KR100796395B1 - Cosmetic Raw Material Extract and Manufacturing Method Thereof - Google Patents

Abstract

The present invention relates to a cosmetic raw material extract using natural vegetable fermentation waste and a method for producing the same, and more specifically, using a fermentation waste (solid content such as fiber, wood, etc.), which is a natural vegetable fermentation (enzyme) substance classified as a waste material. It is intended to produce natural cosmetics.

Cosmetic raw material extract according to the present invention, the natural plant extract fermentation ripening material is composed of the raw material as 95% by weight of the natural plant extract residue composed of 80% by weight of fiber and solids, 15% by weight of the fermentation broth, extracting the natural plant As a subsidiary material to be mixed with the residue, 1.0% by weight of natural and synthetic cosmetics thickener, 1.0% by weight of food thickener, 0.7% by weight of tocopherol, 0.9% by weight of retinol, 0.9% by weight of arbutin, 0.3% by weight of collagen, 0.2 natural preservatives It is characterized in that it is made by mixing with the raw material by selecting the weight percentage as a subsidiary material. Another feature of the present invention is the step of fermenting and aging the natural plant processing to 95% by weight of residue consisting of 80% by weight of fiber and wood solids and 15% by weight stock solution; Squeezing the processed debris from the above step by squeezing fibrous and wood solids with a compactor, leaving 15% by weight of the stock solution; A grinding step of grinding the residue into particles of 60 to 1000 mesh through a grinder; Characterized in that the method for producing a cosmetic raw material extract consisting of a step of blending 5% by weight of the subsidiary material to the coarse dregs to produce a cosmetic raw material.

Description

Ingredient extract for cosmetics and manufacturing method

The present invention relates to a cosmetic raw material extract using natural vegetable fermentation waste and a method for producing the same, and more specifically, using a fermentation waste (solid content such as fiber, wood, etc.), which is a natural vegetable fermentation (enzyme) substance classified as a waste material. It is intended to produce natural cosmetics.

In general, external skin preparations include cosmetics, medicines, and quasi-drugs. Especially, external skin preparations for the purpose of preventing and improving skin aging and damage are conventionally used in combination with various raw materials, starting with raw materials extracted from natural products. For example, ginseng extract, yeast extract, extracts such as pine mushroom extract, natural polymers such as collagen, skin activators such as amino acids and vitamins, or moisturizing agents such as glycerin and 1,3-butylene glycol are used to prevent skin damage. And it has been used in skin cosmetics for the purpose of improvement, but these materials have not been widely used as a skin solvent because they do not overcome the expensiveness such as being rare and also used for some food.

Molecular oxygen is very important to humans and it is difficult to sustain life in the absence of oxygen. However, even though oxygen in the air is not reactive as it is, when it receives energy for a little time, oxygen becomes an electron with an auxiliary electron, and this state is called active oxygen, which reacts with other biological components, organic compounds, and ultimately carbon dioxide and water, Generates and excretes some phosphorus and sulfur oxides. However, small amounts of free radicals react with other biomaterials to act as highly toxic oxides.

On the other hand, various inorganic substances (for example, calcium phosphate, which is a major component of bone) are not affected by oxygen in the air, but, for example, lipids containing fatty acids (or more unsaturated fatty acids) make up the living body. It is very unstable to oxygen in the air, which is essential as a cell membrane component and essential for life support.

Compared with saturated fatty acids, unsaturated fatty acids are easy to oxidize. Unsaturated fatty acids of triene or more are more easily oxidized in proportion to the number of active methylene groups contained in each of diene fatty acids. Eventually, lipid peroxide (ROOH) is produced from lipids to destroy vitamins, inhibit oxygen activity, and destroy cell membranes, resulting in necrosis of cell constituents, leading to aging of the skin or organs. Free radicals are involved in the peroxidation of cell membrane lipids, and lipids are the major targets of free radicals. Irradiation of ultraviolet light creates lipid radicals from unsaturated fatty acids, which rapidly combine with oxygen to form lipid peroxide radicals. Lipid peroxide radicals combine with other unsaturated fatty acids and form lipid peroxides. Lipid peroxidation is also formed from cholesterol. The following is the process.

