JPS59141473A - Rare metal picture formation on ceramic products - Google Patents
Rare metal picture formation on ceramic productsInfo
- Publication number
- JPS59141473A JPS59141473A JP1476583A JP1476583A JPS59141473A JP S59141473 A JPS59141473 A JP S59141473A JP 1476583 A JP1476583 A JP 1476583A JP 1476583 A JP1476583 A JP 1476583A JP S59141473 A JPS59141473 A JP S59141473A
- Authority
- JP
- Japan
- Prior art keywords
- gold
- platinum
- ultraviolet
- transfer paper
- ceramic products
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000919 ceramic Substances 0.000 title claims description 11
- 230000015572 biosynthetic process Effects 0.000 title claims description 3
- 229910052751 metal Inorganic materials 0.000 title description 2
- 239000002184 metal Substances 0.000 title description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 23
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims description 15
- 229910052737 gold Inorganic materials 0.000 claims description 13
- 239000010931 gold Substances 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 12
- 229910052697 platinum Inorganic materials 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 11
- 238000009472 formulation Methods 0.000 claims description 7
- 229910052709 silver Inorganic materials 0.000 claims description 7
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 6
- 239000004332 silver Substances 0.000 claims description 6
- 239000010970 precious metal Substances 0.000 claims description 5
- 229910052797 bismuth Inorganic materials 0.000 claims description 3
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 claims description 3
- 229920003002 synthetic resin Polymers 0.000 claims description 2
- 239000000057 synthetic resin Substances 0.000 claims description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 2
- 229910017052 cobalt Inorganic materials 0.000 claims 1
- 239000010941 cobalt Substances 0.000 claims 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- -1 hyflom Chemical class 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 150000002902 organometallic compounds Chemical class 0.000 claims 1
- 150000002941 palladium compounds Chemical class 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 description 9
- 239000011347 resin Substances 0.000 description 7
- 229920005989 resin Polymers 0.000 description 7
- 238000001035 drying Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 150000002894 organic compounds Chemical class 0.000 description 4
- 239000010948 rhodium Substances 0.000 description 4
- 238000009835 boiling Methods 0.000 description 3
- 238000010304 firing Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 229910052703 rhodium Inorganic materials 0.000 description 3
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 3
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- 241000779819 Syncarpia glomulifera Species 0.000 description 2
- 239000012298 atmosphere Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 239000011651 chromium Substances 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000001739 pinus spp. Substances 0.000 description 2
- 238000007639 printing Methods 0.000 description 2
- 238000007650 screen-printing Methods 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- 229940036248 turpentine Drugs 0.000 description 2
- 208000032170 Congenital Abnormalities Diseases 0.000 description 1
- 206010010356 Congenital anomaly Diseases 0.000 description 1
- 229920001353 Dextrin Polymers 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- 244000062793 Sorghum vulgare Species 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229940072049 amyl acetate Drugs 0.000 description 1
- PGMYKACGEOXYJE-UHFFFAOYSA-N anhydrous amyl acetate Natural products CCCCCOC(C)=O PGMYKACGEOXYJE-UHFFFAOYSA-N 0.000 description 1
- 230000007698 birth defect Effects 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 235000019425 dextrin Nutrition 0.000 description 1
- 238000010017 direct printing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- MNWFXJYAOYHMED-UHFFFAOYSA-M heptanoate Chemical compound CCCCCCC([O-])=O MNWFXJYAOYHMED-UHFFFAOYSA-M 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 235000019713 millet Nutrition 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 239000000025 natural resin Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000013557 residual solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 230000002747 voluntary effect Effects 0.000 description 1
Landscapes
- Other Surface Treatments For Metallic Materials (AREA)
- Chemically Coating (AREA)
- Ceramic Capacitors (AREA)
Abstract
(57)【要約】本公報は電子出願前の出願データであるた
め要約のデータは記録されません。(57) [Summary] This bulletin contains application data before electronic filing, so abstract data is not recorded.
