KR0123840B1 - Process making of feed in fish oil - Google Patents
Process making of feed in fish oilInfo
- Publication number
- KR0123840B1 KR0123840B1 KR1019940018503A KR19940018503A KR0123840B1 KR 0123840 B1 KR0123840 B1 KR 0123840B1 KR 1019940018503 A KR1019940018503 A KR 1019940018503A KR 19940018503 A KR19940018503 A KR 19940018503A KR 0123840 B1 KR0123840 B1 KR 0123840B1
- Authority
- KR
- South Korea
- Prior art keywords
- fish oil
- parts
- feed
- weight
- water
- Prior art date
Links
- 235000021323 fish oil Nutrition 0.000 claims abstract description 53
- 150000003904 phospholipids Chemical class 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 11
- 239000006227 byproduct Substances 0.000 claims abstract description 10
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004202 carbamide Substances 0.000 claims abstract description 4
- 239000003054 catalyst Substances 0.000 claims abstract description 4
- 239000000203 mixture Substances 0.000 claims abstract 4
- 238000001816 cooling Methods 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 5
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 4
- 230000001877 deodorizing effect Effects 0.000 claims description 4
- 238000009938 salting Methods 0.000 claims description 4
- 239000000292 calcium oxide Substances 0.000 claims description 2
- 235000012255 calcium oxide Nutrition 0.000 claims description 2
- 238000000227 grinding Methods 0.000 claims description 2
- 238000007127 saponification reaction Methods 0.000 claims description 2
- 238000010025 steaming Methods 0.000 claims description 2
- 238000004332 deodorization Methods 0.000 abstract description 5
- 238000000855 fermentation Methods 0.000 abstract description 3
- 230000004151 fermentation Effects 0.000 abstract description 3
- 235000008733 Citrus aurantifolia Nutrition 0.000 abstract 1
- 235000011941 Tilia x europaea Nutrition 0.000 abstract 1
- 239000004571 lime Substances 0.000 abstract 1
- 241000251468 Actinopterygii Species 0.000 description 8
- MBMBGCFOFBJSGT-KUBAVDMBSA-N all-cis-docosa-4,7,10,13,16,19-hexaenoic acid Chemical compound CC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CCC(O)=O MBMBGCFOFBJSGT-KUBAVDMBSA-N 0.000 description 6
- 235000019688 fish Nutrition 0.000 description 6
- 239000002994 raw material Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- JAZBEHYOTPTENJ-JLNKQSITSA-N all-cis-5,8,11,14,17-icosapentaenoic acid Chemical compound CC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CCCC(O)=O JAZBEHYOTPTENJ-JLNKQSITSA-N 0.000 description 3
- 230000006866 deterioration Effects 0.000 description 3
- 235000020669 docosahexaenoic acid Nutrition 0.000 description 3
- 229940090949 docosahexaenoic acid Drugs 0.000 description 3
- 235000020673 eicosapentaenoic acid Nutrition 0.000 description 3
- 229960005135 eicosapentaenoic acid Drugs 0.000 description 3
- JAZBEHYOTPTENJ-UHFFFAOYSA-N eicosapentaenoic acid Natural products CCC=CCC=CCC=CCC=CCC=CCCCC(O)=O JAZBEHYOTPTENJ-UHFFFAOYSA-N 0.000 description 3
- 238000003672 processing method Methods 0.000 description 3
- 241000283690 Bos taurus Species 0.000 description 2
- 229940013317 fish oils Drugs 0.000 description 2
- 244000144972 livestock Species 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 150000002978 peroxides Chemical class 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 241000555825 Clupeidae Species 0.000 description 1
- 241001149724 Cololabis adocetus Species 0.000 description 1
- 241000282849 Ruminantia Species 0.000 description 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 230000007123 defense Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 235000013310 margarine Nutrition 0.000 description 1
- 239000003264 margarine Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000000306 recurrent effect Effects 0.000 description 1
- 235000019512 sardine Nutrition 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/20—Animal feeding-stuffs from material of animal origin
- A23K10/22—Animal feeding-stuffs from material of animal origin from fish
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/10—Animal feeding-stuffs obtained by microbiological or biochemical processes
- A23K10/12—Animal feeding-stuffs obtained by microbiological or biochemical processes by fermentation of natural products, e.g. of vegetable material, animal waste material or biomass
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/24—Compounds of alkaline earth metals, e.g. magnesium
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K40/00—Shaping or working-up of animal feeding-stuffs
- A23K40/25—Shaping or working-up of animal feeding-stuffs by extrusion
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Animal Husbandry (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- Molecular Biology (AREA)
- Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- Physiology (AREA)
- Marine Sciences & Fisheries (AREA)
- Inorganic Chemistry (AREA)
- Sustainable Development (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Fats And Perfumes (AREA)
Abstract
Description
본 발명은 어유(漁油)를 주원료로 사는 사료 제조방법에 관한 것으로서, 특히 DHA(Docosa Hexaenoic Acid) 및 EPA(Eicosa Pentaenoic Acid)를 다량 함유하고 있는 어종을 가공하여 얻은 어유를 주원료로 하되, 어유를 다시 분말화하여 사료로 이용하고자 하는 것이다.The present invention relates to a feed production method of buying fish oil as a main raw material, and in particular, fish oil obtained by processing fish species containing a large amount of DHA (Docosa Hexaenoic Acid) and EPA (Eicosa Pentaenoic Acid) as a main raw material, Is to be used again as a feed powder.
