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KR101413964B1 - Method for preparing hemiptera repellant containing a garlic extract and hemiptera repellant containing a garlic extract by the same - Google Patents

Method for preparing hemiptera repellant containing a garlic extract and hemiptera repellant containing a garlic extract by the same Download PDF

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KR101413964B1
KR101413964B1 KR1020130164321A KR20130164321A KR101413964B1 KR 101413964 B1 KR101413964 B1 KR 101413964B1 KR 1020130164321 A KR1020130164321 A KR 1020130164321A KR 20130164321 A KR20130164321 A KR 20130164321A KR 101413964 B1 KR101413964 B1 KR 101413964B1
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garlic
yellowing
hemiptera
garlic juice
garlic extract
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임창미
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Environmental Sciences (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Pest Control & Pesticides (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

본 발명은 마늘즙액을 포함하는 노린재 기피제의 제조 방법 및 이에 의하여 제조된 마늘즙액을 포함하는 노린재 기피제에 대한 것이다.
본 발명에 의한 노린재 기피제는 천연 마늘을 이용함으로써 인체에 위험한 요소가 없고 과수에 사용하여 잔류하더라도 부작용을 초래할 염려가 전혀 없을 뿐만 아니라, 마늘의 알리신에 의해 노린재에 대한 뛰어난 방충 효과를 나타낸다.The present invention relates to a process for producing a yellowing repellent containing garlic juice and a yellowing repellent containing the garlic juice produced thereby.
The yellowing repellent according to the present invention has no dangerous elements in human body by using natural garlic and has no fear of causing side effects even if it is used in fruit water, and also shows excellent insecticidal effect on alumina by alicin of garlic.

Description

마늘즙액을 포함하는 노린재 기피제의 제조 방법 및 이에 의하여 제조된 마늘즙액을 포함하는 노린재 기피제 {METHOD FOR PREPARING HEMIPTERA REPELLANT CONTAINING A GARLIC EXTRACT AND HEMIPTERA REPELLANT CONTAINING A GARLIC EXTRACT BY THE SAME}FIELD OF THE INVENTION [0001] The present invention relates to a method for producing a yellowing repellent containing garlic juice, and a garlic extract containing the garlic juice. [0002]

본 발명은 마늘즙액을 포함하는 노린재 기피제의 제조 방법 및 이에 의하여 제조된 마늘즙액을 포함하는 노린재 기피제에 대한 것이다.
The present invention relates to a process for producing a yellowing repellent containing garlic juice and a yellowing repellent containing the garlic juice produced thereby.

최근 한국에서는 흡수성 노린재류가 쌀, 보리, 콩 등의 식량작물과 사과, 감, 배 등을 포함하는 과수작물의 중요한 해충으로 대두되었다. 이들은 작물의 종실 및 과일을 구침으로 찔러 흡즙하여 섭식하므로 농업 생산의 목표 산물을 직접 가해하여 그 경제적 피해가 크며, 이동성이 강하여 살충제를 사용해서 방제하기가 어려운 실정이다.In recent years, absorptive yellowing has emerged as an important pest of fruit crops including rice, barley, soybean, food crops, apple, persimmon, and pear. Because they feed on the seeds and fruits of the crops by plowing them and feeding them, they are difficult to control by using insecticides because they have a great economic impact due to direct addition of agricultural products.

또한, 해충을 손쉽게 구제하기 위해 이용되는 화학합성농약은 맹독성 물질이므로 인체에 위험한 요소가 많고 사용 후 분해되는데 많은 시일이 걸리기 때문에 잔류하여 부작용을 초래할 뿐만 아니라 환경오염을 일으키는 등의 문제가 있다.In addition, the chemical synthetic pesticide used for easy rescue of pests is a toxic substance, so there are a lot of dangerous elements in the human body, and since it takes a lot of time to be decomposed after use, it causes a side effect and causes environmental pollution.

