JPS557530A - Manufacture of anhydrous sodium carbonate - Google Patents
Manufacture of anhydrous sodium carbonateInfo
- Publication number
- JPS557530A JPS557530A JP7853978A JP7853978A JPS557530A JP S557530 A JPS557530 A JP S557530A JP 7853978 A JP7853978 A JP 7853978A JP 7853978 A JP7853978 A JP 7853978A JP S557530 A JPS557530 A JP S557530A
- Authority
- JP
- Japan
- Prior art keywords
- sodium carbonate
- nacl
- temp
- transition
- soln
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 title abstract 8
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 8
- 239000011780 sodium chloride Substances 0.000 abstract 4
- 230000007704 transition Effects 0.000 abstract 4
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 abstract 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 abstract 2
- MQRJBSHKWOFOGF-UHFFFAOYSA-L disodium;carbonate;hydrate Chemical compound O.[Na+].[Na+].[O-]C([O-])=O MQRJBSHKWOFOGF-UHFFFAOYSA-L 0.000 abstract 2
- 239000003792 electrolyte Substances 0.000 abstract 2
- 229940001593 sodium carbonate Drugs 0.000 abstract 2
- 229910000029 sodium carbonate Inorganic materials 0.000 abstract 2
- 229940076133 sodium carbonate monohydrate Drugs 0.000 abstract 2
- 235000002918 Fraxinus excelsior Nutrition 0.000 abstract 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 abstract 1
- 238000009621 Solvay process Methods 0.000 abstract 1
- 235000019270 ammonium chloride Nutrition 0.000 abstract 1
- 239000002956 ash Substances 0.000 abstract 1
- 238000001354 calcination Methods 0.000 abstract 1
- 239000001569 carbon dioxide Substances 0.000 abstract 1
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract 1
- 238000005868 electrolysis reaction Methods 0.000 abstract 1
- 230000005484 gravity Effects 0.000 abstract 1
- 230000000887 hydrating effect Effects 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 150000004682 monohydrates Chemical class 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 abstract 1
- 235000017557 sodium bicarbonate Nutrition 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/35—Varying the content of water of crystallisation or the specific gravity
- C01D7/37—Densifying sodium carbonate
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D7/00—Carbonates of sodium, potassium or alkali metals in general
- C01D7/35—Varying the content of water of crystallisation or the specific gravity
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Glass Compositions (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
PURPOSE: To obtain anhydrous sodium carbonate easy to handle and having high bulk specific gravity and hardness by holding an aq. soln. of sodium carbonate at a temp. 3W7°C above the transition temp. of sodium carbonate monohydrate in the presence of NaCl.
CONSTITUTION: 10W22 wt% of NaCl is added to an aq. soln. of sodium carbonate, and the soln. is held at a temp. 3W7°C above the transition temp. of sodium carbonate monohydrate into anhydrous sodium carbonate to induce the transition, thus obtaining anhydrous sodium carbonate. The raw material monohydrate may be formed by hydrating light ashes obtd. by calcining crude sodium bicarbonate of Solvay process or an ammonium chloride concurrent production process. An electrolyte from diaphragm method NaCl electrolysis may be carbonated with carbon dioxide or sodium bicarbonate, and the carbonated electrolyte can directly be supplied to an anhydrous salt transition vessel since it contains NaCl.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7853978A JPS557530A (en) | 1978-06-30 | 1978-06-30 | Manufacture of anhydrous sodium carbonate |
| BE0/195843A BE877106A (en) | 1978-06-30 | 1979-06-20 | PROCESS FOR THE PRODUCTION OF ANHYDROUS SODIUM CARBONATE BY TRANSFORMATION OF SODIUM CARBONATE MONOHYDRATE |
