reducing the use of salt of sodium component which is harmful to human body and producing seaweed by substituting salt of rattan extract having antimicrobial effect with a significantly lower sodium content. The first step is to select the fish for the fermented fish and to remove the water by washing the fish with 5% to 20% salt water. A second step of immersing the washed fish in an extract of rhusi mushroom to be salt; A third step of extracting the above-mentioned fish from which the salt has been removed to remove water and then aging; And seasoning with the seasoning after the aging, sterilized by far-infrared rays, and packaged.
According to the present invention, there is provided a fermented fermented seaweed extract according to the present invention, which has a low sodium content and low antioxidant activity, and is capable of lowering the sodium content and improving the preservation period And the shelf life of the fermented fish is increased.
Description
본 발명은 기능성 젓갈 및 그 제조방법에 관한 것으로, 더욱 상세하게는 붉나무 추출물을 사용하여 보존성을 향상시킨 젓갈 및 그 제조방법에 관한 것이다. The present invention relates to a fermented salted fish and a method of preparing the same, and more particularly to a fermented salted fish having improved preservability by using a rattan extract.
젓갈은 발효 과정 중에 생성된 유리 아미노산이나 저분자 펩타이드와 각종 방향성 성분에 의해 특유의 감칠 맛과 풍미를 지니고 있으므로 쌀을 주식으로 하는 우리 나라 사람들의 기호도에 적합한 부식이자 단백질, 지방, 무기질의 공급원으로서 국민 영양상 중요한 위치를 차지하고 있다. 한편, 현대인의 건강에 대한 관심이 증대되고 고염도의 식품이 인체에 유해할 수 있다는 각종 연구 결과가 발표됨에 따라 종래의 식염농도 15~20%의 고염 젓갈은 7~10%의 저염 젓갈로 변모하고 있다. Since the fermented seafood has distinctive flavor and flavor due to the free amino acids and low molecular peptides produced by the fermentation process and various aromatic components, it is a corrosion source suitable for the preference of the people of Korea and it is a source of protein, It occupies an important nutritional position. On the other hand, according to the results of various researches that the interest of modern people on health is increased and that highly salted foods may be harmful to the human body, the conventional salted salted fish having a salt concentration of 15 ~ 20% is changed into salted fish salted with 7 ~ 10% .
젓갈은 새우, 멸치, 오징어젓 등 대중적인 수산어류가 많이 이용되었고, 창란젓, 멍게젓, 명란젓 등 기호성이 강한 젓갈제품은 부분적으로 사용되고 있다. 젓갈, 양념젓갈, 액젓, 조미액젓, 식해류 등 5종류로 분류되는데 젓갈은 수분함량이 높고 살균이 어려워 변질 문제가 있다. 더욱이 종래 식염만을 단순 침장원으로 사용한 젓갈제품에서 기호성과 편이성을 부여하기 위해 고춧가루, 마늘, 조미료를 넣은 양념젓갈 형태가 늘어나고 있다. 그러나 이러한 향신료에는 미생물의 초기 오염이 많아 젓갈 고유의 자기분해효소와 미생물의 작용과 더불어 최종제품의 지속적인 가수분해가 일어나 품질이 불안정하고 보존성이 낮아진다. 그리고 유통과정도 다양화됨에 따라 유통과정에서 변질로 인하여 반품되는 제품도 상당하여 막대한 경제적 손실이 있다. 따라서 젓갈제품에 적용 시킬 수 있는 천연 보존료의 개발이 시급하다. Salted fish, such as shrimp, anchovy, and squid, have been popularly used. Salted fish products, such as Shanxiang, Swordfish, and Mandarin, have been partially used. It is classified into five kinds such as salted fish, salted fish, salted fish, salted fish, salted fish, salted fish, salted fish, salted fish, Furthermore, in order to give palatability and ease of use to the fermented seafood product, which is conventionally used only as a simple sink, there is an increase in the form of seasoned seafood containing red pepper powder, garlic, and seasonings. However, since the initial contamination of microorganisms is high in these spices, the hydrolysis of the final product occurs due to the action of the enzymes and microorganisms inherent to salted fish, resulting in unstable quality and low preservability. Also, as the distribution process is diversified, the products that are returned due to the deterioration in the distribution process are also considerable, resulting in huge economic losses. Therefore, it is urgent to develop a natural preservative that can be applied to the seafood product.
본 발명은 상기한 바와 같은 종래 기술의 문제점을 해결하기 위한 것으로, 인체에 유해한 나트륨성분의 소금의 사용을 줄이고, 나트륨의 함량이 현저히 적고 항균효능이 있는 붉나무 추출물을 소금 대신 투입하여 젓갈을 제조함으로써 저염 젓갈로서 보존 효력이 향상된 기능성 젓갈 및 그 제조방법을 제공하는데 그 목적이 있다. Disclosure of Invention Technical Problem [8] Accordingly, the present invention has been made to solve the above problems occurring in the prior art, and it is an object of the present invention to reduce the use of salt of sodium component harmful to the human body, And a method for producing the same.
상기 목적을 달성하기 위하여 본 발명은 젓갈용 생선을 선별하고 5%~20% 소금물에 세척하여 물기를 빼는 제1단계; 상기 세척된 생선을 붉나무 추출액에 침지하여 가염하는 제2단계; 상기 가염된 생선을 건져내 물기를 제거한 후 숙성하는 제3단계; 및 상기 숙성 후 양념으로 조미하여 원적외선으로 살균시켜 포장하는 것을 특징으로 하는 기능성 젓갈의 제조방법에 의해 달성될 수 있다.In order to accomplish the above object, the present invention provides a method for removing seaweed, comprising the steps of: selecting fish for salted fish; washing the salted fish with 5% to 20% brine; A second step of immersing the washed fish in an extract of rhusi mushroom to be salt; A third step of extracting the above-mentioned fish from which the salt has been removed to remove water and then aging; And seasoning with the seasoning after the aging, sterilized by far-infrared rays, and packaged.
