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JPH0686633A - Protein-containing acidic drink - Google Patents

Protein-containing acidic drink

Info

Publication number
JPH0686633A
JPH0686633A JP3358731A JP35873191A JPH0686633A JP H0686633 A JPH0686633 A JP H0686633A JP 3358731 A JP3358731 A JP 3358731A JP 35873191 A JP35873191 A JP 35873191A JP H0686633 A JPH0686633 A JP H0686633A
Authority
JP
Japan
Prior art keywords
protein
fatty acid
weight
acid ester
milk
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP3358731A
Other languages
Japanese (ja)
Inventor
Yukihiro Amamiya
幸弘 雨宮
Nobuyuki Yokozawa
暢之 横沢
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NITSUSEE KK
Nissei Ltd
Original Assignee
NITSUSEE KK
Nissei Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NITSUSEE KK, Nissei Ltd filed Critical NITSUSEE KK
Priority to JP3358731A priority Critical patent/JPH0686633A/en
Publication of JPH0686633A publication Critical patent/JPH0686633A/en
Pending legal-status Critical Current

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  • Non-Alcoholic Beverages (AREA)
  • Dairy Products (AREA)

Abstract

PURPOSE:To provide a protein-containing acidic drink containing a specific amount of a specific polyglycerol fatty acid ester and free from the problem of coagulation, separation and precipitation caused by protein. CONSTITUTION:This acidic drink is produced by adding 0.005-0.2wt.% of a polyglycerol fatty acid ester having an HLB of >=8 and a polymerization degree of 6-10 (e.g. monoester of polyglycerol and a saturated fatty acid such as palmitic acid or an unsaturated fatty acid such as oleic acid) to an acidic drink comprising a fermented milk having pH of <=4.5 and a milk solid content of 0.1-5wt.%.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の目的】[Object of the Invention]

【産業上の利用分野】本発明は乳酸菌飲料等のタンパク
質含有酸性飲料に関し、特にタンパク質の凝集、分離、
沈澱のない飲料に係るものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a protein-containing acidic beverage such as a lactic acid bacterium beverage, and particularly to protein aggregation, separation,
It concerns beverages without precipitation.

【0002】[0002]

【発明の背景】近年、各種飲料の需要の伸びとともに、
タンパク質を含有する酸性飲料もその消費が拡大されつ
つある。しかしタンパク質は酸性下では不安定であり、
凝集物が発生しやすく、これにより飲用時に口中に違和
感が生じて飲料としての価値を半減させることになる。
そこで従来はゼラチン、ペクチン、CMCなどの高分子
多糖類により粘度や比重を高めることで凝集物の発生防
止を図ろうとしていたが、これを達成することはできな
かった。またHLB13以上のショ糖脂肪酸エステルを用
いてタンパク質の凝集物を防止する製造法( 特公昭59
−41709号)や、ポリグリセリン脂肪酸エステルと
カラギナンなどの安定剤との併用によりコーヒー飲料な
どの安定性を高める方法(特公平2−261366号)
などが開発されているが、前者ではやはり発酵乳の凝集
物を完全に防止できず、また後者でもPH4.5以下の
酸性下では発酵乳のタンパク質と安定剤との反応性が高
まり、凝集や沈澱を多くするといった問題があった。
BACKGROUND OF THE INVENTION In recent years, along with the growing demand for various beverages,
Consumption of protein-containing acidic beverages is also expanding. However, proteins are unstable under acidic conditions,
Aggregates are likely to be generated, which causes discomfort in the mouth during drinking and reduces the value as a beverage by half.
Therefore, in the past, attempts were made to prevent the formation of aggregates by increasing the viscosity and specific gravity by using high molecular weight polysaccharides such as gelatin, pectin, and CMC, but this could not be achieved. Further, a production method for preventing protein aggregates by using a sucrose fatty acid ester having an HLB of 13 or more (Japanese Patent Publication Sho 59)
-41709) or a method of enhancing the stability of a coffee beverage or the like by using a polyglycerin fatty acid ester and a stabilizer such as carrageenan (Japanese Patent Publication No. 2-261366).
However, the former cannot completely prevent the agglomerates of fermented milk, and the latter also increases the reactivity between the proteins of the fermented milk and the stabilizer under an acidity of pH 4.5 or less, resulting in agglomeration and aggregation. There was a problem of increasing precipitation.

【0003】[0003]

【開発を試みた技術的事項】本発明はこのような背景に
鑑みなされたものであって、発酵乳を使用した酸性飲料
の凝集、分離、沈澱などの問題を解決しようとしたタン
パク質含有酸性飲料の開発を試みたものである。
[Technical Items Attempted to Develop] The present invention has been made in view of such a background, and a protein-containing acidic beverage intended to solve problems such as aggregation, separation, and precipitation of an acidic beverage using fermented milk Is an attempt to develop.

【0004】[0004]

【発明の構成】[Constitution of the invention]

【目的達成の手段】即ち本発明たるタンパク質含有酸性
飲料は、発酵乳の乳固形分が0.1〜5 重量%であり、
PH4.5以下の酸性飲料において、HLB8以上で重
合度6〜10のポリグリセリン脂肪酸エステルが0.0
05〜0.2重量%添加されて成ることを特徴として成
るものであり、もって前記目的を達成しようとするもの
である。
[Means for Achieving the Object] That is, the protein-containing acidic beverage of the present invention has a milk solid content of fermented milk of 0.1 to 5% by weight,
In acidic beverages with a pH of 4.5 or less, the polyglycerin fatty acid ester having an HLB of 8 or more and a polymerization degree of 6 to 10 is 0.0.
It is characterized by being added in an amount of 05 to 0.2% by weight, and is intended to achieve the above object.