RH -R

R- + O2 -ROO

ROO- + RH -ROOH- + R

(RH: unsaturated fatty acid, R-: lipid radical,

ROO-: lipid peroxide radical, ROOH-: lipid peroxide)

In general, there are antioxidants such as super oxide dismutase (SOD) in vivo, but these substances are known to have weak activity in skin cells, and in order for us to supply antioxidants from the outside, they must actually be absorbed percutaneously. Plant ingredients are relatively low molecular weight, so the percutaneous absorption is well expected to be expected a lot of efficacy effect on the skin and is actually being studied a lot.

Currently known substances that have an antioxidant effect on plant components are phenolic compounds (flavonoids, lignans, tannins, vitamin E, etc.), pigment compounds belonging to carotenoids, and compounds belonging to saponins.

Therefore, the leaves of natural plants have a large amount of substances that have an antioxidant effect, so there is an advantage that can be easily obtained, but there are some examples of using them as external preparations for skin such as cosmetics, but very little research and limited research has not been commercialized or commercialized It was.

On the other hand, the cause of the change of leaves, such as plants, is not yet fully identified, but in normal natural conditions, it occurs in the order of age, and the leaves at the bottom of the branches are yellowed first, then the leaves at the middle, and finally at the end. The color of young leaves will change. In Korea, in late summer or early autumn, not only the chlorophyll in the leaves of the plant is made, but also the blue pigment already in the leaves is rapidly destroyed. At the same time, the yellow pigment in the leaves begins to appear. By this time, the leaves of the sycamore tree, birch and birch are yellow because the blue pigment that covered the yellow cow disappears during the summer.

Autumn leaves contain yellow and red leaves. The golden yellow color found in the leaves of Ginkgo and Prunus is the combination of yellow pigment and tan pigment, tannin.

On the other hand, red leaves such as maple, shin, and maple leaves and red leaves, various oaks, dogwoods, and maples have red leaves because they produce red pigments. As the color of the plant leaves changes and leaves fall, the blue pigment is destroyed and the yellow pigment, which is hidden, appears clearly, and the new pigment material that has not existed before appears in the leaves. With this change in foliage, yellow pigments, such as carotene and xanthophyll, are always in the leaves along with the blue pigment, which has stability that does not break down under the sun's rays, and these pigments are long after the blue pigment is destroyed. Can remain in the leaves. In fact, leaves such as silver maple, candy maple, beech, blooming, sycamore, birch, and oak are mostly yellow in autumn colors. The red color in autumn does not exist in the leaves but is newly synthesized. It is due to the descent.

Thus, foliage leaves may be edible such as green plants or similar leaves and roots and plants such as dandelion, wild chrysanthemum, brush, wormwood, mulberry leaf, rootroot and its leaves, acacia, forget-me-not, horseradish, motherwort, bellflower, etc. Plants contain many components that are not found in natural leaves due to changes in temperature and external environment, and these components are expected to provide new functions. It has not happened.

Accordingly, an object of the present invention, edible leaves and root plants, such as dandelion, wild chrysanthemum, sol, mugwort, mulberry leaf, rootroot and its leaves, acacia, forget-me-not, horseradish, motherwort, bellflower It is an object to provide a cosmetic raw material extract excellent in various skin improvement effects by applying the extract of edible plants, such as these, to a cosmetic raw material.

Another object of the present invention is to provide a skin cosmetic raw material composition containing a natural plant raw material extract, and to provide a skin raw material anti-aging cosmetic raw material extract containing a natural plant raw material extract.

Still another object of the present invention is to provide a cosmetic raw material extract, which can be used for nutritional and moisturizing packs and related massages.

Still another object of the present invention is edible leaves and root plants, which are natural plants with excellent stability, such as dandelion, wild chrysanthemum, sol, mugwort, mulberry leaf, rootroot and its leaves, acacia, forget-me-not, horseradish, motherwort, bellflower It is to provide a cosmetic raw extract manufacturing method for applying the extract of the edible plant such as cosmetic raw materials.