상기 제2단계의 붉나무 추출액에 침지하는 단계에 앞서 원료 생선의 총 중량 100 중량부 대비 8~20 중량부의 소금을 혼입하여 가염하는 단계를 추가로 포함하여 구성될 수 있다.The method may further include adding salt of 8 to 20 parts by weight to the total weight of the raw fish in advance of the step of immersing the fish extract in the second step.
상기 붉나무 추출물은 붉나무의 열매, 잎, 가지, 줄기, 뿌리로 이루어진 그룹에서 일 이상 선택된 재료 100 중량부 대비 용매 30~50 중량부를 첨가하여 분쇄하고 부유물을 제거하여 추출하는 것을 특징으로 한다.The rhusi extract is pulverized by adding 30 to 50 parts by weight of a solvent to 100 parts by weight of a material selected from the group consisting of fruit, leaves, branches, stems and roots of rhusi than one or more selected materials.
또한, 상기 붉나무 추출물은 붉나무의 열매, 잎, 가지, 줄기, 뿌리로 이루어진 그룹에서 일 이상 선택된 붉나무 재료 100 중량부 대비 용매 50~500중량부를 첨가하여 진탕 추출하여 여과하는 것을 특징으로 한다. In addition, the rattan extract may be obtained by adding 50 to 500 parts by weight of a solvent to 100 parts by weight of rhusi fruit material selected from the group consisting of fruit, leaves, branches, stems and roots of one or more ruminants.
또한, 제1단계에 의한 세척된 젓갈용 생선을 마이크로웨이브를 조사하여 살균하는 단계를 추가로 포함하는 것을 특징으로 한다.The method may further include the step of sterilizing the washed fish for the fermented fish by the first step by irradiating microwaves.
이에 더하여, 본 발명은 상기 제조방법에 의해 제조되는 기능성 젓갈에 의해 달성될 수 있다.
In addition, the present invention can be achieved by a functional fermented fish produced by the above-mentioned production method.
본 발명에 따른 기능성 젓갈의 제조방법에 의하면, 다량의 소금 대신 나트륨 함량이 적고 항균효능이 있는 붉나무 추출물에 젓갈 원료를 침지하고 가염하여 젓갈을 제조하므로 나트륨의 함량을 낮출 수 있고, 보존기간이 향상되어 젓갈의 유통기간이 늘어나는 효과가 있다. According to the present invention, there is provided a fermented fermented seaweed extract according to the present invention, which has a low sodium content instead of a large amount of salt, and which is capable of lowering the sodium content and improving the preservation period And the shelf life of the fermented fish is increased.
또한, 마이크로웨이브 조사방식으로 원료를 살균함으로써 위생적이고 보존기간이 향상된다.
In addition, by sterilizing the raw material by a microwave irradiation method, it is hygienic and the preservation period is improved.
도 1은 본 발명에 따른 젓갈 제조공정을 나타낸 흐름도이다.
도 2는 본 발명의 다른 일 실시예에 따른 젓갈 제조공정을 나타낸 흐름도이다.1 is a flowchart illustrating a process for manufacturing a salted pickled fish according to the present invention.
FIG. 2 is a flowchart illustrating a process of manufacturing a salted pickle according to another embodiment of the present invention.
이하, 첨부된 도면을 참조하여 본 발명을 보다 상세히 설명한다.Hereinafter, the present invention will be described in more detail with reference to the accompanying drawings.
첨부된 도면은 본 발명의 예시적인 실시예를 보인 것으로, 이는 본 발명을 보다 상세히 설명하기 위하여 제공되는 것일 뿐, 이에 의해 본 발명의 기술적 범위가 한정되는 것은 아니다. BRIEF DESCRIPTION OF THE DRAWINGS The accompanying drawings, which are included to provide a further understanding of the invention and are incorporated in and constitute a part of this application, illustrate embodiments of the invention and, together with the description, serve to explain the principles of the invention.
도 1은 본 발명에 따른 젓갈 제조공정을 나타낸 흐름도이고 도 2는 본 발명의 다른 일 실시예에 따른 젓갈 제조공정을 나타낸 흐름도이다.FIG. 1 is a flow chart illustrating a process of manufacturing a salted fish according to the present invention, and FIG. 2 is a flowchart illustrating a process of manufacturing salted fish according to another embodiment of the present invention.
도 1에 도시된 바와 같이, 본 발명에 따른 젓갈의 제조공정은, 젓갈용 생선을 선별하고 5%~20% 소금물에 세척하여 물기를 빼는 제1단계; 상기 세척된 생선을 붉나무 추출액에 침지하여 가염하는 제2단계; 상기 가염된 생선을 건져내 물기를 제거한 후 숙성하는 제3단계; 및 상기 숙성 후 양념으로 조미하여 원적외선으로 살균시켜 포장하는 제4단계를 포함하여 이루어진다.As shown in FIG. 1, the process for manufacturing the fermented fish meal according to the present invention comprises: a first step of selecting fish for fermentation, washing the fermented fish with 5% to 20% brine to remove water; A second step of immersing the washed fish in an extract of rhusi mushroom to be salt; A third step of extracting the above-mentioned fish from which the salt has been removed to remove water and then aging; And a fourth step of sterilizing and sterilizing with the far-infrared rays seasoned with the seasoning after the aging.
이하, 각 단계를 상세하게 설명하면 다음과 같다.
Each step will be described in detail as follows.
1단계(S1)Step 1 (S1)
젓갈용 생선은 정어리, 새우, 멸치, 오징어, 조기, 멍게, 골뚜기 등 다양하고 비교적 생산량이 많은 대중적인 수산어류 및 기호성이 강한 수산어류가 사용되어지고 있다. 이들 원료 생선은 선별하고 5% ~ 20% 소금물에 세척하여 협잡물이나 세균, 오염원 등을 제거한다. 소금물에 담았다가 꺼내는 과정은 수회 반복할 수 있다. Fishes for salted fish have been used in a variety of popular fish species such as sardines, shrimps, anchovies, squid, early, urchins, These raw fish are selected and washed with 5% to 20% salt water to remove contaminants, bacteria and pollutants. The process of putting in salt water and taking out can be repeated several times.