살충제 사용 외의 노린재의 방제법으로 (1)집합페로몬을 이용한 유인트랩을 사용하는 행동적 방제법과 (2)노린재 알에 기생하는 기생벌에 의한 생물적 방제법 등이 알려져 있다. 특히 안전 농산물을 선호하는 소비자의 소비패턴의 변화로 친환경인증 농경지의 면적이 2007년 현재 122,882ha로 매년 증가하고 있어(농산물품질 관리원 2007, http://www.naqs.go.kr) 위의 두 방법은 친환경적 해충 방제법으로 주목을 받고 있다. (1) Behavioral control methods using manned traps using aggregated pheromones and (2) biological control methods using parasitic parasitic arthropods are known. In particular, due to changes in consumption patterns of consumers who prefer safe agricultural products, the area of certified eco-friendly agricultural land is increasing every year to 122,882ha as of 2007 (Agricultural Product Quality Management Office 2007, http://www.naqs.go.kr) The method is attracting attention as an environmentally friendly pest control method.

상기한 (1)의 방법은 이미 국내 특허등록 제10-0853616호에서 공지되어 있으며 (주)그린아그로텍에서 통발형 유인트랩으로 상품화하여 널리 사용되고 있다. 천적을 이용한 (2)의 방법은 과거 미국, 일본, 브라질 등의 많은 국가에서 성공적으로 실시되었으나(Orr 1988, Fla. Entomol. 71: 506-527), 국내에서는 현실적으로 적용이 어렵다. 그 이유는 (1)방제 대상인 노린재가 주로 노지 작물에서 발생되는 경우가 많기 때문에 방대한 수의 천적의 증식에 많은 비용이 들어가 가격 경쟁력이 떨어지며, (2)공장에서 증식된 천적들은 야외 방사 시에 환경 적응성이 떨어지는 단점이 있어 그 효과가 일관되지 못하는 경우가 많기 때문이다. 이에 따라 친환경 노린재 기피제를 연구 개발해야 할 필요성이 증대되고 있다. The method (1) described above is already known from Korean Patent Registration No. 10-0853616, and is commercialized as a trap type attracting trap in Green Agrotech Co., Ltd. and is widely used. The method of (2) using natural enemies has been successful in many countries such as the USA, Japan, and Brazil in the past (Orr 1988, Fla. Entomol. 71: 506-527). The reason is that (1) the irritant, which is the object to be controlled, is often generated from the non-crop, and therefore, the cost of the vast number of natural enemies is increased and the cost competitiveness is poor; (2) This is because there are disadvantages of poor adaptability and the effects are often inconsistent. As a result, there is a growing need to research and develop environment-friendly yellowing agents.

따라서 최근 해충의 저항성 관리에 충분한 약제의 효과적인 돌려쓰기를 위한 새로운 약제에 대한 요구가 증가하고 있다.Thus, there is a growing demand for new drugs for effective return of drugs that are recently sufficient to control pest resistance.

또한 상기와 같은 화학합성농약의 한계를 극복하기 위하여 세대 농약의 개발 일환으로 미생물, 천적, 또는 천연추출물을 이용한 생물학적 방제에 대한 연구가 활발히 진행되고 있다. 특히 천연물로부터 추출된 추출물을 방제용 약제로 이용하는 연구가 활발히 진행되고 있는데, 대한민국 공개특허공보 특2002-0074793호에는 대회향, 양고추냉이, 마늘 및 겨자 등으로부터 추출된 살충 조성물이 개시되어 있고, 대한민국 공개특허공보 특2003-0030319호에는 어등 추출물과 고삼 추출물이 동시에 함유된 천연 살충 조성물이 개시되어 있으며, 대한민국 공개특허공보 제10-2004-0035218호에는 살충제 및 항균제로 이용되는 은행잎 추출물이 개시되어 있다.
In order to overcome the limitations of chemical synthetic pesticides as described above, researches on biological control using microorganisms, natural enemies, or natural extracts have been actively conducted as part of development of household pesticides. Particularly, researches using an extract extracted from natural materials as a medicine for controlling are actively proceeding. Korean Patent Publication No. 2002-0074793 discloses an insecticide composition extracted from a horseradish, horseradish, horseradish, garlic and mustard. Japanese Patent Application Laid-Open No. 2003-0030319 discloses a natural insecticidal composition containing a fish extract and a ginseng extract at the same time, and Korean Patent Laid-Open Publication No. 10-2004-0035218 discloses a ginkgo leaf extract used as an insecticide and an antibacterial agent .