Cosmetic raw material extract according to the present invention for achieving the above object, the natural plant extract fermentation ripening material composed of raw materials as 95% by weight of natural plant extract residue composed of 80% by weight of fiber and solid content, 15% by weight of fermentation broth. And, as a subsidiary material to be mixed in each of the natural plant extract residue, 1.0% by weight of natural and synthetic cosmetics thickener, 1.0% by weight of food thickener, 0.7% by weight of tocopherol, 0.9% by weight of retinol, 0.9% by weight of arbutin, collagen 0.3 Weight%, 0.2% by weight of a natural preservative is selected as a subsidiary material, characterized in that made by mixing with the raw materials.

       Other features of the present invention, natural fermentation of edible natural plants, such as dandelion, wild chrysanthemum, brush, mugwort, mulberry leaves, roots and its leaves, acacia, forget-me-not, horseradish, motherwort, bellflower, etc. Processing to 95% by weight of residues comprising 15% by weight and 15% by weight of the stock solution;

Squeezing the processed debris from the above step by squeezing fibrous and wood solids with a compactor, leaving 15% by weight of the stock solution;

A grinding step of grinding the residue into particles of 60 to 1000 mesh through a grinder;

Characterized in that the method for producing a cosmetic raw material extract consisting of a step of blending 5% by weight of the subsidiary material to the coarse dregs to produce a cosmetic raw material.

Natural edible stems, roots and leaves of edible wild and cultivated plants, in particular, are distributed in a variety of plants throughout the country, easy to harvest and can be obtained easily anywhere. For example, green plants or similar leaves and roots and plants are broadly included. Edible plants such as dandelion, wild chrysanthemum, sol, wormwood, mulberry leaf, rootroot and its leaves, acacia, forget-me-not, horseradish, motherwort, bellflower, etc. It contains many ingredients that cannot be seen, and it is expected that these ingredients may provide new functions, but there have been no reports of extracting them and applying them to cosmetic raw materials. Collected to prepare a cosmetic raw material extract.

The cosmetic raw material extract was selected as the raw material of 95% by weight of natural plant extracts composed of 80% by weight of natural plants to ferment the natural substance to fiber and solids, 15% by weight of fermentation broth.

As a subsidiary material mixed with the raw materials, 1.0% by weight of natural and synthetic cosmetic thickeners, 1.0% by weight of food thickeners, 0.7% by weight of tocopherols, 0.9% by weight of retinol, 0.9% by weight of arbutin, collagen mixed with natural plant extract residues 0.3% by weight and 0.2% by weight of natural preservative were selected and mixed with the raw materials.

(1) The composition of raw materials constituting the cosmetic raw material extract was as shown in Table 1 below.

Raw materials (natural plant extract residue) Fibrin and Solids Fermentation broth Sum 80 wt% 15 wt% 95 wt%
Here, the natural plant as a raw material is edible natural plants such as dandelion, wild chrysanthemum, brush, mugwort, mulberry leaf, rootroot and its leaves, acacia, forget-me-not, horseradish, motherwort, bellflower, etc. Natural fermentation was carried out for 24 hours at a temperature of 50 ℃.

(2) The composition of the submaterial constituting the cosmetic raw material extract was as shown in Table 2 below.

          Subsidiary Material (Additive Mixture)  Thickeners for natural and synthetic cosmetics  1.0 wt%  Food Thickener  1.0 wt%  Tocopherol  0.7 wt%  Retinol  0.9 wt%  Arbutin  0.9 wt%  Collagen  0.3 wt%  Natural preservative  0.2 wt%

The mixing and composition ratio of the raw materials and subsidiary materials may be achieved by adjusting the mixing ratio according to the ratio obtained through several repeated experiments or the age, climatic conditions and environment of the user, but is preferably adjusted based on the above ratio. .

Method for producing a cosmetic raw material extract of the present invention as described above was as follows. Natural fermentation of natural plants and processing of solid wastes of fiber and wood are carried out, and the processed residues are squeezed with a compressor, leaving 15% by weight of the undiluted solution. After pulverizing into 1000 mesh particles to form raw materials, 1.0% by weight of natural and synthetic cosmetics thickener, 1.0% by weight of food thickener, 0.7% by weight of tocopherol, 0.9% by weight of retinol, 0.9% by weight of arbutin, 0.3% by weight of collagen, and 0.2% by weight of natural preservatives were mixed with the raw materials to prepare an extract as a cosmetic raw material.