지금까지 어유는 사료로서 이용하지 못하고 어유를 경화 처리하여 식용마아가린이나 비누제조등에 이용하고 있는 정도로서, 어유를 사료로서 이용하지 못하고 있는 가장 큰 이유중 하나는 어유가 가지고 있는 독특한 냄새 즉, 어취(漁臭)를 쉽게 제거하지 못한 문제점과 또 어유는 쉽게 변질하기 때문에 사료로 이용하기에는 또다른 가공 공정이 필요할 뿐 아니라 소, 젖소등과 같은 반추동물에게는 소화기능상 어유 자체를 직접 사료로 이용할 수 없는 등 해결해야 할 많은 문제점이 있었다.Until now, fish oil is not used as feed, but cured fish oil is used in food margarine or soap manufacturing, and one of the biggest reasons why fish oil is not used as feed is the unique smell of fish oil, that is, 문제점) The problem of not being easily removed and fish oil is easily deteriorated, so it is not only necessary to use another processing step for feed, but also for ruminants such as cattle, cows, etc. There were many problems to do.
본 출원인은 상기한 문제점의 해결수단으로서, 어유에 포함된 어취를 제거하기 위해 MSG부산물을 이용한 어유의 탈취 가공 방법을 특허출원하여 특허(공고번호 제 93-779호, 93. 2. 4일)된 바 있다.Applicant has applied for a deodorization processing method of fish oil using MSG by-products to remove the fish odor contained in the fish oil as a means of solving the above problems (Notification No. 93-779, February 4, 93) It has been.
상기한 특허에서 발명한 어유의 탈취 가공 방법은, 어유에 함유되어 있는 어취의 근본원인인 인지질을 제거하기 위하여 M.S.G(Mono Sodium Gulutamate) 부산물을 물과 같이 어유에 투입하고 가열하면 M.S.G내의 수용성 단백질에 의하여 어유의 유용성 인지질을 수용성으로 전위시켜 주고, 이 전위된 수용성 인지질을 정체 분리 방법에 의해 어유와 분리시켜 순수한 어유의 지방이 상층부로 부상하게 한 후, 이를 제거함으로서 어유내의 포함되어 있는 인지질을 호과적으로 완벽하게 제거시켜주고, 인지질이 제거된 어유를 진공예열, 수증기중류에 의한 진공탈취하여 불포화 저급지방산을 제거하여 진공냉각시켜 정체 처리 완료하고, 완료처리한 후 20일이 경과한 후에도 과산화물가(P.O.V)가 kg당 10밀리몰(10M/kg) 정도에 지나지 않게 되므로 재발성 악취가 전혀 발생되지 않아 어취의 환원 즉 어취의 변질이 이루어지지 않게 되어 양질의 어류를 얻을 수 있게 되는 것이다.The deodorization processing method of fish oil invented in the above patent is to remove the phospholipids, which is the root cause of fish odor contained in fish oil, by adding MSG (Mono Sodium Gulutamate) by-product to fish oil like water and heating to water-soluble protein in MSG. By dissolving the useful phospholipid of fish oil into water soluble, and separating the displaced soluble phospholipid from fish oil by stagnation separation method, the fat of pure fish oil rises to the upper part, and then removes the phospholipid contained in fish oil. Completely remove the excess oil and remove the phospholipids from the fish oil by vacuum preheating and vacuum deodorization by steam midstream to remove unsaturated lower fatty acids and vacuum-cooling to complete the stagnation treatment. POV) is only about 10 millimoles per kilogram (10 M / kg), so no recurrent odor occurs It is not possible to reduce the smell of fish, that is, the deterioration of the fish will not be able to obtain a good quality fish.