마늘은(Garlic, Allium sativum) 중앙아시아가 원산지이며, 백합과의 식물로써 예로부터 가정에서는 조미료 및 향신료로 사용되었으며, 민간요법으로는 종양, 기생충, 궤양 등 치료에 사용되었다. 이러한 마늘의 효능은, 혈액순환을 원활히 하여 신선한 혈액을 공급하고 진정효과가 있어 신경을 안정시키고 호르몬 분비를 촉진 시킨다. 또한 면역력을 증강시키는 효과, 병원균과 암세포에 대한 저항을 높이는 효과, 순환기병의 예방과 치료효과 등 많은 효능이 있다고 알려져 있으며, 세계의 10대 건강식품으로 선정될 정도로 전 세계적으로도 알려져 있다.Garlic (Garlic, Allium sativum) Origin of Central Asia. It is a plant of lilies. It has been used as a seasoning and spice at home. It has been used for treatment of tumors, parasites and ulcers in folk remedies. The efficacy of this garlic smoothes blood circulation, supplies fresh blood, and has a soothing effect to stabilize nerves and promote hormone secretion. It is also known to be one of the top 10 health food products in the world and has been known to have many effects such as improving immunity, increasing resistance to pathogens and cancer cells, preventing and treating circulatory cavalry, and the like.

또한, 마늘은 인체에 매우 유용한 필수 아미노산 등 매우 다양한 성분을 포함하고 유익한 효과가 있으며, 마늘의 대표적 성분은 유기유황(有機硫黃) 성분인 알린(Allin)인데, 이 알린이라는 성분은 마늘을 자르거나 빻을 때 세포가 파괴되면서 알리나아제라는 효소의 작용에 의해 매운 맛과 냄새가 나는 알리신(allicin)으로 변하여 독특한 냄새로서 동물의 후각과 미각을 자극하게 된다.
In addition, garlic contains a very wide variety of ingredients, including essential amino acids, which are very useful in human body, and has a beneficial effect. A representative component of garlic is Allin, an organic sulfur component, When cells are destroyed when they are nibbled, Alina Azera is transformed into allicin, which has a pungent flavor and smell due to the action of enzymes, which stimulates the olfactory sense and taste of animals as a unique smell.

본 발명은 마늘의 알리신 성분을 활용하여 노린재 기피 효과를 나타낼 수 있도록 마늘즙액을 포함하는 노린재 기피제의 제조 방법을 제공하는 것을 목적으로 한다. It is an object of the present invention to provide a method for producing a yellowing repellent agent containing garlic juice so as to exhibit a yellowing effect by utilizing an allysine component of garlic.

본 발명은 또한, 본 발명의 제조 방법에 의하여 제조된 마늘즙액을 포함하는 노린재 기피제를 제공하는 것을 목적으로 한다.
The present invention also aims to provide a yellowing repellent containing garlic juice produced by the production method of the present invention.

본 발명은 상기와 같은 과제를 해결하기 위하여 The present invention has been made to solve the above problems

마늘을 분쇄하는 제 1 단계;A first step of pulverizing garlic;

분쇄된 마늘 100g 내지 1000g 중량부당 물 0.5L 내지 5L의 비율로 혼합하는 제 2 단계; A second step of mixing 0.5 to 5 L of water per 100 g to 1000 g of ground garlic;

상기 혼합액을 60~78℃에서 24~50시간 숙성시켜서 마늘즙액을 제조하는 제 3 단계; A third step of aging the mixed solution at 60 to 78 ° C for 24 to 50 hours to prepare garlic juice;

상기 마늘즙액을 여과하는 제 4 단계; 및 A fourth step of filtering the garlic juice; And

상기 마늘즙액에 알코올을 첨가하는 제 5 단계;를 포함하는 마늘즙액을 포함하는 노린재 기피제의 제조 방법을 제공한다. And a fifth step of adding alcohol to the garlic juice. The method for producing the garlic extract of the present invention comprises the step of adding garlic juice to the garlic juice.

본 발명에 의한 노린재 기피제의 제조 방법에 있어서, 상기 마늘즙액은 여과 후 물로 100배 내지 1000배의 비율로 희석하는 단계를 더 포함하는 것을 특징으로 한다. In the method for producing a yellowing repellent according to the present invention, the garlic juice is further diluted with water at a ratio of 100 to 1000 times with water after the filtration.