The thickener was selected from among natural thickeners and cosmetic thickeners, and commonly used thickeners were mixed.

Lab-level experiments were conducted to examine the survival rate of fibroblasts that form the dermal tissue of the skin and to measure the antioxidant effect of eliminating free radicals. .

As a result, it showed an excellent effect as a skin external preparation, especially a cosmetic.

The cosmetic raw material extract prepared according to the present invention was found to easily reach to the polar layer, which is an intermediate layer of the skin epidermis, on the skin tissue. In other words, it penetrates into the stratum corneum, granule layer, and polar layer to provide excellent moisturizing and nutrient supply to skin tissue.

These results indicate that the natural plant extract fermentation broth and ground solids change the material from the high molecular material to the low molecular material during the fermentation process and the natural plant itself. Pigments have stability that is not destroyed in sunlight, and these pigments increase the constituent stability of the plant, which is a raw material during the ripening fermentation of the plant, as well as can remain in the leaves for a long time after the blue pigment is destroyed. The functional pharmacological action of natural plants is expected to affect the skin tissue. Particularly, the solid residue is applied to the skin by applying microelements such as vitamins and minerals to form a skin membrane without flowing down for a certain period of time. When fermentation of natural plants, the color changes as if the leaves fall on the leaves. This color does not exist in the leaves before, but is newly synthesized, depending on the change of temperature or the change of environment. For reference, in the present invention, as the fermentation ripens natural plants, the color ranges from yellow and brown to black based, which is mainly close to gray. This depends on the natural plant properties used. If only roots are used, the color will be close to black, and using only blue plant leaves can range from yellow to brown.

On the other hand, the natural plant extract according to the present invention is suitable for the skin cosmetic formulation amount of about 95% by weight (fiber and solids 80% by weight, undiluted 15% by weight) bar, greatly deviating from this standard to improve the skin effect It is difficult to expect, and too much content did not increase the effect even if combined more.

In addition, the extract of the present invention is easily mixed with water, while it is difficult to be mixed with fats and oils and organic solvents, but it can be blended into the skin cosmetic even in a suspended state and does not have any effect on the effect.

In addition, the extract according to the present invention is suitable to be used as skin cosmetics, and common ingredients, such as oil, water, surfactants, moisturizers, lower alcohols, thickeners, chelating agents, pigments, preservatives, fragrances, etc. It is also possible to formulate as much as necessary.

Hereinafter, the present invention will be described in detail by examples of the present invention. The examples are illustrative of the present invention and the scope of the present invention is not limited to the examples.

Example 1

-Fermented and matured natural plants, 95% raw material extract consisting of 80% by weight of fiber and solid content, 15% by weight of fermentation broth-

(1) Commonly growing crops and wild natural plants were harvested and fermented to produce 95% by weight of residue.

(2) looked at the antioxidant effect of the extract according to the present invention.

In order to measure the antioxidant effect in the present invention, after measuring the active oxygen produced by xanthine and xanthine oxidase by NBT method, the test substance evaluates the effect of removing the active oxygen, that is, the effect of removing the active oxygen, Skin anti-wrinkle and anti-inflammatory effects were examined.

After generating free radicals by xanthine and xanthine oxidase, the amount of free radicals was measured by reacting with nitroblue tetrazolium (NBT) and measuring the blue color produced thereby. The sample used in the fermentation ripened plant was in the state of dregs, and the extract of fermentation showed the stronger antioxidant effect of the fermented fermented state.

On the other hand, various test methods have been introduced to prove the efficacy of various plant extracts, but among them, the method using cultured cells has been used in many fields because it can accurately determine the action of the test substance.

