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JPS54115390A - Preparation of large ring ethylenedioate - Google Patents

Preparation of large ring ethylenedioate

Info

Publication number
JPS54115390A
JPS54115390A JP2202378A JP2202378A JPS54115390A JP S54115390 A JPS54115390 A JP S54115390A JP 2202378 A JP2202378 A JP 2202378A JP 2202378 A JP2202378 A JP 2202378A JP S54115390 A JPS54115390 A JP S54115390A
Authority
JP
Japan
Prior art keywords
aluminum compound
ethylenedioate
large ring
give
fatty acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2202378A
Other languages
Japanese (ja)
Inventor
Hideto Matsuoka
Kenji Saeki
Noriaki Kihara
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Petrochemical Industries Ltd
Original Assignee
Mitsui Petrochemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Petrochemical Industries Ltd filed Critical Mitsui Petrochemical Industries Ltd
Priority to JP2202378A priority Critical patent/JPS54115390A/en
Publication of JPS54115390A publication Critical patent/JPS54115390A/en
Pending legal-status Critical Current

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  • Catalysts (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)

Abstract

PURPOSE: To obtain the title compound useful as musk perfumes, in a simple process in high yield, by polymerizing a dibasic fatty acid with ethylene glycol in the presence of an aluminum compound having a carbonate radical, and by depolymeirzing and ring closure of the polymer in vacuo.
CONSTITUTION: A basic aqueous solution of an aluminum compound, e.g. Al(OH)3, is brought into contact with CO2 gas or a substance which produces CO2 gas, to give an aluminum compound having a carbonate radical. A dibasic fatty acid of formula I: (n is an integer 6W14) or its ester is polymerized with ethylene glycol or ethylene oxide in the presence of the aluminum compound thus obtained at 50W250°C, preferably 100W200°C, and subjected to depolymerization and ring closure at 180W300°C, preferably 240W280°C, at a pressure of 10-2W 10 mm Hg, preferably 10-1Wl mm Hg, to give a large ring ethylenedioate of formula II.
COPYRIGHT: (C)1979,JPO&Japio
JP2202378A 1978-03-01 1978-03-01 Preparation of large ring ethylenedioate Pending JPS54115390A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2202378A JPS54115390A (en) 1978-03-01 1978-03-01 Preparation of large ring ethylenedioate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2202378A JPS54115390A (en) 1978-03-01 1978-03-01 Preparation of large ring ethylenedioate

Publications (1)

Publication Number Publication Date
JPS54115390A true JPS54115390A (en) 1979-09-07

Family

ID=12071376

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2202378A Pending JPS54115390A (en) 1978-03-01 1978-03-01 Preparation of large ring ethylenedioate

Country Status (1)

Country Link
JP (1) JPS54115390A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4594434A (en) * 1982-08-02 1986-06-10 National Distillers And Chemical Corporation Process for the depolymerization of polyesters using dawsonite as the catalyst
CN1059903C (en) * 1993-10-25 2000-12-27 朱守一 Macrocyclic musk dilactone compound and its processing method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4594434A (en) * 1982-08-02 1986-06-10 National Distillers And Chemical Corporation Process for the depolymerization of polyesters using dawsonite as the catalyst
CN1059903C (en) * 1993-10-25 2000-12-27 朱守一 Macrocyclic musk dilactone compound and its processing method

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