본 발명에 의한 노린재 기피제의 제조 방법에 있어서, 상기 제 5 단계에서는 상기 여과된 마늘즙액 1L 당 그을음병 방지를 위한 알코올을 1ml 내지 100ml 첨가하는 것을 특징으로 한다. In the method for producing a yellowing repellent according to the present invention, in the fifth step, 1 ml to 100 ml of alcohol for preventing soot disease is added per liter of the filtered garlic juice.

본 발명에 의한 노린재 기피제의 제조 방법에 있어서, 상기 제 5 단계에서 상기 알코올은 에틸알코올, 주정 및 메틸알코올로 이루어진 그룹에서 선택되는 것을 특징으로 한다.
In the method for producing a yellowing repellent according to the present invention, in the fifth step, the alcohol is selected from the group consisting of ethyl alcohol, alcohol, and methyl alcohol.

본 발명은 또한, 본 발명의 제조 방법에 의하여 제조된 노린재 기피제를 제공한다. The present invention also provides a yellowing repellent prepared by the method of the present invention.

본 발명에 의한 노린재 기피제는 천연 마늘을 이용함으로써 인체에 위험한 요소가 없고 과수에 사용하여 잔류하더라도 부작용을 초래할 염려가 전혀 없을 뿐만 아니라, 마늘의 알리신에 의해 노린재에 대한 뛰어난 방충 효과를 나타낸다.
The yellowing repellent according to the present invention has no dangerous elements in human body by using natural garlic and has no fear of causing side effects even if it is used in fruit water, and also shows excellent insecticidal effect on alumina by alicin of garlic.

이하에서는 본 발명을 실시예에 의하여 더욱 상세히 설명한다. 그러나, 본 발명이 이하의 실시예에 의하여 더욱 한정되는 것은 아니다.
Hereinafter, the present invention will be described in more detail by way of examples. However, the present invention is not limited by the following examples.

<< 제조예Manufacturing example > 노린재 기피제의 제조> Manufacture of yellowing repellent

국산 생마늘 100g, 300g, 500g 을 각각 절편기를 이용하여 잘게 분쇄하고 물 1L 와 혼합한 후, 약 65℃에서 30시간 숙성시켰다. 숙성된 마늘즙액을 여과한 후 마늘즙액 1L 당 물을 500L 희석하여 노린재 기피제를 제조하였다.
100 g, 300 g and 500 g of domestic raw garlic were finely pulverized using a kneader, mixed with 1 L of water, and aged at about 65 캜 for 30 hours. The aged garlic juice was filtered and diluted 500 L of water per liter of garlic juice to prepare a yellowing repellent.

<실험예> 마늘즙액의 노린재에 대한 기피시험&Lt; Experimental Example > The avoidance test for the garlic juice

상기 제조예에서 각각 제조된 노린재 기피제를 사과 나무 과수원에 살포하고, 노린재가 발생하는지를 관찰하였다. 국산 생마늘 100g을 분쇄하여 제조한 마늘즙액 1L를 물 500L와 혼합한 경우 노린재가 20% 이상 발생하였고, 국산 생마늘 300g을 분쇄하여 제조한 마늘즙액 1L를 물 500L와 혼합한 경우 피해율이 약 5% 이었으며, 국산 생마늘 500g을 분쇄하여 제조한 마늘즙액 1L를 물 500L와 혼합한 경우 노린재는 발생하지 않고, 약간의 그을음 병이 발생되었다.
The yellowing repellent prepared in each of the above production examples was sprayed on an apple tree orchard, and it was observed whether or not yellowing occurred. When 1L of garlic juice prepared by grinding 100g of domestic raw garlic was mixed with 500L of water, 20% or more of the raw material was produced. When 1L of garlic juice prepared by grinding 300g of domestic raw garlic was mixed with 500L of water, the damage rate was about 5% , And 1L of the garlic juice prepared by pulverizing 500g of domestic raw garlic was mixed with 500L of water, no stain occurred and some soot was generated.