이와 같이 어유에 M.S.G부산물을 가하여 인지질을 제거한 후 상기와 같이 진공예열, 진공탈취 밀 냉각 공정등의 과정을 거쳐 산가 등을 현저히 저하시켜 주므로서, 간단한 작업공정으로 어유에 포함된 어취의 제거작업을 극히 염가로서 완벽하게 처리할 수 있게 되었고, 저가의 과산화물가(P.O.V)를 장시간 유지시켜 주게 됨으로서 장기보존 및 안전성을 향상시켰다.In this way, MSG by-products are added to fish oil to remove phospholipids, and as a result, the acid value of the fish oil is remarkably lowered through vacuum preheating, vacuum deodorizing mill cooling, and the like. It is extremely inexpensive and can be completely processed. The long-term maintenance of low-cost peroxide (POV) has been improved for long-term preservation and safety.
본 발명은 상술한 바와 같이 지금까지 어유를 사료로 이용할 수 없었던 어유에 포함된 어취 제거 및 변질 문제를 저가로 그리고 완벽하게 해결한 상기 특허를 기술적 배경으로 하고 있으며, 나아가 다른 사료와 배합하여 이용할 수 있도록 상기 어유를 분말화하고자 하는 것이다.The present invention has the technical background of the above-mentioned patent that solves the problem of removing fish smell and deterioration contained in fish oil which has not been available as fish oil as feed as described above, and can be used in combination with other feeds. It is intended to powder the fish oil so that.
다시 말하면 본 발명은 어유의 냄새를 제거하고 변질을 방지한 선특허 MSG 부산물을 이용한 어유의 탈취 가공방법에 의한 어유를 생성하는 과정에서 어유를 다시 분말화하는 새로운 과정을 제공함을 특징으로 하는 어유를 주원료로 한 사료 제조방법에 관한 것으로서, M.S.G 부산물과 함께 요소(Urea)를 첨가하여 발효시키는 과정과 발표된 어유에 포함된 물 및 인지질을 분리제거하는 과정, 분리된 어유에 생석회를 첨가하여 검화 및 염석시키는 과정을 거쳐 냉각시킨 후 냉각 롤라 또는 압출기등을 이용하여 분말화한 사료를 얻는 것이다.In other words, the present invention provides a new process for powdering the fish oil in the process of producing fish oil by the deodorization processing method of fish oil using the patented MSG by-product to remove the smell of fish oil and prevent deterioration The present invention relates to a method of preparing feed as a main raw material, which includes fermentation by adding urea with MSG by-products, separating and removing water and phospholipids contained in published fish oils, and adding saponification to the separated fish oils. After cooling through salting, the powdered feed is obtained using a cooling roll or an extruder.
이와 같은 과정을 거친 분말화된 사료는 다른 종류의 사료와 적당량 배합하여 사료로서 가축을 사육하는데 사용하는 것이다.The powdered feed that has undergone this process is used to raise livestock as feed in combination with other types of feed.
이상 설명한 본 발명의 어유를 주성분으로 한 사료 제조방법을 좀더 구체적으로 설명하면,When explaining the feed production method based on the fish oil of the present invention as described above in more detail,
(제1공정)(Step 1)
MSG 부산물을 이용한 어유를 탈취 가공하는 과정중 어유 100중량부에 물 60중량부 및 MSG부산물 20중량부의 비율로 교반기에 투입혼합하여 서서히 온도를 상승시켜 가열교반하되, 상기 혼합물의 온도가 40℃이상이 되면 촉매로서 온도를 어유중량비 100중량부에 대해 1.5-2.0중량부되게 첨가하여 95℃ 될때까지 계속 가열교반하면서 1시간 정도 교반증숙하여 발효시킨다.During the process of deodorizing fish oil using MSG by-products, 100 parts by weight of fish oil was mixed with a stirrer at a ratio of 60 parts by weight of water and 20 parts by weight of MSG by-products, and then gradually heated and stirred by heating to a temperature. In this case, the temperature is added 1.5-2.0 parts by weight to 100 parts by weight of fish oil as a catalyst, followed by fermentation by stirring and steaming for about 1 hour while continuously heating and stirring until it reaches 95 ° C.