상기 1단계(S1)에 의해 세척된 젓갈용 생선은 마이크로웨이브 조사방식으로 원료를 살균하는 단계를 추가로 포함한다. 세척된 원료는 컨베이어 인라인자동화기기를 통해 이동하여 마이크로웨이브살균기로 이동하고, 마이크로웨이브가 원료에 조사된다. 마이크로웨이브 살균기는 대장균을 비롯한 유해세균을 살균하는 효과가 있고, 자외선 방식 살균기는 살균효과를 높이려면 온도를 높여야 하는데, 그럴 경우 식품 변색이 일어나거나 타버리는 부작용이 있는데 자외선 살균기와 달리 마이크로웨이브로 연속 저온 살균하기 때문에 천연색상을 그대로 유지할 수 있는 장점이 있다. 마이크로파 발생장치, 플라즈마 램프, 도파관, 수납실, 마이크로 파 차단망으로 이루어진 마이크로웨이브살균장치를 이용하여 살균한다. 특히 마이크로 파 발생장치는 마그네트론, 클라이스트론과 같은 여러 가지 마이크로 파 발생장치 중 선택되는 것으로, 컨베이어에 직접 조사하게 되며, 쌓여있는 경우는 마이크로파의 침투력이 높은 주파수를 갖는 마그네트론을 사용하는 것이 바람직하다.
The fish for the fermented fish washed by the first step (S1) further includes a step of sterilizing the raw material by the microwave irradiation method. The washed material is transferred through a conveyor inline automation machine to the microwave sterilizer, and the microwave is irradiated to the raw material. Microwave sterilizer has the effect of sterilizing harmful bacteria including E. coli, and ultraviolet sterilizer has to raise the temperature to increase the sterilization effect. In this case, there is a side effect that food coloring occurs or burns. Unlike ultraviolet sterilizer, Because it is sterilized at low temperatures, it has the advantage of preserving natural color. Sterilization is carried out by using a microwave sterilizer composed of a microwave generator, a plasma lamp, a waveguide, a storage chamber and a microwave screening net. In particular, the microwave generator is selected from various microwave generators such as a magnetron and a klystron, and is directly irradiated onto the conveyor. When the microwave generator is piled up, it is preferable to use a magnetron having a high permeability of microwaves.
2단계(S2) Step S2 (S2)
다음으로, 세척된 생선은 붉나무 추출액에 침지하여 가염한다.Next, the washed fish is immersed in the rusks extract to be converted.
상기 붉나무 추출액은 붉나무에서 채취한 줄기, 잎줄기, 잎, 열매, 뿌리로 이루어진 그룹에서 선택된 일 이상의 원료에서 붉나무추출액을 제조한다.The rhusi extract extracts rhusi extract from one or more raw materials selected from the group consisting of stem, leaf stem, leaf, fruit, and root collected from rhusi.
붉나무(Rhus Javanica Linne)는 무환자나무목 옻나무과의 납역관목으로, 뿔나무 또는 염부목이라고도 한다. 붉나무는 옻나무에 속하지만 옻나무와 달리 독성이 없다. 굵은 가지는 드문드문 나오며 작은 가지에는 노란빛을 띤 갈색 털이 있다. 잎은 어긋나고 7 내지 13개의 작은 잎으로 된 깃꼴겹잎이며, 작은 잎은 달걀모양으로 굵은 톱니가 있고 뒷면에는 갈색 털이 있다. 꽃은 노란빛을 띈 흰색이며 꽃이삭에 털이 있다. 열매는 기울어진 공모양의 편구형 핵과(droupe)로 노란빛을 띤 붉은색이며 열매의 겉에는 흰색의 물질이 소금처럼 생긴다. 열매가 익을 무렵에 하얗게 달라붙어 있는 가루가 시면서도 짠맛이 난다. Rhus Javanica Linne is also known as a hornblende tree or a rhododendron tree. Rhusme belongs to a lacquer tree, but unlike a lacquer tree, it is not toxic. The thick branches are sparse and the small branches have yellowish brown hairs. Leaves are alternate phyllotaxis of 7-13 small leaves. Small leaf is ovate with coarse sawtooth and brown hairs on the back. The flower is white with yellowish color and the flower has hair on the ears. The fruit is an oblique ball shaped droupe with a reddish yellowish color and a white substance on the surface of the fruit like salt. When the fruit is ripe, the powder which is attached to white is salty, but it is salty.
본 발명에서 사용되는 붉나무는 줄기, 잎줄기, 잎, 열매, 뿌리 가운데 일 이상을 선택하여 사용한다. 열매의 겉에 생긴 흰색 물질이 짠맛을 내므로 나트륨함량은 낮으면서 소금의 짠맛을 부여하기 위해서 열매를 사용하는 것이 효과적이다. 그러나 열매는 수확기간과 수확량이 한정되어 있어 붉나무의 줄기, 잎줄기, 잎, 뿌리를 사용하여 붉나무 유효성분을 추출한다. 붉나무의 줄기, 잎줄기, 잎, 뿌리, 열매에서 붉나무 유효성분 추출이 가능하다. The rhusin used in the present invention may be selected from among stem, leaf stem, leaf, fruit and root. Since the white matter on the surface of the fruit gives a salty taste, it is effective to use the fruit to give the salty taste of the salt while the sodium content is low. However, the fruit is limited in harvesting time and yield, and extracts the active ingredient of rhus chinensis by using stem, leaf stem, leaf, and root of rhusm. It is possible to extract active ingredient of rhusjon from stem, leaf stem, leaf, root, and fruit of rhusm.
이들 붉나무 원료는 채취하여 유효성분 추출에 바로 사용할 수 있으나 건조하여 수분을 제거하고 추출하는 것이 붉나무의 유효성분 추출효율이 높았다.
