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JPS556423A - Production of benzthiazolylsulfenamide - Google Patents

Production of benzthiazolylsulfenamide

Info

Publication number
JPS556423A
JPS556423A JP7704978A JP7704978A JPS556423A JP S556423 A JPS556423 A JP S556423A JP 7704978 A JP7704978 A JP 7704978A JP 7704978 A JP7704978 A JP 7704978A JP S556423 A JPS556423 A JP S556423A
Authority
JP
Japan
Prior art keywords
primary
water
alkyl groups
secondary amine
benzthiazolylsulfenamide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP7704978A
Other languages
Japanese (ja)
Inventor
Yoshikimi Yamamoto
Taizo Sako
Yoshio Nagai
Shigeru Torii
Hideo Tanaka
Masafumi Ukita
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ouchi Shinko Chemical Industrial Co Ltd
Original Assignee
Ouchi Shinko Chemical Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ouchi Shinko Chemical Industrial Co Ltd filed Critical Ouchi Shinko Chemical Industrial Co Ltd
Priority to JP7704978A priority Critical patent/JPS556423A/en
Publication of JPS556423A publication Critical patent/JPS556423A/en
Pending legal-status Critical Current

Links

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  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)

Abstract

PURPOSE: To virtually eliminate disposition problems of soiled water and waste water and produce the captioned amide by causing direct electrolytic oxidation crosscoupling of the specific primary or secondary amine and 2-mercaptobenzthiazole or bisbenzthiazole disulfide.
CONSTITUTION: The primary or secondary amine expressed by H2NR or HNR'R" (R is alkyl groups of straight-chain-, branch-or ring-form of C3 to C8, R', R" are similar alkyl groups of C2 thru C8 and indicate the groups forming rings with R', R") and MBT or MBTS are electrolytically oxidized and crosscoupled in the single or mixed solvent selected from aprotic polar solvents such as acetonitrile, nitrobenzene or other, protic solvents such as of alcohols, primary or secondary amines or other and water, without particularly adding supporting salt, whereby the benzthiazolylsulfenamide shown by formula I or II is directly produced.
COPYRIGHT: (C)1980,JPO&Japio
JP7704978A 1978-06-27 1978-06-27 Production of benzthiazolylsulfenamide Pending JPS556423A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP7704978A JPS556423A (en) 1978-06-27 1978-06-27 Production of benzthiazolylsulfenamide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP7704978A JPS556423A (en) 1978-06-27 1978-06-27 Production of benzthiazolylsulfenamide

Publications (1)

Publication Number Publication Date
JPS556423A true JPS556423A (en) 1980-01-17

Family

ID=13622915

Family Applications (1)

Application Number Title Priority Date Filing Date
JP7704978A Pending JPS556423A (en) 1978-06-27 1978-06-27 Production of benzthiazolylsulfenamide

Country Status (1)

Country Link
JP (1) JPS556423A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6536449B1 (en) 1997-11-17 2003-03-25 Mattson Technology Inc. Downstream surface cleaning process
CN104109879A (en) * 2014-07-21 2014-10-22 河南省科学院高新技术研究中心 Process for synthesizing rubber vulcanization accelerator TBBS by electrolytic method in water phase
CN104109878A (en) * 2014-07-21 2014-10-22 河南省科学院高新技术研究中心 Process for synthesizing rubber vulcanization accelerator CBS by electrolytic method in water phase
CN108727302A (en) * 2017-10-23 2018-11-02 科迈化工股份有限公司 A kind of environment-friendly type N tert butyl benzothiazole 2 sulfenamide(NS)Synthesis technology

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6536449B1 (en) 1997-11-17 2003-03-25 Mattson Technology Inc. Downstream surface cleaning process
CN104109879A (en) * 2014-07-21 2014-10-22 河南省科学院高新技术研究中心 Process for synthesizing rubber vulcanization accelerator TBBS by electrolytic method in water phase
CN104109878A (en) * 2014-07-21 2014-10-22 河南省科学院高新技术研究中心 Process for synthesizing rubber vulcanization accelerator CBS by electrolytic method in water phase
CN108727302A (en) * 2017-10-23 2018-11-02 科迈化工股份有限公司 A kind of environment-friendly type N tert butyl benzothiazole 2 sulfenamide(NS)Synthesis technology

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