이때 첨가된 요소는 MSG의 수용성 단백질과 어유내에 함유되어 있는 유용성 인지질이 서로 반응발효하여 어유의 유용성 인지질을 수용성으로 전위시키는 과정을 촉진시키는 촉매의 역할을 하게 되는 것이다.At this time, the added urea acts as a catalyst to promote the process of translating the oil-soluble phospholipids into water-soluble by the water-soluble protein of MSG and oil-soluble phospholipid contained in fish oil.
(제2공정)(2nd step)
이와 같이 발효된 어유는 다시 원심분리기로 어유에 포함된 물 및 인지질을 분리제거하므로서 완전탈취 및 정제된 순수한 어유를 얻는 것이다.The fish oil fermented in this way is obtained by completely deodorizing and purified pure fish oil by separating and removing the water and phospholipid contained in the fish oil by centrifugation again.
(제3공정)(3rd step)
그리고 상기 제1 및 제2공정을 거쳐 얻어진 인지질이 제거된 순수한 어유를 분말사료화하기 위한 공정으로서, 어유 100중량부에 물 50중량부 및 생석회 15중량부를 첨가하여 검화 및 염석시키는 과정을 거쳐 다시 냉각처리한 후 압축기 또는 냉각롤러로서 분말화하므로서 어유를 주원료로 하는 분말화된 사료를 얻게 되는 것이다.In addition, as a process for powder-feeding pure fish oil from which the phospholipids obtained through the first and second processes have been removed, 50 parts by weight of water and 15 parts by weight of quicklime are added to 100 parts by weight of fish oil, and then cooled again by salting and salting. After processing, the powdered powder is compressed into a compressor or a cooling roller to obtain a powdered feed containing fish oil as a main raw material.
그리고 본 발명의 어유는 DHA 및 EPA를 비교적 많이 함유하고 있는 어종으로 알려진 참치, 정어리, 방어, 꽁치 등을 대상으로 하고 있으나 상기한 어종의 어유를 한정하는 것은 아니다.And the fish oil of the present invention targets the tuna, sardines, defense, saury, etc. known as a fish species containing a relatively high DHA and EPA, but does not limit the fish oil of the above species.
이와 같은 본 발명의 어유를 주원료로한 사료 제조방법은 간단한 공정으로 어유를 사료로 이용하지 못한 문제점을 분말화하는 공정으로 해결하고 있을 뿐만 아니라 본 발명의 어유를 분말화한 사료와 다른 사료와를 배합하여 가축을 사육한다면 저렴한 가격으로 사료의 다양한 선택을 할 수 있는 것이다.Such a feed production method using the fish oil of the present invention as a main raw material not only solves the problem of not using fish oil as a feed in a simple process, but also the feed and powdered fish oil powder of the present invention and other feed If you raise livestock in combination, you can choose a variety of feed at a low price.
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1019940018503A KR0123840B1 (en) | 1994-07-28 | 1994-07-28 | Process making of feed in fish oil |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1019940018503A KR0123840B1 (en) | 1994-07-28 | 1994-07-28 | Process making of feed in fish oil |
Publications (2)
Publication Number | Publication Date |
---|---|
KR960003593A KR960003593A (en) | 1996-02-23 |
KR0123840B1 true KR0123840B1 (en) | 1997-11-20 |
Family
ID=19389196
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019940018503A KR0123840B1 (en) | 1994-07-28 | 1994-07-28 | Process making of feed in fish oil |
Country Status (1)
Country | Link |
---|---|
KR (1) | KR0123840B1 (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20020051903A (en) * | 2002-05-07 | 2002-06-29 | 김철곤 | A method for manufacturing refined fish oil |
KR101439419B1 (en) * | 2013-05-15 | 2014-09-11 | 이완희 | Method of extracting tunny oil |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100581076B1 (en) * | 2004-12-28 | 2006-05-16 | 주식회사 마니커 | Purified fish oil, broiler feed composition and use thereof for producing DHA-rich meat |
-
1994
- 1994-07-28 KR KR1019940018503A patent/KR0123840B1/en not_active IP Right Cessation
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20020051903A (en) * | 2002-05-07 | 2002-06-29 | 김철곤 | A method for manufacturing refined fish oil |
KR101439419B1 (en) * | 2013-05-15 | 2014-09-11 | 이완희 | Method of extracting tunny oil |
Also Published As
Publication number | Publication date |
---|---|
KR960003593A (en) | 1996-02-23 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US5696278A (en) | Degumming of crude glyceride oils not exposed to prior enzymatic activity | |