These rusk materials can be used directly for extracting the active ingredient, but dry extraction of water removes active ingredients of rhusin.
본 발명의 붉나무추출액은 식물 추출물의 제조방법에 따라 제조될 수 있으며, 구체적으로는 냉침추출법, 온침추출법, 용매추출법 또는 열수추출법 등의 방법으로 추출하며 추출기기는 초음파분쇄 추출기, 열수추출기기, 분획기 등의 기기를 이용한다. 추출한 추출물은 이후, 헥산, 메틸렌클로라이드, 아세톤, 에틸아세테이트, 에틸에테르, 클로로포름, 물 및 이들의 혼합물로 이루어진 군으로부터 선택된 용매로 분획과정을 더욱 실시할 수 있다. 상기 제조된 추출물 또는 상기 분획과정을 수행하여 수득한 분획물은 이후 여과하거나 농축 또는 건조과정을 수행하여 용매를 제거할 수 있으며, 여과, 농축 및 건조를 모두 수행할 수 있다. 구체적으로 상기 여과는 여과지를 이용하거나 감압여과기를 이용할 수 있으며, 상기 농축은 감압 농축기, 일예로 회전 증발기를 이용하여 감압 농축할 수 있으며, 상기 건조는 일예로 동결건조법으로 수행할 수 있다. The extract of the present invention may be prepared by a method of producing a plant extract, and specifically extracting the extract by a method such as a cold extraction method, a warm extraction method, a solvent extraction method or a hot water extraction method, and the extraction apparatus may be an ultrasonic pulverizing extractor, Equipment and so on. The extracted extract can then be further fractionated with a solvent selected from the group consisting of hexane, methylene chloride, acetone, ethyl acetate, ethyl ether, chloroform, water and mixtures thereof. The thus-prepared extract or the fraction obtained by performing the fractionation process may be filtered, concentrated or dried to remove the solvent, and may be subjected to both filtration, concentration and drying. Specifically, the filtration can be performed using a filter paper or a vacuum filter, and the concentration can be reduced by using a vacuum concentrator, for example, a rotary evaporator. The drying can be performed by, for example, freeze drying.
본 발명에 따른 붉나무추출액은 용매추출법에 의해 추출하며, 용매로는 헥산(Hexane), 에틸아세테이트(Ethyl acetate), 메탄올(Methanol), 에탄올(Ethanol)을 이용하여 추출하였다. 붉나무의 줄기, 잎줄기, 잎, 뿌리, 열매를 채취하여 건조하고 분쇄하여 원료를 준비하고, 상기 원료 총중량 1 대비 5 중량비의 용매를 첨가하여 환류 냉각관을 통해 75℃ 수욕상에서 3시간 추출하고 여과하여 회전진공증발기(rotary vacuum evaporator)로 농축하여 추출물을 얻었다. 상기 용매별 추출물을 클로로포름(chloroform)으로 분획하여 클로로포름 분획물(chloroform fraction)을 얻고 다시 에틸아세테이트(ethyl acetate), 부탄올(butanol) 및 물(H2O) 순서로 분획하여 분획물을 얻었다. 이 분획물을 45℃ 수욕상에서 회전진공증발기를 이용하여 농축하여 붉나무추출액을 제조하였다.
The extracts of rhusi extract according to the present invention were extracted by solvent extraction and extracted with hexane, ethyl acetate, methanol and ethanol as solvents. Dried, and pulverized to prepare a raw material. A solvent of 5 wt% based on the total weight of the raw material was added, and the mixture was extracted through a reflux condenser for 3 hours on a water bath at 75 ° C. Filtration And concentrated with a rotary vacuum evaporator to obtain an extract. The chloroform fraction was fractionated with chloroform and the fractions were fractionated with ethyl acetate, butanol and water (H 2 O). The fractions were concentrated on a rotary vacuum evaporator at 45 ° C in a water bath to prepare rhusi extract.
표 1은 용매별 추출 수율을 나타낸 것으로, 극성이 높은 메탄올과 에탄올 용매를 사용한 경우 추출율이 높았다. 메탄올이 가장 높은 14.53%, 다음으로 에탄올 11.20%로 높고, 에틸아세테이트와 헥산이 비교적 낮은 추출수율을 나타내었다.
Table 1 shows the extraction yield of each solvent. When methanol and ethanol solvents having high polarity were used, the extraction rate was high. Methanol was the highest at 14.53%, followed by ethanol at 11.20%, and ethyl acetate and hexane showed relatively low extraction yields.
상기 용매추출방법이외에, 본 발명에 따른 붉나무추출액은 붉나무에서 채취한 줄기, 잎줄기, 잎, 열매, 뿌리로 이루어진 그룹에서 선택된 일 이상의 원료에 원료 총중량 1 대비 4~8 중량비의 물을 첨가하여 열수추출하는 것이 바람직하다.In addition to the solvent extraction method, the ruschii extract according to the present invention may be prepared by adding water in an amount of 4 to 8 parts by weight based on the total weight of raw materials to one or more raw materials selected from the group consisting of stem, leaf stem, leaf, It is preferable to extract it.
붉나무에서 유효성분을 충분히 추출하기 위해서 130℃ ~ 150℃ 의 고온에서 고압으로 열수추출한다. 130℃ 미만에서는 유효성분이 충분히 추출되지 않고, 150℃ 이상에서는 시간은 단축되나 효율성이 떨어진다. 압력은 2~5 ㎏/㎤ 범위가 바람직하다. 이러한 고압이 붉나무의 식물벽을 약화시켜 추출 효율을 증대시키므로 낮은 압력에서는 유효성분 추출 수율이 떨어진다.
In order to extract the effective components sufficiently from rhusi, hot water is extracted at high temperature of 130 ℃ ~ 150 ℃. If the temperature is less than 130 ° C, the active ingredient is not sufficiently extracted, and if the temperature is more than 150 ° C, the time is shortened but the efficiency is decreased. The pressure is preferably in the range of 2 to 5 kg / cm < 3 >. These high pressures weaken the plant wall of rhus wood and increase the extraction efficiency, so the yield of extracting the active ingredient is low at low pressure.
