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JPS6419057A - Allyl(1-propenyl) disulfide and production thereof - Google Patents

Allyl(1-propenyl) disulfide and production thereof

Info

Publication number
JPS6419057A
JPS6419057A JP62174007A JP17400787A JPS6419057A JP S6419057 A JPS6419057 A JP S6419057A JP 62174007 A JP62174007 A JP 62174007A JP 17400787 A JP17400787 A JP 17400787A JP S6419057 A JPS6419057 A JP S6419057A
Authority
JP
Japan
Prior art keywords
formula
halogenating agent
allyl
methyl
expressed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP62174007A
Other languages
Japanese (ja)
Inventor
Tokiyuki Hiramitsu
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Mektron KK
Original Assignee
Nippon Mektron KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Mektron KK filed Critical Nippon Mektron KK
Priority to JP62174007A priority Critical patent/JPS6419057A/en
Publication of JPS6419057A publication Critical patent/JPS6419057A/en
Pending legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/55—Design of synthesis routes, e.g. reducing the use of auxiliary or protecting groups

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

NEW MATERIAL:A compound expressed by formula I (X and Y are H or methyl; Y is methyl when X is H and X is methyl when Y is H). EXAMPLE:Allyl(trans 1-propenyl) disulfide. USE:A garlic component useful as a spice, folk, medicine, etc. PREPARATION:A 1-propenethiol derivative expressed by formula II (A is thiol- protecting group eliminating by a halogenating agent) is reacted with an allyl mercaptan derivative expressed by formula III in the presence of a halogenating agent in a solvent, such as THF, at 0-100 deg.C for 30-180min to afford the aimed compound expressed by formula I. The halogenating agent is used in an amount of 1-3 equiv. based on the compound expressed by formula II and the excessive halogenating agent is removed by treating with a reducing agent, such as sodium sulfite, after completing the reaction.
JP62174007A 1987-07-14 1987-07-14 Allyl(1-propenyl) disulfide and production thereof Pending JPS6419057A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP62174007A JPS6419057A (en) 1987-07-14 1987-07-14 Allyl(1-propenyl) disulfide and production thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP62174007A JPS6419057A (en) 1987-07-14 1987-07-14 Allyl(1-propenyl) disulfide and production thereof

Publications (1)

Publication Number Publication Date
JPS6419057A true JPS6419057A (en) 1989-01-23

Family

ID=15971013

Family Applications (1)

Application Number Title Priority Date Filing Date
JP62174007A Pending JPS6419057A (en) 1987-07-14 1987-07-14 Allyl(1-propenyl) disulfide and production thereof

Country Status (1)

Country Link
JP (1) JPS6419057A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5011975A (en) * 1988-03-04 1991-04-30 Nippon Miktron Limited Novel (trans 1-propenyl)disulfide derivative and process for preparing the same
EP0464521A2 (en) * 1990-06-22 1992-01-08 Wakunaga Seiyaku Kabushiki Kaisha Polysulfide compounds and lipid peroxidation inhibitor containing the polysulfide compounds as active ingredient
US5231114A (en) * 1990-06-22 1993-07-27 Wakunaga Seiyaku Kabushiki Kaisha Polysulfides compounds and lipid peroxidation inhibitor containing the polysulfide compounds as active ingredient

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5011975A (en) * 1988-03-04 1991-04-30 Nippon Miktron Limited Novel (trans 1-propenyl)disulfide derivative and process for preparing the same
EP0464521A2 (en) * 1990-06-22 1992-01-08 Wakunaga Seiyaku Kabushiki Kaisha Polysulfide compounds and lipid peroxidation inhibitor containing the polysulfide compounds as active ingredient
US5231114A (en) * 1990-06-22 1993-07-27 Wakunaga Seiyaku Kabushiki Kaisha Polysulfides compounds and lipid peroxidation inhibitor containing the polysulfide compounds as active ingredient

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