JPS6451328A - Production of cuprous chloride having high purity - Google Patents
Production of cuprous chloride having high purityInfo
- Publication number
- JPS6451328A JPS6451328A JP20481487A JP20481487A JPS6451328A JP S6451328 A JPS6451328 A JP S6451328A JP 20481487 A JP20481487 A JP 20481487A JP 20481487 A JP20481487 A JP 20481487A JP S6451328 A JPS6451328 A JP S6451328A
- Authority
- JP
- Japan
- Prior art keywords
- soln
- cuprous chloride
- filtrate
- chloride
- contg
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
- ing And Chemical Polishing (AREA)
Abstract
PURPOSE:To obtain cuprous chloride having high purity with a simple apparatus by adding iron to an aq. soln. contg. cupric chloride under a specified condition to produce a soln. of cuprous chloride, by filtering, by diluting the filtrate with water while maintaining the filtrate at a specified pH and by washing the deposited cuprous chloride with diluted acid. CONSTITUTION:The content of free hydrochloric acid in the aq. soln. contg. cupric chloride is regulated to 10-110g/l, and iron, copper, zinc or Al is added and reacted at 50-100 deg.C the temp. of the soln. to produce copper(I)chloro complex soln. The reaction soln. is filtered under keeping warm to remove undissolved residue and the filtrate is diluted with pure water to about 5-10 times to deposit cuprous chloride alone while keeping the pH of the filtrate at <=3. The deposited cuprous chloride is filtered and washed with diluted acid (preferably hydrochloric acid) having <=3 pH to obtain the cuprous chloride crystal having high purity. In this case, the cost can be reduced by using waste water produced in etching copper plate in place of the soln. contg. cupric chloride and scrap, cutting waste, etc., in place of reducing agent such as iron.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP20481487A JPS6451328A (en) | 1987-08-18 | 1987-08-18 | Production of cuprous chloride having high purity |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP20481487A JPS6451328A (en) | 1987-08-18 | 1987-08-18 | Production of cuprous chloride having high purity |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS6451328A true JPS6451328A (en) | 1989-02-27 |
JPH0331645B2 JPH0331645B2 (en) | 1991-05-08 |
Family
ID=16496818
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP20481487A Granted JPS6451328A (en) | 1987-08-18 | 1987-08-18 | Production of cuprous chloride having high purity |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6451328A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100380031B1 (en) * | 2000-04-08 | 2003-04-14 | 서안켐텍 주식회사 | Process for preparing cuprous chloride from cupric chloride waste |
KR100390589B1 (en) * | 2000-09-14 | 2003-07-07 | 서안켐텍 주식회사 | Process for preparing cuprous chloride from cupric chloride waste |
KR101030080B1 (en) * | 2009-02-03 | 2011-04-19 | (주)에이치에스켐텍 | Method and system for preparing copper chloride from copper waste liquid |
CN112062148A (en) * | 2020-09-09 | 2020-12-11 | 东华大学 | Method for preparing cuprous chloride by using copper-containing sludge in electroplating circuit board wastewater |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6058169A (en) * | 1983-06-14 | 1985-04-04 | トマス・ジエイ・フオガテイ− | Catheter deflection guide apparatus and method |
JPS6112849A (en) * | 1985-04-19 | 1986-01-21 | Nippon Steel Corp | Reinforced steel bar with excellent low temperature toughness and seawater resistance |
-
1987
- 1987-08-18 JP JP20481487A patent/JPS6451328A/en active Granted
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6058169A (en) * | 1983-06-14 | 1985-04-04 | トマス・ジエイ・フオガテイ− | Catheter deflection guide apparatus and method |
JPS6112849A (en) * | 1985-04-19 | 1986-01-21 | Nippon Steel Corp | Reinforced steel bar with excellent low temperature toughness and seawater resistance |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100380031B1 (en) * | 2000-04-08 | 2003-04-14 | 서안켐텍 주식회사 | Process for preparing cuprous chloride from cupric chloride waste |
KR100390589B1 (en) * | 2000-09-14 | 2003-07-07 | 서안켐텍 주식회사 | Process for preparing cuprous chloride from cupric chloride waste |
KR101030080B1 (en) * | 2009-02-03 | 2011-04-19 | (주)에이치에스켐텍 | Method and system for preparing copper chloride from copper waste liquid |
CN112062148A (en) * | 2020-09-09 | 2020-12-11 | 东华大学 | Method for preparing cuprous chloride by using copper-containing sludge in electroplating circuit board wastewater |
Also Published As
Publication number | Publication date |
---|---|
JPH0331645B2 (en) | 1991-05-08 |
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