본 발명의 다른 일예로, 상기 붉나무 추출물은 붉나무 껍질을 건조하고 분쇄하여 건조시료를 제조한 후, 상기 건조시료를 열수에 첨가하고 추출하여 조추출액을 얻은 후에, 상기 조추출액을 감압 농축하여 제조할 수 있다. 상기 수득한 붉나무 추출물은 사용 시까지 급속 냉동고(deep freezer)에 보관할 수 있다. 상기 붉나무 추출물은 상기 수득된 추출액을 농축 및 동결건조를 통하여 수분을 완전히 제거시킨 것일 수 있으며, 상기 수분을 완전히 제거시킨 붉나무 추출물은 분말형태로 사용하거나 상기 분말을 증류수 또는 통상의 용매에 녹여 사용할 수 있다.
In another embodiment of the present invention, the rhusi extract is dried and pulverized to prepare a dried sample. The dried sample is added to hot water and extracted to obtain a crude extract. The crude extract is then concentrated under reduced pressure to prepare a crude extract . The obtained rattan extract can be stored in a deep freezer until use. The rattan extract can be obtained by completely removing moisture through concentration and lyophilization of the obtained extract, and the rattan extract that has completely removed the moisture can be used in the form of powder, or the powder can be dissolved in distilled water or a common solvent have.
또는, 상기 붉나무 추출물은 붉나무 열매, 잎, 가지, 줄기, 뿌리로 이루어진 그룹에서 일 이상 선택된 재료 100 중량부 대비 물 30~50 중량부를 첨가하여 분쇄하고 부유물을 제거하여 추출한 것으로 사용한다.
Alternatively, the rattan extract may be prepared by adding 30 to 50 parts by weight of water to 100 parts by weight of a material selected from the group consisting of fruit, leaves, branches, stems and roots, and removing the suspension.
또 다른 방법으로, 상기 붉나무 추출물은 붉나무의 열매, 잎, 가지, 줄기, 뿌리로 이루어진 그룹에서 일 이상 선택된 붉나무 재료 100 중량부 대비 용매 50~500중량부를 첨가하여 진탕 추출하여 여과한 것이다.
Alternatively, the rattan extract may be obtained by adding 50 to 500 parts by weight of a solvent to 100 parts by weight of a selected one or more rhexin materials selected from the group consisting of fruit, leaves, branches, stems and roots of rhusin, and extracting with shaking and filtering.
표 2 는 본 발명에 사용되는 붉나무추출액에 대한 플라즈마 분광 분석결과이다. 붉나무추출액을 유도플라즈마 분광분석(Inductively Coupled Plasma Spectrophotometer)로 분석한 것으로 2단계에 의한 붉나무추출액을 질산과 과산화수소로 전처리한 다음 핫플레이트로 산분해하고 분석하였다.
Table 2 shows the results of plasma spectroscopic analysis of the rusks extract used in the present invention. The rhusi extract was analyzed by inductively coupled plasma spectrophotometry. The rusk extract was pretreated with nitric acid and hydrogen peroxide and analyzed by acidic decomposition on a hot plate.
시료명
Name of sample
표 2 에서 알 수 있듯이, 붉나무 추출액에는 칼슘, 마그네슘, 망간, 니켈, 아연, 알루미늄, 나트륨, 인 등의 무기질이 포함되어 있어 인체에 필요한 미네랄 공급원이 될 수 있다. 한편, 나트륨은 1리터당 22.3mg이 포함되어 있는데 해수의 나트륨이 1리터당 100000mg 임을 감안하면 매우 미미한 양임을 알 수 있다. 본 발명에 따른 붉나무소금은 짠맛을 나타내지만 나트륨 성분이 거의 없다. As can be seen from Table 2, the rusks extract contains inorganic minerals such as calcium, magnesium, manganese, nickel, zinc, aluminum, sodium and phosphorus, which can be a mineral source necessary for the human body. On the other hand, sodium is 22.3mg per liter, which is very insignificant considering that sodium in seawater is 100000mg per liter. Rousseau salt according to the present invention exhibits salty taste, but has almost no sodium component.
상기 붉나무 추출액에 세척된 생선을 침지하여 가염한다. 다량의 소금 대신 나트륨 함량이 적고 항균효능이 있는 붉나무 추출물에 젓갈 원료를 침지하고 가염하여 젓갈을 제조하므로 나트륨의 함량을 낮출 수 있다.
The washed fish is immersed in the rhusi extract to be salt. Instead of a large amount of salt, it is possible to lower the sodium content by preparing the fermented seaweed extract by immersing the fermented raw material in the rattan extract having low sodium content and antibacterial activity.
