JPS56118666A - Process of removing iron content from total iron measuring reagent - Google Patents
Process of removing iron content from total iron measuring reagentInfo
- Publication number
- JPS56118666A JPS56118666A JP2182280A JP2182280A JPS56118666A JP S56118666 A JPS56118666 A JP S56118666A JP 2182280 A JP2182280 A JP 2182280A JP 2182280 A JP2182280 A JP 2182280A JP S56118666 A JPS56118666 A JP S56118666A
- Authority
- JP
- Japan
- Prior art keywords
- solution
- iron
- reagent
- water
- measuring reagent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/22—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using chemical indicators
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Molecular Biology (AREA)
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Biophysics (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
PURPOSE:To make it possible to remove iron content from a total iron measuring reagent by a single treatment without using injurious solvent, by adding iron reducing agent and bathophenantroline acetic acid solution or ethanol solution to the reagent, and filtering thus produced precipitate. CONSTITUTION:500g of a total iron measuring reagent (ammonium acetate and hydroxylamine hydrochloride) for measuring iron content in hoiler water and boiler- supplying water is dissolved in water to produce 1 litre of solution, and to this solution, in the case of using ammonium acetate as an iron reducing agent, 10ml of water solution of hydroxylamine hydrochloride (10w/v%) and also 10ml of bathophenantroline acetic acid solution or ethanol solution (1/400M) are added. Thus, mixed solution is agitated for more than 1hr and set still for 24hr, and then by using a millipore filter having small holes of 1.2mu in diameter, thus formed complex precipitate is filtered to produce iron-free reagent solution. In this process, unlike the conventional process, it is possible to obtain a large quantity of iron-free solution by a single treatment without using injurious solvent.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2182280A JPS56118666A (en) | 1980-02-23 | 1980-02-23 | Process of removing iron content from total iron measuring reagent |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2182280A JPS56118666A (en) | 1980-02-23 | 1980-02-23 | Process of removing iron content from total iron measuring reagent |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS56118666A true JPS56118666A (en) | 1981-09-17 |
Family
ID=12065745
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2182280A Pending JPS56118666A (en) | 1980-02-23 | 1980-02-23 | Process of removing iron content from total iron measuring reagent |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS56118666A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2016109478A (en) * | 2014-12-03 | 2016-06-20 | 株式会社 商船三井 | Analysis method and analysis kit for cylinder drain |
JP2018508014A (en) * | 2015-01-14 | 2018-03-22 | トタル マルケティン セルビスス | Method and kit for measuring iron ions in lubricating composition |
CN114870903A (en) * | 2022-04-07 | 2022-08-09 | 浙江西热利华智能传感技术有限公司 | Mixed catalyst for dissolving trace colloidal iron in water vapor of power station |
-
1980
- 1980-02-23 JP JP2182280A patent/JPS56118666A/en active Pending
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2016109478A (en) * | 2014-12-03 | 2016-06-20 | 株式会社 商船三井 | Analysis method and analysis kit for cylinder drain |
JP2018508014A (en) * | 2015-01-14 | 2018-03-22 | トタル マルケティン セルビスス | Method and kit for measuring iron ions in lubricating composition |
CN114870903A (en) * | 2022-04-07 | 2022-08-09 | 浙江西热利华智能传感技术有限公司 | Mixed catalyst for dissolving trace colloidal iron in water vapor of power station |
CN114870903B (en) * | 2022-04-07 | 2024-04-23 | 浙江西热利华智能传感技术有限公司 | Mixed catalyst for dissolving trace colloidal iron in water vapor of power station |
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