<실험예> 마늘즙액의 노린재에 대한 기피시험&Lt; Experimental Example > The avoidance test for the garlic juice

위 실험에서 최고의 효능을 보인, 국산 생마늘 500g을 분쇄하여 만든 마늘즙액 1L를 알코올 50ml와 물 500L를 혼합하여 제조한 노린재 기피제를 사과 과수원에서 홍로 품종과 부사 품종에 대해서 시험하였는바, 일정 지역에 존재하는 사과나무에 노린재 기피제를 20일 간격으로 3개월간 살포하고, 나머지 지역에는 노린재 기피제를 살포하지 않는 방식으로 진행하였다.
In the experiment above, 1L of garlic juice, which was obtained by grinding 500g of domestic raw garlic, which had the best efficacy in the above experiment, was tested in the apple orchard for the Hongro variety and adverbial varieties which were prepared by mixing 50ml of alcohol and 500L of water. Were sprayed on the apple trees for 3 months at intervals of 20 days, and the remaining areas were sprayed with no yellowing agent.

홍로 품종에 대해서는 노린재 기피제를 살포한 지역에서 수확된 사과 12000 개 중에 노린재 피해 사과는 0개 이고, 그을음병 피해 사과도 0개인데 비해, 노린재 기피제를 살포하지 않은 지역에서는 10000개 중 노린재 피해 사과가 498개 약 5%의 피해율을 보이는바, 본원 발명에 의한 노린재 기피제의 효과가 살포하지 않은 비교예에 비해 매우 우수하다는 것을 알 수 있었다.
Among the 12,000 apples harvested in the area sprayed with yellowing detergents, no apples were damaged from soiling, while apples from soot disease were 0, while apples from yellowing detergents were not applied. 498 and about 5%, respectively, and it was found that the effect of the yellowing repellent according to the present invention was much better than that of the comparative example not sprayed.

부사 품종에 대해서는 노린재 기피제를 살포한 지역에서 수확된 사과 90000 개 중에 노린재 피해 사과는 70개로 그 피해율이 0.08%에 불과한 반면, 노린재 기피제를 살포하지 않은 지역에서는 10000개 중 노린재 피해 사과가 475개로 4.75%의 피해율을 보이고 있어, 본원 발명에 의한 노린재 기피제의 효과가 살포하지 않은 비교예에 비해 매우 우수하다는 것을 알 수 있었다.Among the 90,000 apples harvested in the area where the yellowing agent was sprayed, the damage rate was only 0.08%, while the number of apples damaged by the yellowing agent was only 0.08%. In the area where no yellowing agent was sprayed, %, And it was found that the effect of the yellowing repellent according to the present invention was much better than that of the comparative example not sprayed.

Claims (5)

마늘을 분쇄하는 제 1 단계;
분쇄된 마늘 500g 중량부에 물 1L를 혼합하는 제 2 단계;
상기 혼합액을 60~78℃에서 30시간 숙성시켜서 마늘즙액을 제조하는 제 3 단계;
상기 마늘즙액을 여과한 후 마늘즙액 1L당 알코올 50ml를 첨가하는 제 4 단계; 및
상기 제조된 혼합액에 물 500L를 희석하는 제 5 단계; 를 포함하는 마늘즙액을 포함하는 노린재 기피제의 제조 방법.
A first step of pulverizing garlic;
A second step of mixing 1 L of water with 500 g of the ground garlic powder;
A third step of aging the mixed solution at 60 to 78 ° C for 30 hours to prepare garlic juice;
A fourth step of filtering the garlic juice and adding 50 ml of alcohol per liter of the garlic juice; And
A fifth step of diluting 500 L of water into the prepared mixed solution; And a garlic juice containing the garlic juice.
제 1 항에 있어서,
상기 제 5 단계의 상기 알코올은 에틸알코올, 주정, 및 메틸알코올로 이루어진 그룹에서 선택되는 것인 마늘즙액을 포함하는 노린재 기피제의 제조 방법.
The method according to claim 1,
Wherein the alcohol in the fifth step is selected from the group consisting of ethyl alcohol, alcohol, and alcohol.
삭제delete 삭제delete 삭제delete
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102083670B1 (en) * 2018-12-13 2020-03-02 대한민국 Aggregation pheromone composition for attracting and controlling Dolycoris baccarum and Trap using thereof

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* Cited by examiner, † Cited by third party
Title
인터넷 (2009.12.29) *
인터넷 (2009.12.29)*

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102083670B1 (en) * 2018-12-13 2020-03-02 대한민국 Aggregation pheromone composition for attracting and controlling Dolycoris baccarum and Trap using thereof

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