| FR7915822A FR2429749A1 (en) | 1978-06-30 | 1979-06-20 | PROCESS FOR PRODUCING ANHYDROUS SODIUM CARBONATE BY PROCESSING SODIUM CARBONATE MONOHYDRATE |
| GB7922190A GB2024187B (en) | 1978-06-30 | 1979-06-26 | Process for producing anhydrous sodium carbonate |
| DE19792926380 DE2926380A1 (en) | 1978-06-30 | 1979-06-29 | METHOD FOR PRODUCING WATER-FREE SODIUM CARBONATE |
| IT23987/79A IT1121968B (en) | 1978-06-30 | 1979-06-29 | PROCESS FOR THE PRODUCTION OF SODIUM CARBONATE ANHYDROUS |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7853978A JPS557530A (en) | 1978-06-30 | 1978-06-30 | Manufacture of anhydrous sodium carbonate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS557530A true JPS557530A (en) | 1980-01-19 |
| JPS616010B2 JPS616010B2 (en) | 1986-02-22 |
Family
ID=13664708
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7853978A Granted JPS557530A (en) | 1978-06-30 | 1978-06-30 | Manufacture of anhydrous sodium carbonate |
Country Status (6)
| Country | Link |
|---|---|
| JP (1) | JPS557530A (en) |
| BE (1) | BE877106A (en) |
| DE (1) | DE2926380A1 (en) |
| FR (1) | FR2429749A1 (en) |
| GB (1) | GB2024187B (en) |
| IT (1) | IT1121968B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5756318A (en) * | 1980-09-19 | 1982-04-03 | Asahi Glass Co Ltd | Manufacture of dense ash |
| KR20140110921A (en) * | 2011-12-09 | 2014-09-17 | 메르크 파텐트 게엠베하 | Anhydrous sodium carbonate with few pores |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56109818A (en) * | 1980-02-01 | 1981-08-31 | Asahi Glass Co Ltd | Manufacture of anhydrous sodium carbonate crystal |
| JPS56109819A (en) * | 1980-02-04 | 1981-08-31 | Asahi Glass Co Ltd | Manufacture of anhydrous sodium carbonate crystal |
| FR2576589B1 (en) * | 1985-01-30 | 1987-03-27 | Solvay | PROCESS FOR THE MANUFACTURE OF DENSE ANHYDROUS SODIUM CARBONATE AND DENSE ANHYDROUS SODIUM CARBONATE OBTAINED BY THIS PROCESS |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2133455A (en) * | 1935-05-07 | 1938-10-18 | Solvay Process Co | Production of dense soda asii |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1076651B (en) * | 1958-10-09 | 1960-03-03 | Chem Fab Kalk Ges Mit Beschrae | Process for the production of a coarsely crystalline and abrasion-resistant sodium carbonate |
-
1978
- 1978-06-30 JP JP7853978A patent/JPS557530A/en active Granted
-
1979
- 1979-06-20 FR FR7915822A patent/FR2429749A1/en active Pending
- 1979-06-20 BE BE0/195843A patent/BE877106A/en not_active IP Right Cessation
- 1979-06-26 GB GB7922190A patent/GB2024187B/en not_active Expired
- 1979-06-29 DE DE19792926380 patent/DE2926380A1/en active Granted
- 1979-06-29 IT IT23987/79A patent/IT1121968B/en active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2133455A (en) * | 1935-05-07 | 1938-10-18 | Solvay Process Co | Production of dense soda asii |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5756318A (en) * | 1980-09-19 | 1982-04-03 | Asahi Glass Co Ltd | Manufacture of dense ash |
| JPH0142891B2 (en) * | 1980-09-19 | 1989-09-18 | Asahi Glass Co Ltd | |
| KR20140110921A (en) * | 2011-12-09 | 2014-09-17 | 메르크 파텐트 게엠베하 | Anhydrous sodium carbonate with few pores |
| JP2015500195A (en) * | 2011-12-09 | 2015-01-05 | メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフツングＭｅｒｃｋ Ｐａｔｅｎｔ Ｇｅｓｅｌｌｓｃｈａｆｔ ｍｉｔ ｂｅｓｃｈｒａｅｎｋｔｅｒ Ｈａｆｔｕｎｇ | Anhydrous sodium carbonate with low pore content |
Also Published As
| Publication number | Publication date |
|---|---|
| GB2024187B (en) | 1982-07-21 |
| DE2926380A1 (en) | 1980-01-10 |
| IT1121968B (en) | 1986-04-23 |
| DE2926380C2 (en) | 1988-03-10 |
| IT7923987A0 (en) | 1979-06-29 |
| BE877106A (en) | 1979-12-20 |
| JPS616010B2 (en) | 1986-02-22 |
| FR2429749A1 (en) | 1980-01-25 |
| GB2024187A (en) | 1980-01-09 |
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