2'단계(S2') 2 ' step S2'
상기 제2단계의 붉나무 추출액에 침지하는 단계에 앞서 원료 생선의 총 중량 100 중량부 대비 8~20 중량부의 소금을 혼입하여 가염하는 단계를 추가로 포함한다. 일반적으로 젓갈제조시 젓갈원료에 식염의 침투 속도와 침투량은 가염량, 염장온도 등에 따라 달라진다고 알려져 있다. 즉 가염농도가 높을수록 초기염도 증가속도가 높은 것은 삼투압이 농도에 비례하여 높아지므로 원료 육 조직 속으로 염의 침투속도가 높아지고, 상대적으로 유출되는 액즙 중의 농도도 증가하게 된다. 또한 가염농도가 높을수록 고형물과 유출액의 염도차가 큰 것은 육과 염의 결합력이 가염농도에 비례적으로 증가하지 않기 때문인데 식염의 침투로 식품 중에 식염용액이 형성되고, 여기에 젓갈 원료 생선 단백질이 용해하여 콜로이드 용액을 만들며 이것이 삼투압이 높기 때문에 수분을 다시 흡수하게 된다. 그러나 식염침투량이 많아져, 원료 생선 육의 식염농도가 높아지면 단백질의 용해성이 감소되어 염석현상이 일어나므로 수분의 흡수는 정지된다고 보고되고 있다. 저염 젓갈 완제품의 염도를 8 ~ 10%으로 조정하기 위해서는, 타 조미재료와 배합조성을 감안하여, 염장과 숙성 단계의 염도를 각 10~ 12%, 9~ 11% 정도 유지해야 한다. 염장에서 유출액을 제거한 젓갈 원료 고형물의 염도를 10~12%로 조정하기 위해서는, 가염농도는 13%이상 되어야 한다. 따라서 원료 생선의 총 중량 100 중량부 대비 8~20 중량부의 소금을 혼입하여 가염하는 단계를 추가로 포함하는데, 원료 생선의 총 중량 100 중량부 대비 8 중량부의 소금을 혼입하는 경우 20%중량부의 소금을 혼입하는데 비해 비교적 긴 시간 동안 염장을 해야한다. 대략 소금 13%를 첨가한 경우 약 2시간 이후 원료 생선 고형물의 염도가 수분활성감소를 통한 염도 평형에 도달하였다. The method further includes a step of adding 8-20 parts by weight of salt to 100 parts by weight of the total weight of the raw fish prior to the step of immersing in the rhusin extract in the second step. It is generally known that the rate and amount of salt infiltration to the fermented raw materials during fermentation depends on the amount of salt, salting temperature, and so on. That is, the higher the salt concentration, the higher the initial salinity increase rate is, because the osmotic pressure increases in proportion to the concentration, so that the penetration rate of the salt into the raw meat texture increases and the concentration in the relatively distilled juice increases. In addition, the higher the salt concentration, the greater the salinity difference between the solids and the effluent is because the binding force of the salt and the salt does not increase proportionally with the salt concentration. The salt solution is formed in the food by the infiltration of the salt, It creates a colloidal solution which absorbs moisture again because of its high osmotic pressure. However, it has been reported that as the salt infiltration increases, the solubility of the protein decreases as the salt concentration of the raw fish meat increases, and the absorption of moisture is stopped because salting occurs. In order to adjust the salinity of the low salted pickles to 8 ~ 10%, salinity of the salting and maturing stages should be kept about 10 ~ 12% and 9 ~ 11%, respectively, taking into consideration the ingredients and composition. In order to adjust the salinity of the seaweed solid to 10-12%, the salt concentration should be over 13%. Therefore, the present invention further includes a step of adding 8-20 parts by weight of salt to 100 parts by weight of the total weight of the raw fish. When 8 parts by weight of salt is mixed with 100 parts by weight of the total weight of raw fish, 20% Compared to incorporating a relatively long time must be salted. When about 13% of salt was added, the salinity of the raw fish solids reached the salinity equilibrium by reducing the water activity after about 2 hours.
한편, 온도는 20℃ 이하로 유지하는 것이 바람직한데, 그 이상의 경우 미생물이 증식하게 되어 변질될 수 있다. On the other hand, it is preferable that the temperature is maintained at 20 캜 or lower, and microorganisms may proliferate and deteriorate when the temperature is higher than 20 캜.
염장 후 발생되는 유출액은 염용성 단백질, 엑스분, 비타민, 염류 등을 함유하고 있으나 염장 유출액을 제거하여도 유실된 성분이 젓갈의 관능적품질에 미치는 영향이 미비하여 유출수를 제거함으로써 젓갈 제조공정상의 수분저하에 따른 효율성이 개선될 수 있다.
The effluent after salting contains salt soluble proteins, extracts, vitamins, and salts. However, even if the salted out effluent is removed, the effluent is not removed due to the loss of the sensory quality of the fermented seafood. The efficiency due to degradation can be improved.
3 단계(S3) Step S3 (S3)
다음으로, 상기 가염된 생선을 건져내 물기를 제거한 후 숙성하는 단계를 거치게 된다. 숙성을 하면 Brix는 증가하고, pH는 감소하게 된다. 숙성은 1일 ~ 60일정도 할 수 있다. 교반숙성하는 경우 숙성기간이 단축된다. 숙성 중 미생물의 증식이 되므로 초기 산소와의 접촉을 차단한 상태에서 숙성이 이루어지는 것이 바람직하다. 숙성과정에서 유리아미노산이 증가하는데 원료 생선에 따라 그 유리아미노산의 종류는 차이가 있다. 창란젓갈의 경우 글루타민산(glutamin acid), 아르기닌(arginine), 프롤린(proline), 루신(leucine)이, 굴젓의 경우 글루타민산(glutamin acid), 알라닌(alanine) 의 유리아미노산이 증가하였다.
Next, the above-mentioned fishes are removed, and the water is removed and then aged. When aged, Brix increases and pH decreases. It can be aged from 1 day to 60 days. Aging aging shortens the ripening period. It is preferable that aging is carried out in a state in which contact with initial oxygen is blocked since microbial growth occurs during aging. The free amino acids are increased during the fermentation process, and the kinds of free amino acids are different according to the raw fish. The free amino acids of glutamin acid, arginine, proline, leucine and glutamin acid and alanine were increased in the case of Chang Ranjang.
4단계(S4) Step S4 (S4)
상기 숙성 후 양념으로 조미하여 원적외선으로 살균시켜 포장하여 기능성 젓갈을 제조한다.After the aging, seasoned with seasoning, sterilized by far-infrared rays, and packed to produce a functional fermented seafood.
양념은 원료생선 및 소비자의 기호에 따라 다양한 재료로 다양한 방식으로 제조하여 양념하게 된다. 주요 양념으로 고춧가루는 무균 고춧가루를 사용하는 것이 바람직하다. 이외에도 솔비톨, 마늘, 생강 등의 향신용 재료 등이 사용된다.Seasonings can be produced and seasoned in a variety of ways, depending on the raw fish and consumer preferences. It is preferable to use sterile red pepper powder as a main spice. In addition, fragrance ingredients such as sorbitol, garlic, and ginger are used.
