JPS5356608A - Preparation of dimethylformaide - Google Patents
Preparation of dimethylformaideInfo
- Publication number
- JPS5356608A JPS5356608A JP13152776A JP13152776A JPS5356608A JP S5356608 A JPS5356608 A JP S5356608A JP 13152776 A JP13152776 A JP 13152776A JP 13152776 A JP13152776 A JP 13152776A JP S5356608 A JPS5356608 A JP S5356608A
- Authority
- JP
- Japan
- Prior art keywords
- dimethylformaide
- preparation
- trimethylamine
- iodide
- dimethylformamide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 abstract 3
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 abstract 2
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 abstract 2
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
PURPOSE: To prepare dimethylformamide in high yield and selectivity by reacting monomethylamine and trimethylamine with CO by use of I2, Br2, an iodide or a bromide as a catalyst.
COPYRIGHT: (C)1978,JPO&Japio
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP13152776A JPS5356608A (en) | 1976-11-01 | 1976-11-01 | Preparation of dimethylformaide |
GB4353077A GB1554676A (en) | 1976-11-01 | 1977-10-19 | Process for producing dimethylformamide |
DE19772747999 DE2747999C3 (en) | 1976-11-01 | 1977-10-26 | Process for the production of dimethylformamide |
US05/972,257 US4218398A (en) | 1976-11-01 | 1978-12-22 | Process for producing dimethylformamide |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP13152776A JPS5356608A (en) | 1976-11-01 | 1976-11-01 | Preparation of dimethylformaide |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5356608A true JPS5356608A (en) | 1978-05-23 |
JPS5629856B2 JPS5629856B2 (en) | 1981-07-10 |
Family
ID=15060140
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP13152776A Granted JPS5356608A (en) | 1976-11-01 | 1976-11-01 | Preparation of dimethylformaide |
Country Status (3)
Country | Link |
---|---|
JP (1) | JPS5356608A (en) |
DE (1) | DE2747999C3 (en) |
GB (1) | GB1554676A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5587750A (en) * | 1978-12-27 | 1980-07-02 | Nitto Chem Ind Co Ltd | Preparation of dimethylformamide |
JPS5742660A (en) * | 1980-08-26 | 1982-03-10 | Ube Ind Ltd | Preparation of formamide |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5822105B2 (en) * | 1978-06-23 | 1983-05-06 | 三菱瓦斯化学株式会社 | Dimethylformamide manufacturing method |
CN112479919A (en) * | 2020-11-30 | 2021-03-12 | 安徽金禾实业股份有限公司 | Method for recovering dilute DMF (dimethyl formamide) in sucralose crystallization mother liquor wastewater |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2677706A (en) * | 1951-08-16 | 1954-05-04 | Commercial Solvents Corp | Preparation of n substituted formamides |
-
1976
- 1976-11-01 JP JP13152776A patent/JPS5356608A/en active Granted
-
1977
- 1977-10-19 GB GB4353077A patent/GB1554676A/en not_active Expired
- 1977-10-26 DE DE19772747999 patent/DE2747999C3/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5587750A (en) * | 1978-12-27 | 1980-07-02 | Nitto Chem Ind Co Ltd | Preparation of dimethylformamide |
JPS5742660A (en) * | 1980-08-26 | 1982-03-10 | Ube Ind Ltd | Preparation of formamide |
Also Published As
Publication number | Publication date |
---|---|
JPS5629856B2 (en) | 1981-07-10 |
DE2747999A1 (en) | 1978-05-03 |
DE2747999C3 (en) | 1981-07-16 |
DE2747999B2 (en) | 1980-10-16 |
GB1554676A (en) | 1979-10-24 |
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