DE3751599T2 (en) | EXTRACTION PROCEDURE OF PLANT OIL. | |
CN1266260C (en) | Purifying crude pufa oils | |
DE60018053T2 (en) | METHOD FOR PRODUCING A PANS THROUGHOUT FEED ADDITIVE | |
CA2383537C (en) | Method for manufacturing fatty acid calcium salts from high glyceride content oils | |
CN102334563A (en) | Method for controlling content of 3-chloro-1,2-propanediol or ester thereof in oil | |
RU2383586C1 (en) | Method for production of calcium soaps for animal feeds | |
DE69906089T2 (en) | METHOD FOR CONVERTING PHYTATE IN INORGANIC PHOSPHATE | |
JP3631465B2 (en) | Method for producing refined fish oil | |
US6111120A (en) | Method of refining oils and fats | |
KR0123840B1 (en) | Process making of feed in fish oil | |
US5693358A (en) | Animal feed manufacturing method based on fish oil | |
JPS59113099A (en) | Highly unsaturated oil composition | |
JPH02234684A (en) | Production method of fatty acid calcium salt | |
JPH08275734A (en) | Production of feed additive | |
AU778384B2 (en) | Method for manufacturing fatty acid calcium salts from high glyceride content oils | |
Shivashankar et al. | Chapter-6 Processing of Oil Palm Bunches and Valorization of Oil Palm Biomass | |
JPS59172596A (en) | Purified fish oil and manufacture | |
KR900004518B1 (en) | Manufacturing method of plant oil | |
US2121545A (en) | Art of refining edible oils, fats and analogous products | |
RU2158752C1 (en) | Method of preparing vegetable oil processing products | |
KR20020051903A (en) | A method for manufacturing refined fish oil | |
SU1763476A1 (en) | Method of soap preparation from fat-containing waste | |
EP1218680A1 (en) | Method for drying particulate substances or mixtures thereof | |
CA2346407A1 (en) | Process of converting rendered triglyceride oil from marine sources into bland, stable oil |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A201 | Request for examination | ||
PA0109 | Patent application |
Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19940728 |
|
PA0201 | Request for examination |
Patent event code: PA02012R01D Patent event date: 19940728 Comment text: Request for Examination of Application |
|
PG1501 | Laying open of application | ||
E902 | Notification of reason for refusal | ||
PE0902 | Notice of grounds for rejection |
Comment text: Notification of reason for refusal Patent event date: 19970423 Patent event code: PE09021S01D |
|
E701 | Decision to grant or registration of patent right | ||
PE0701 | Decision of registration |
Patent event code: PE07011S01D Comment text: Decision to Grant Registration Patent event date: 19970814 |
|
GRNT | Written decision to grant | ||
PR0701 | Registration of establishment |
Comment text: Registration of Establishment Patent event date: 19970919 Patent event code: PR07011E01D |
|
PR1002 | Payment of registration fee |
Payment date: 19970919 End annual number: 3 Start annual number: 1 |
|
PG1601 | Publication of registration | ||
PR1001 | Payment of annual fee |
Payment date: 20000919 Start annual number: 4 End annual number: 4 |
|
PR1001 | Payment of annual fee |
Payment date: 20010919 Start annual number: 5 End annual number: 5 |
|
PR1001 | Payment of annual fee |
Payment date: 20020919 Start annual number: 6 End annual number: 6 |
|
PR1001 | Payment of annual fee |
Payment date: 20030922 Start annual number: 7 End annual number: 7 |
|
PR1001 | Payment of annual fee |
Payment date: 20040921 Start annual number: 8 End annual number: 8 |
|
FPAY | Annual fee payment |
Payment date: 20050909 Year of fee payment: 9 |
|
PR1001 | Payment of annual fee |
Payment date: 20050909 Start annual number: 9 End annual number: 9 |
|
LAPS | Lapse due to unpaid annual fee | ||
PC1903 | Unpaid annual fee |
Termination category: Default of registration fee Termination date: 20070810 |