한편 양념 조미한 젓갈은 원적외선으로 살균건조하여 포장하여 젓갈을 제조한다.
On the other hand, seasoned salted seafood is sterilized by far infrared rays and packed to produce seafood.
비교예Comparative Example 1 One
오징어젓갈용 원료 오징어를 선별하고 껍질과 내장을 제거하였다, 오징어를 20% 소금물에 1시간 담근 다음 꺼내어 물기를 제거하였다. 가염된 원료 오징어를 건져내 물기를 제거한 후 적당한 크기로 절단하여, 5℃ 숙성실에서 3일간 숙성시켰다. 숙성 후 고춧가루, 마늘, 설탕, 글루타민산나트륨, 솔빈산(sorbio acid), 소금, 비타민 C를 포함한 양념을 준비하여 숙성된 원료 오징어에 혼합하고 원적외선으로 살균한 다음 포장용기에 담아 밀봉하였다.
The raw squid was removed from the squid, and the skin and the viscera were removed. The squid was soaked in 20% saline for 1 hour, and then the water was removed. The raw fish squid was removed, the water was removed, cut to a suitable size, and aged in a 5 ° C aging room for 3 days. After aging, sauce containing red pepper powder, garlic, sugar, sodium glutamate, sorbio acid, salt, and vitamin C was prepared and mixed with aged raw squid, sterilized by far infrared rays, and sealed in a packaging container.
실시예Example 1 One
창란젓갈용 원료 창란을 선별하여 10kg준비하고, 소금 1kg을 고루 혼합하여 5℃에서 24시간 저장한 다음 기생충과 협잡물을 제거하였다. 다음으로 창란을 13% 소금물에 30분간 담근 다음 꺼내어 물기를 제거하고, 다시 붉나무추출액에 침지하여 10rpm으로 2시간 교반 가염하고, 생성된 유출수를 제거하였다. 가염된 원료 창란을 건져내 물기를 제거한 후 적당한 크기로 절단하여, 5℃ 숙성실에서 30일간 숙성시켰다. 숙성 후 고춧가루, 마늘, 설탕, 글루타민산나트륨, 솔빈산(sorbio acid), 소금, 비타민 C를 포함한 양념을 준비하여 숙성된 원료 창란에 혼합하고 원적외선으로 살균한 다음 포장용기에 담아 밀봉하였다.
The broiler chrysanthemums were prepared by weighing 10 kg of broiler chrysanthemum, and 1 kg of salt was mixed thoroughly, stored at 5 ° C for 24 hours, and then parasites and contaminants were removed. Next, the straw was immersed in 13% brine for 30 minutes, then taken out to remove water, and then immersed in rusk extract, stirred at 10 rpm for 2 hours, and the produced effluent was removed. The frozen raw broth was removed, the water was removed, and the broth was cut to a suitable size and aged for 30 days in a 5 ° C aging room. After aging, spices containing red pepper powder, garlic, sugar, sodium glutamate, sorbio acid, salt and vitamin C were prepared, sterilized by the far infrared ray, and sealed in a packaging container.
실시예Example 2 2
오징어젓갈용 원료 오징어를 선별하고 껍질과 내장을 제거하였다, 오징어를 13% 소금물에 30분간 담근 다음 꺼내어 물기를 제거하고, 다시 붉나무추출액에 2시간 침지하여 가염하였다. 가염된 원료 오징어를 건져내 물기를 제거한 후 적당한 크기로 절단하여, 5℃ 숙성실에서 3일간 숙성시켰다. 숙성 후 고춧가루, 마늘, 설탕, 글루타민산나트륨, 솔빈산(sorbio acid), 소금, 비타민 C를 포함한 양념을 준비하여 숙성된 원료 오징어에 혼합하고 원적외선으로 살균한 다음 포장용기에 담아 밀봉하였다.
The raw squid was removed from the squid, and the squid was immersed in 13% brine for 30 minutes, then the water was removed, and the squid was immersed in the rusk extract for 2 hours. The raw fish squid was removed, the water was removed, cut to a suitable size, and aged in a 5 ° C aging room for 3 days. After aging, sauce containing red pepper powder, garlic, sugar, sodium glutamate, sorbio acid, salt, and vitamin C was prepared and mixed with aged raw squid, sterilized by far infrared rays, and sealed in a packaging container.
젓갈의 보존성 시험Conservation test of fermented seafood
위 비교예 1, 실시예2에 따른 각각의 젓갈을 밀폐용기에 나누어 담은 후 마개를 닫고 마개부위를 밀착필름으로 감고 나서 20℃에 저장하면서 일일 단위로 마개를 열어 냄새를 확인하였다. 비교예 1은 4일차 변질이 일어났으나 실시예2에 따른 젓갈은 8일만에 변질이 일어났다.
Each of the fermented fish according to Comparative Example 1 and Example 2 was put in a sealed container, and the stopper was closed. The end portion of the stopper was wrapped with an adhesive film, and the stopper was opened every day while storing at 20 ° C to confirm the smell. In the case of Comparative Example 1, four days of alteration occurred, but in the case of Example 2, the fermentation occurred in only eight days.
이와 같이 본 발명에 따른 붉나무추출액에 침지하여 가염하여 젓갈을 제조하는 경우 기존 방식으로 제조한 젓갈에 비해 제품의 유통기한이 연장되었다.
In case that the fermented seaweed extract is immersed in the rhusin extract according to the present invention to produce the fermented seafood, the shelf life of the fermented seafood product is extended as compared with the fermented seafood produced by the conventional method.