Description
【発明の詳細な説明】
こめ発明は、窯業製品に金、銀、白金等の貴金属画像を
形成する方法に関するものである。窯業製品に貴金属巴
を給付する方法には、合液（水金）、白金液、銀液等′
９ｒ、細毛筆又はゴム印で描画する方法と貝金属有機物
調合ベース）ｋ用いて直刷り、或いはスライド転写する
方法とがある。DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a method for forming precious metal images such as gold, silver, platinum, etc. on ceramic products. Methods of applying precious metal tomoe to ceramic products include mixed liquid (water and gold), platinum liquid, silver liquid, etc.
9r, a method of drawing with a fine brush or a rubber stamp, and a method of direct printing using a shell metal organic substance blend base) or a method of slide transfer.
従来、スライド転写法の場合［賞金Ｓ４有機物調合ペー
ストは金、白金等の貴金属ｆ機「ヒ合物、クロム、ビス
マス等の金＠！磯比合物、アルキッド樹脂のようなポリ
エステル型樹脂、ロジン等の天然樹脂、テレピン油等の
植物精油、プチルセロンルヘ等のエーテル類、酢酸上ア
ミル等のエステル類等の溶剤で調合されている。このよ
うなペースト盆使用してスクリーン印刷等に↓９転写紙
（吸水性のある紙にデキストリン全塗布した台紙）に印
刷し、乾燥後、溶剤型カバーコート（トップコート）を
画像にカバーして、ｃｎ２乾燥後、水に浸漬し、離脱し
たカバーコート上の画像を窯業製品にスライド転写し、
焼成していた。然るに、前記の方法では中高沸点の溶剤
の混入で印刷した転写紙の乾燥時間が長くか〃）り、乾
Ｕ１％場所及び面積が大となる。直に、池の巳彩ペース
トインキケ重ねｔＪｉＱ ｔ）する・混合も、乾ブ：■
時間が長い為に、次のエナ”Ａへの移動が遅くなり、非
効率的である。又、低沸点浴：１１會使用した喘合ば、
−６剤の蒸発によるペーストの安定性がなく、印刷中の
目堪りが生じ、乾燥時間の短縮は出来ても良い画像が得
ら１ない。Conventionally, in the case of the slide transfer method [Prize S4 organic compound paste is made of precious metals such as gold and platinum. It is formulated with solvents such as natural resins such as turpentine, vegetable essential oils such as turpentine, ethers such as butyl seron luhe, and esters such as amyl acetate.Use such paste trays for screen printing, etc.↓9 Transfer paper (Water-absorbent paper fully coated with dextrin), after drying, cover the image with a solvent-based cover coat (top coat), after cn2 drying, immerse in water, and remove the separated cover coat. Slide transfer the image onto the ceramic product,
It was being fired. However, in the above-mentioned method, the drying time of the printed transfer paper becomes long due to the mixing of medium-to-high boiling point solvents, and the drying area and area become large. Directly layer Ikenomisai paste ink tJiQ t) Mix and dry:■
Because the time is long, the movement to the next EnerA is slow and inefficient.Also, if the low boiling point bath is used for 11 sessions,
There is no paste stability due to the evaporation of the -6 agent, resulting in rough edges during printing, and even if the drying time can be shortened, good images cannot be obtained.
その上、印幅１後、画像上にカバーコート７カバーする
が、残存溶剤の為焼成雰囲気を悪阻させ、又、残存溶剤
とカバーコートの溶１１すとの混合すてよる画像の発色
及び光沢Ｃ・て悪影響ケ与える等の欠陥があった。父、
溶剤の蒸髭によって環境？４？生上の欠陥も有してい足
のである。Moreover, after printing width 1, the image is covered with cover coat 7, but the remaining solvent adversely affects the firing atmosphere, and the color development and gloss of the image due to the mixture of the remaining solvent and the cover coat solution 11. C. There were defects that caused negative effects. father,
Environmental by the vaporization of solvent? 4? They also have some birth defects.