In the present invention, the cell proliferation rate of cultured mouse skin fibroblasts was measured by the MTT reduction method in order to measure the cell proliferation effect of the fermented and aged plant extract, and this action was compared with other extracts. When the substance called 'empty' is reduced by N.D.H enzyme, which is present in the intracellular mitochondria, the blue color is used. This blue amount indicates the amount and metabolic activity of mitochondria. The stronger the blue color, the higher the activity of the cell. As a result, the effect of proliferating fibroblasts from the fermented and aged plant extracts was confirmed. In addition, when compared with the green leaf extract of the plant before fermentation fermentation of the same concentration, the leaves of fermented ripening plants showed more than 40% cell growth rate compared to the control group without any treatment, and the general green leaf extract compared to the control group The cell growth of fermented and matured plant leaves showed high 23% growth rate, suggesting that it can help to maintain healthy skin with the activity of skin cells, and by supplying a large amount of elements such as vitamins and minerals It has been suggested that the elements can form a skin membrane to enable skin moisturization and active nutrition.

Example 2

-Fermentation ripening of natural plants, cosmetic raw material extract mixed with subsidiary material with 95% raw material extract consisting of 80% by weight of fiber and solid content, 15% by weight of fermentation broth-

 Commonly grown crops and wild natural plants are collected, fermented and matured to form 95% by weight of residues to form raw materials.As a raw material, 1.0% by weight of natural and synthetic cosmetic thickeners, 1.0% by weight of food thickeners, 0.7% by weight of tocopherol, 0.9% by weight of retinol, 0.9% by weight of arbutin, 0.3% by weight of collagen, and 0.2% by weight of natural preservative were mixed with the raw materials to prepare an extract as a cosmetic raw material. Here, the ingredients used have been verified that the stability is generally selected as an edible ingredient that is commonly used as food ingredients as a cosmetic component. However, these components may be composed of a large amount of ingredients, but they are expensive and can not be used indefinitely, so that only a small amount of subsidiary materials are used to form a cosmetic raw material.

The cosmetic raw material extract thus produced was found to have excellent skin color improvement, antioxidant effect, and anti-aging and whitening effect of the raw material, and was found to be particularly stable and suitable for use as a raw material or massage material for moisturizing packs. It became.

As described above, the cosmetic raw material extract according to the present invention is stable as a natural product and, when applied to cosmetics, exhibits an excellent moisturizing effect on the skin and can supply moisturizing and sufficient nutrition to the skin surface. It can be widely used as a material, and it can supply the skin with abundant trace elements such as vitamins and minerals that plants have, and it can prevent skin aging and whitening by improving skin color and antioxidant effect. Therefore, there is an effect that can provide a high quality, high functional cosmetic raw material at low cost.

Claims (4)

delete delete       80% by weight of fiber and wood solids and raw stock 15% of edible natural plants mixed with edible natural plants consisting of dandelion, wild chrysanthemum, brush, mugwort, mulberry leaves, root roots and leaves, acacia, forget-me-not, horseradish, motherwort and bellflower Processing to 95% by weight of debris; Squeezing the processed debris from the above step by squeezing fibrous and wood solids with a compactor, leaving 15% by weight of the stock solution; A grinding step of grinding the residue into particles of 60 to 1000 mesh through a grinder; Comprising the 5% by weight of the subsidiary material to the coarse residue after the pulverization step is made of a cosmetic raw material, the thickener included in the subsidiary material is characterized in that to use selected from natural thickeners or cosmetic thickeners Cosmetic raw material extract manufacturing method.      80% by weight of fiber and wood solids and raw stock 15% of edible natural plants mixed with edible natural plants consisting of dandelion, wild chrysanthemum, brush, mugwort, mulberry leaves, root roots and leaves, acacia, forget-me-not, horseradish, motherwort and bellflower Processing to 95% by weight of debris; Squeezing the processed debris from the above step by squeezing fibrous and wood solids with a compactor, leaving 15% by weight of the stock solution; A grinding step of grinding the residue into particles of 60 to 1000 mesh through a grinder; It is made of a step of preparing a cosmetic raw material by blending 5% by weight of the subsidiary material to the coarse dregs,        The thickener included in the subsidiary material is selected from among natural thickeners or cosmetic thickeners, and the submaterial is 1.0 wt% of natural and synthetic cosmetic thickeners, 1.0 wt% of food thickeners and 0.7 wt% of tocopherols. , 0.9% by weight of retinol, 0.9% by weight of arbutin, 0.3% by weight of collagen, 0.2% by weight of a natural preservative, a method of producing a cosmetic raw material extract.