JPS56159221A - Equipment for continuous solid-phase polymerization - Google Patents
Equipment for continuous solid-phase polymerizationInfo
- Publication number
- JPS56159221A JPS56159221A JP6166880A JP6166880A JPS56159221A JP S56159221 A JPS56159221 A JP S56159221A JP 6166880 A JP6166880 A JP 6166880A JP 6166880 A JP6166880 A JP 6166880A JP S56159221 A JPS56159221 A JP S56159221A
- Authority
- JP
- Japan
- Prior art keywords
- viscosity
- vacuum
- controller
- predetermined
- chips
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000006116 polymerization reaction Methods 0.000 title abstract 5
- 239000007790 solid phase Substances 0.000 title abstract 2
- 229920000642 polymer Polymers 0.000 abstract 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 229910001873 dinitrogen Inorganic materials 0.000 abstract 1
- 238000002844 melting Methods 0.000 abstract 1
- 230000008018 melting Effects 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
Landscapes
- Polyesters Or Polycarbonates (AREA)
Abstract
PURPOSE: A part of polymer chips taken out of the continuous solid polymerization tank is continuously melted and its viscosity is measured, then the vacuum in the polymerizer is controlled according to the viscosity, thus producing the chip product with less fluctuation in polymerization degree.
CONSTITUTION: In the solid-phase polymerization tank 1, chips reaching a predetermined polymerization degree are always trapped in the hopper 14 and pneumatically conveyed through pipe 18 with a rotary valve 19 under cooling with a nitrogen gas 15. A very small part of the chips in the hopper 14 is continuously sent through by-pass 21 to the melting extruder 20 and the viscosity of the melted polymer is detected with the detector 23 mounted to pipe 22. The detected values are compared with the predetermined one in the controller 29 to calculate the difference. The signals from the controller 29 to the vacuum controller 28 to change the set value of vacuum degree one corresponding to the measured viscosity and to control the valve 6, thus keeping the inside of the polymerizer to the predetermined vacuum.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP6166880A JPS56159221A (en) | 1980-05-12 | 1980-05-12 | Equipment for continuous solid-phase polymerization |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP6166880A JPS56159221A (en) | 1980-05-12 | 1980-05-12 | Equipment for continuous solid-phase polymerization |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS56159221A true JPS56159221A (en) | 1981-12-08 |
Family
ID=13177835
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP6166880A Pending JPS56159221A (en) | 1980-05-12 | 1980-05-12 | Equipment for continuous solid-phase polymerization |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS56159221A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0527032U (en) * | 1991-09-12 | 1993-04-06 | 日本エステル株式会社 | Continuous solid-state polymerization equipment |
JPH0537937U (en) * | 1991-10-29 | 1993-05-21 | 日本エステル株式会社 | Continuous solid-state polymerization equipment |
JP2008543993A (en) * | 2005-06-14 | 2008-12-04 | フェリンガー,マーカス | Method for increasing the intrinsic viscosity of a polyester material by solid phase polycondensation and apparatus therefor |
-
1980
- 1980-05-12 JP JP6166880A patent/JPS56159221A/en active Pending
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0527032U (en) * | 1991-09-12 | 1993-04-06 | 日本エステル株式会社 | Continuous solid-state polymerization equipment |
JPH0537937U (en) * | 1991-10-29 | 1993-05-21 | 日本エステル株式会社 | Continuous solid-state polymerization equipment |
JP2008543993A (en) * | 2005-06-14 | 2008-12-04 | フェリンガー,マーカス | Method for increasing the intrinsic viscosity of a polyester material by solid phase polycondensation and apparatus therefor |
KR101298818B1 (en) * | 2005-06-14 | 2013-08-23 | 마르쿠스 펠린게르 | Method and device for increasing the limiting viscosity of polyester materials by solid phase polycondensation |
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