そこでこの発明は、前述の欠陥勿除去する目的で、溶ｉ
？ＩＩ會ＩＷ用せず、紫外線硬化性樹脂ｒ用いることに
よる窯業製品に対する画像音形成させるものである。Therefore, in order to remove the above-mentioned defects, this invention
? In this method, an image sound is formed on a ceramic product by using an ultraviolet curable resin R without using IW.
μ［、本発明の一実施例ヶ詳述する。μ [, An embodiment of the present invention will be described in detail.
１、 プライトゴールドペースト、１４Ｉｆｔ比硫比、
面詣金 （Ａ、ｕ ２５％含＠）４０硫比樹脂銀
（Ａｇ２０％含仔） ５０ジユウム樹梢（Ｒｈ ５
％含有） ８ビスマス噌脂 （Ｂｉ 、１０ゝチ含有
） ５り ロ ム樹脂 （Ｏｖ ５％含有） ２
尉脂モノマー ５紫外線硬化性櫃
脂調合物 ４０
上記配合にニジ紫外線硬化性金色用（ブライトゴールド
）ペースト７得る。1. Prite gold paste, 14Ift specific sulfur ratio,
Menmoikin (A, containing 25% u) 40 sulfur ratio resin silver
(Contains 20% Ag) 50% treetop (Rh 5
8 Bismuth paste (Contains 10% of Bi) 5 Rubber resin (Contains 5% of Ov) 2
Bright gold paste 7 is obtained from the above formulation.
２− ブライトブラチニュウムベース）硫ｆヒ宿脂白金
（Ｐｔ１０％含有） １５硫化樹脂金 （Ａｕ２
５％含有）８０ロジュウム面脂（Ｒ，ｈ ５％含有）
Φビスマス樹脂（旨 （ＢｉｌＯ％含有） ５ク
ロム樹脂 （Ｏｖ ５％含有） ｌ噌を信モノマ
ー ５紫外線硬化性樹脂調合物
４０
上記配合Ｖｃニジ紫外線硬化性白金巴川（ブライトグラ
チニュウム）ペースト奮得る。2- Bright Bratinium Base) Sulfurized Bratinium Platinum (Contains 10% Pt) 15 Sulfurized Resin Gold (Au2
5% content) 80 rhodium skin fat (R, h 5% content)
Φ Bismuth resin (Contains BilO%) 5 Chromium resin (Contains Ov 5%) Monomer 5 Ultraviolet curable resin formulation
40 The above formulation Vc rainbow curable platinum Tomoegawa (Bright Gratinium) paste is available.
前述の金色、白金６用ペーストは本発明の溶剤ケ使用し
ないで、紫外線で硬【ヒさせる目的の調合物の例で、そ
′ｎに金粉末、銀粉末、・くラジュウム粉末等の貴金属
粉末と市販の７ラツクス（ガラス１褒焉剤）全添加すれ
は艶消貴金帆有機ｆヒ合物ベーストが出来る。貴金属と
して白金の代りにノ々ラジュウムを用いることも出来る
。而して、前記の艶消黄金４有機比合物ペーストＩ／ｉ
次の通りである。The above-mentioned paste for gold and platinum 6 is an example of a composition for hardening with ultraviolet rays without using a solvent according to the present invention. By adding all of the commercially available 7 Lacs (Glass 1 Compliment Agent), a matte precious gold sail organic compound base can be obtained. Nonoradium can also be used as the precious metal instead of platinum. Thus, the matte golden 4 organic compound paste I/i
It is as follows.
第１例のペースト ｉｏ。First example paste io.