S1 : 제 1 단계
S2: 제 2 단계
S2' : 제 2' 단계
S3 : 제 3 단계
S4: 제 4 단계
S1: first step S2: second step
S2 ': the second step S3: the third step
S4: Step 4
Claims (8)
상기 세척된 생선을 붉나무 추출액에 침지하여 가염하는 제2단계;
상기 가염된 생선을 건져내 물기를 제거한 후 숙성하는 제3단계; 및
상기 숙성 후 양념으로 조미하여 살균시켜 포장하는 제4단계를 포함하는 것을 특징으로 하는 기능성 젓갈의 제조방법.
The first step is to select the fishes for the fermented fishes and wash them with 5% to 20% salt water to remove the water.
A second step of immersing the washed fish in an extract of rhusi mushroom to be salt;
A third step of extracting the above-mentioned fish from which the salt has been removed to remove water and then aging; And
And a fourth step of sterilization and packaging after seasoning with the seasoning after the aging.
상기 제2단계의 붉나무 추출액에 침지하는 단계에 앞서 원료 생선의 총 중량 100 중량부 대비 8~20 중량부의 소금을 혼입하여 가염하는 단계를 추가로 포함하는 것을 특징으로 하는 기능성 젓갈의 제조방법.
The method according to claim 1,
Further comprising the step of adding 8-20 parts by weight of salt to 100 parts by weight of the total weight of the raw fish prior to the step of immersing in the rush extract of the second step.
상기 붉나무추출액은 붉나무에서 채취한 줄기, 잎줄기, 잎, 열매, 뿌리로 이루어진 그룹에서 선택된 일 이상의 원료에 원료 총중량 1 대비 5~10 중량비의 에탄올 또는 메탄올을 첨가하여 상등액을 분리하여 추출하는 것을 특징으로하는 기능성 젓갈의 제조방법.
The method according to claim 1,
The rhusi extract is prepared by separately extracting the supernatant by adding ethanol or methanol in an amount of 5 to 10 wt% based on the total weight of the raw material to one or more raw materials selected from the group consisting of stem, leaf stem, leaf, By weight.
상기 붉나무추출액은 붉나무에서 채취한 줄기, 잎줄기, 잎, 열매, 뿌리로 이루어진 그룹에서 선택된 일 이상의 원료에 원료 총중량 1 대비 4~8 중량비의 물을 첨가하여 열수추출하는 것을 특징으로하는 기능성 젓갈의 제조방법.
The method according to claim 1,
Wherein the rattan extract is added with one or more raw materials selected from the group consisting of stem, leaf stem, leaf, fruit, and root collected from the rhusi, and water is extracted in a ratio of 4 to 8 by weight based on the total weight of the raw material to perform hot water extraction. Gt;
상기 붉나무 추출물은 붉나무의 열매, 잎, 가지, 줄기, 뿌리로 이루어진 그룹에서 일 이상 선택된 재료 100 중량부 대비 용매 30~50 중량부를 첨가하여 분쇄하고 부유물을 제거하여 추출하는 것을 특징으로 하는 기능성 젓갈의 제조방법.
The method according to claim 1,
Wherein said rattan extract is pulverized by adding 30 to 50 parts by weight of a solvent relative to 100 parts by weight of a material selected from the group consisting of fruit, leaves, branches, stems and roots of rhusin, Gt;
상기 붉나무 추출물은 붉나무의 열매, 잎, 가지, 줄기, 뿌리로 이루어진 그룹에서 일 이상 선택된 붉나무 재료 100 중량부 대비 용매 50~500중량부를 첨가하여 진탕 추출하여 여과하는 것을 특징으로 하는 기능성 젓갈의 제조방법.
The method according to claim 1,
Wherein said rattan extract is added with 50 to 500 parts by weight of a solvent relative to 100 parts by weight of a selected one or more rusks selected from the group consisting of fruit, leaves, branches, stems and roots of rhusin, and extracted with shaking and filtered. .
제1단계에 의한 세척된 젓갈용 생선을 마이크로웨이브를 조사하여 살균하는 단계를 추가로 포함하는 것을 특징으로 하는 기능성 젓갈의 제조방법.
The method according to claim 1,
Further comprising the step of sterilizing the washed fish for the fermented fish by the first step by irradiating microwaves.
A functional fermented fish meal produced by the method according to any one of claims 1 to 7.
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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KR102084370B1 (en) * | 2019-09-20 | 2020-03-03 | 송금희 | A manufacturing method of salted and fermented squid |
KR20200062514A (en) | 2018-11-27 | 2020-06-04 | 단국대학교 천안캠퍼스 산학협력단 | Polymer cell mixed spheroids, method for preparing thereof, and use thereof |
KR20240038229A (en) | 2022-09-16 | 2024-03-25 | 유한회사 해담홀딩스 | manufacturing method of the seasoning fermented seafood in which the black tea syrup is added |
KR102658580B1 (en) * | 2023-08-03 | 2024-04-18 | 주식회사 세강식품 | Seasoned laver composition containing Aronia powder and a method of manufacturing seasoning laver using the same |
KR102658579B1 (en) * | 2023-08-03 | 2024-04-18 | 주식회사 세강식품 | Cosmetic laver composition and method for manufacturing cosmetic laver using |
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2015
- 2015-06-16 KR KR1020150085472A patent/KR20160140291A/en not_active Withdrawn
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20200062514A (en) | 2018-11-27 | 2020-06-04 | 단국대학교 천안캠퍼스 산학협력단 | Polymer cell mixed spheroids, method for preparing thereof, and use thereof |
KR102084370B1 (en) * | 2019-09-20 | 2020-03-03 | 송금희 | A manufacturing method of salted and fermented squid |
KR20240038229A (en) | 2022-09-16 | 2024-03-25 | 유한회사 해담홀딩스 | manufacturing method of the seasoning fermented seafood in which the black tea syrup is added |
KR102658580B1 (en) * | 2023-08-03 | 2024-04-18 | 주식회사 세강식품 | Seasoned laver composition containing Aronia powder and a method of manufacturing seasoning laver using the same |
KR102658579B1 (en) * | 2023-08-03 | 2024-04-18 | 주식회사 세강식품 | Cosmetic laver composition and method for manufacturing cosmetic laver using |
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