金粉末（平均粒度１ミクロン） ７
フラツクス（市販ガラス接着剤） ｌ
上記の工うに製造しプこ貴会４有機化合物調合ペースト
χ用いて転写紙に画像を印判し、このベース）ｋ紫外線
で硬ｆヒさせ、硬化させた画像上に紫外線硬「ヒ型ｆＡ
脂調合物（ドッグコート）又は、市販の合成樹１１旨調
合物（溶剤型トップコート）ｔカバーコーテングして転
写紙？得る。この転写紙を水に浸漬し、台紙の裏面から
の吸水でデキス） ＩＪンが溶解し１８画像はトップコ
ートと共に剥離する。Gold powder (average particle size 1 micron) 7. Flux (commercially available glass adhesive) 1. Stamp the image on transfer paper using the above-mentioned 4 organic compound blended paste χ, and harden it with ultraviolet light (this base). UV hardening “H type fA” is applied on the cured image.
Oil formulation (dog coat) or commercially available synthetic resin formulation (solvent type top coat) t cover coating and transfer paper? obtain. This transfer paper is immersed in water, and the transfer paper is dissolved by water absorption from the back side of the mount, and the 18 image is peeled off together with the top coat.
こｆｌ−７ｒ、スライドさせて窯業製品に転写し、水分
全乾燥させた後、焼成す１ば、トップコートは焼失し、
窯−゛６製品に金、銀、白金、その他の黄金用膜の所望
の画像が得ら扛る。勿論、）−記調合物中、樹＝ｉｉｔ
は睨成に際してゝ焼失し、ビスマス、クロムは寅＠属の
附Ｎ盆増大し、（に、ロジュウムト共に光沢全増大させ
る。This fl-7r was transferred onto a ceramic product by sliding it, and after being completely dried, the top coat was burned out.
Kiln - 6 The desired image of gold, silver, platinum and other gold films is obtained on the product. Of course, in the formulation)-iit
is burnt out during formation, bismuth and chromium increase in the genus N, and rhodium and rhodium increase in luster.
以上詳述せるが叩く、中高沸点の溶剤は不要で、乾燥呼
量の短縮で、重ね刷りの為の時間的ロスもなく、環境衛
生的にも同上し、（に、残存溶剤がない為に焼成炉の雰
囲気も良好で、ペーストとトップコートの溶削と、／）
混合もなく、焼成後の窯業製品の画像の発色及び光沢が
（侃めて優ｎだものとなる。As detailed above, there is no need for solvents with medium to high boiling points, the drying volume is shortened, there is no time loss due to overprinting, and it is also environmentally hygienic (as there is no residual solvent). The atmosphere in the firing furnace was good, and the paste and top coat were melted and /)
There is no mixing, and the color development and gloss of the image of the ceramic product after firing are excellent.
じ二５ 、・
す杭抽市冴
昭和５８手５．４８日
特許庁 長官 若杉和夫殿
■ 事件の表示
特願昭５８−０１４７６５号
２ 発明の名称
窯粟製品への貴悄頃画像形成法
イ１所
エ ア、 床式会社 水面スクリーン印刷４ｄ（突所
外１名４ 代 理 人
〒１０３ 東京都中央区［３木梧茅場町１丁目１１番
２号′Ｉ″ＥＬ （６６８） ７ ９ ２ １〜３
５、 補正命令の日付
自発補正
６、補正のη象
明細書
７、 補正の内容
＋１１ 明細書の第２頁１２行にｔ記載の「ルペＪｘ
「ルブ」と補正する。J25, Sukuikuichi Sae, 1972, 5.48th, Japan Patent Office, Mr. Kazuo Wakasugi, Commissioner ■ Indication of the case, Patent Application No. 1987-014765 2 Name of the invention: Method for forming images on kiln millet products 1 location Air, floor type company Water surface screen printing 4d (Outside office 1 person 4 representatives 〒103 Chuo-ku, Tokyo [3 Kogo Kayaba-cho 1-11-2'I''EL (668) 7 9 2 1-3
5. Date of amendment order Voluntary amendment 6, Amendment specification 7, Contents of amendment + 11 “Lupe Jx” written in t on page 2, line 12 of the specification
Correct with "lube."
＋２１ 明細書の第４頁４行、同１４行に記載の［Ｏ
ｖｊ ＊ ｒａｒ Ｊと補正する。+21 [O
Correct as vj * rar J.
３８１381
Claims (1)
合物及ヒフロム、ニッケル、ビスマス、コバルト等の
金属有機化合物と紫外線硬化性樹ＩＩ！調合物５〜８０
重敞％からなる紫外線硬ｔヒペーストで転写紙にスクリ
ーン等で画像を印刷し、２全紫外線で硬化させ、ｆｖｃ
、紫外＠硬化性カバーコート或いは合成樹脂調合カバー
コートで画像部門七カバーして得らｎだ転写紙欠窯業製
品にスライド転写し、焼成して窯業製品への金、銀、白
金色等の画像形成法。 （２）前記の紫外線硬１ヒペーストに金、白金、銀その
池貴金属粉末で添加し′ｆｃ調合物を匝用し罠転写紙全
窯業製品にスライド転写し、焼成すること全特徴とする
特許請求の範囲第１項の窯業製品への貴金属＠像形成法
。[Claims] (Eleven gold, platinum, palladium
Compounds and metal-organic compounds such as hyflom, nickel, bismuth, and cobalt, and UV-curable trees II! Formulation 5-80
Print an image on transfer paper with a screen or the like using ultraviolet hard paste made of Chungchang%, harden it with ultraviolet rays, and apply fvc.
, cover the image area with an ultraviolet curable cover coat or a synthetic resin compound cover coat, slide transfer onto a ceramic product with no transfer paper, and bake to apply gold, silver, platinum color, etc. images to the ceramic product. Formation method. (2) A patent claim which is characterized in that gold, platinum, silver, and other precious metal powders are added to the ultraviolet-hardened 1hypaste and the 'fc composition is applied, slide-transferred onto trap transfer paper and all ceramic products, and fired. Precious metal @ image forming method for ceramic products in scope 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1476583A JPS59141473A (en) | 1983-02-01 | 1983-02-01 | Rare metal picture formation on ceramic products |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1476583A JPS59141473A (en) | 1983-02-01 | 1983-02-01 | Rare metal picture formation on ceramic products |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS59141473A true JPS59141473A (en) | 1984-08-14 |
Family
ID=11870166
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1476583A Pending JPS59141473A (en) | 1983-02-01 | 1983-02-01 | Rare metal picture formation on ceramic products |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59141473A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61286288A (en) * | 1985-06-10 | 1986-12-16 | 大研化学工業株式会社 | Metallized membrane transfer sheet and formation of metallized membrane on ceramic package |
| WO2004076569A1 (en) | 2003-02-28 | 2004-09-10 | Ferro Gmbh | Radiohardenable printing media, transfer pictures produced therewith, and method for producing ceramic decorations |
| JP2016198895A (en) * | 2015-04-07 | 2016-12-01 | 株式会社ミマキエンジニアリング | Method for producing transfer sheet and use thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5935079A (en) * | 1982-08-16 | 1984-02-25 | 日本写真印刷株式会社 | Transfer sheet for painting ceramic product and manufacture of painted ceramic product therewith |
-
1983
- 1983-02-01 JP JP1476583A patent/JPS59141473A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5935079A (en) * | 1982-08-16 | 1984-02-25 | 日本写真印刷株式会社 | Transfer sheet for painting ceramic product and manufacture of painted ceramic product therewith |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61286288A (en) * | 1985-06-10 | 1986-12-16 | 大研化学工業株式会社 | Metallized membrane transfer sheet and formation of metallized membrane on ceramic package |
| WO2004076569A1 (en) | 2003-02-28 | 2004-09-10 | Ferro Gmbh | Radiohardenable printing media, transfer pictures produced therewith, and method for producing ceramic decorations |
| JP2016198895A (en) * | 2015-04-07 | 2016-12-01 | 株式会社ミマキエンジニアリング | Method for producing transfer sheet and use thereof |
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