【0005】以下本発明の構成要件について具体的に説
明する。まず本発明のタンパク質含有酸性飲料は、動物
性、植物性を問わず、例えば純粋タンパク質のほか、全
乳、脱脂乳等も含み、また二種以上のタンパク質の混合
物も含むものである。このうち本発明では特に乳固形分
が0.1〜5 重量%、PH4.5以下の酸性飲料を対象
とする。これは乳固形分0.1%以下では風味の点でい
わゆるコクがなく、5%以上では粘度が高く清涼感に欠
けるからである。またPH4.5以下というのは、例え
ば乳酸菌の発酵により有機酸が生成する条件であり、こ
の条件のもとでは酸性飲料の嗜好に応じた調整が可能で
ある。因みにPHの調整は発酵の条件によって生成する
有機酸あるいは乳酸などの酸味料による調整でよい。
The constitutional requirements of the present invention will be specifically described below. First, the protein-containing acidic beverage of the present invention, whether animal or vegetable, includes, for example, pure protein, whole milk, skim milk, and the like, and also includes a mixture of two or more proteins. Of these, the present invention particularly targets acidic beverages having a milk solid content of 0.1 to 5% by weight and a pH of 4.5 or less. This is because when the solid content of milk is 0.1% or less, there is no so-called richness in terms of flavor and when it is 5% or more, the viscosity is high and the refreshing feeling is lacking. The pH of 4.5 or less is, for example, a condition under which an organic acid is produced by fermentation of lactic acid bacteria, and under this condition, it can be adjusted according to the taste of the acidic beverage. Incidentally, the pH can be adjusted by an organic acid produced by fermentation conditions or an acidulant such as lactic acid.

【0006】次にポリグリセリン脂肪酸エステルについ
て説明する。このものはポリグリセリンと、パルミチン
酸、ステアリン酸等の飽和脂肪酸またはオレイン酸、リ
ノール酸、リノレン酸等の不飽和脂肪酸とのモノ、ジあ
るいはトリエステルである。尚、トリステアリンのよう
な単純なエステルのほかに混合グリセリド(mixed glyc
eride)でもよい。本発明ではこのようなポリグリセリン
脂肪酸エステルのうち重合度6〜10でHLB8以上の
ものを適用する。尚、HLBとは親水性と疎水性との均
衡をいい、乳化剤が水あるいは油のどちらの傾向に近い
かを示す。HLB8以上のポリグリセリン脂肪酸エステ
ルは水に近い性状をもち、タンパク質となじみやすい性
状を示すものである。またポリグリセリン脂肪酸エステ
ルの添加量は0.005〜0.2重量%とする。これは
添加が0.005重量%以下では凝集物の発生防止がで
きず、逆に0.2重量%以上ではポリグリセリン脂肪酸
エステル自体の沈澱物を生じてしまうからである。
Next, the polyglycerin fatty acid ester will be described. These are mono-, di-, or triesters of polyglycerin and saturated fatty acids such as palmitic acid and stearic acid or unsaturated fatty acids such as oleic acid, linoleic acid, and linolenic acid. In addition to simple esters such as tristearin, mixed glycerides
eride). In the present invention, such polyglycerin fatty acid ester having a polymerization degree of 6 to 10 and an HLB of 8 or more is applied. HLB is a balance between hydrophilicity and hydrophobicity, and indicates whether the emulsifier has a tendency toward water or oil. The polyglycerin fatty acid ester having an HLB of 8 or more has a property close to that of water and exhibits a property of being easily compatible with proteins. The amount of polyglycerin fatty acid ester added is 0.005 to 0.2% by weight. This is because the addition of 0.005% by weight or less cannot prevent the generation of aggregates, and conversely, the addition of 0.2% by weight or more causes precipitation of the polyglycerin fatty acid ester itself.

【0007】本発明のタンパク質含有酸性飲料の構成要
素は以上述べたとおりであるが、その他ショ糖、果糖等
の甘味料、果汁、香料、油脂、色素成分あるいは炭酸ガ
ス等を必要に応じて添加してもよい。尚、本発明の飲料
は飲用時に水等で希釈する濃縮飲料を含むものである。
The components of the protein-containing acidic beverage of the present invention are as described above, but other sweeteners such as sucrose and fructose, fruit juices, flavors, oils and fats, pigment components, carbon dioxide and the like are added as necessary. You may. The beverage of the present invention contains a concentrated beverage that is diluted with water or the like when drinking.

【0008】[0008]

【実施例】【Example】

実施例1 発酵乳(乳固形分20%、乳酸酸度1.0%)15%重
量と、水に砂糖7重量%、オリゴ糖4重量%及びHLB
13のポリグリセリン脂肪酸エステル0.03%を加
え、糖、乳化剤溶液を作る。これに香料0.1%を入れ
て、50%乳酸溶液にてPH4.2とし、全量100%
とする。92℃までプレート殺菌機械にて加温し、85
℃で150kg/cm2の均質化をして、容器充填する。これ
を95℃で15分間殺菌し、冷却する。
Example 1 Fermented milk (milk solid content 20%, lactic acid degree 1.0%) 15% weight, sugar 7% by weight, oligosaccharide 4% by weight and HLB in water
Add 0.03% of polyglycerin fatty acid ester 13 to make sugar and emulsifier solution. Add 0.1% of fragrance to it and adjust to PH4.2 with 50% lactic acid solution, total 100%
And Warm up to 92 ° C with a plate sterilization machine, 85
Homogenize at 150 kg / cm 2 at ℃ and fill the container. It is sterilized at 95 ° C. for 15 minutes and cooled.

【0009】実施例2 発酵乳(乳固形分20%、乳酸酸度1.0%)15重量
%と、水に砂糖10重量%及びHLB11のポリグリセ
リン脂肪酸エステル0.03%を加え、糖、乳化剤溶液
を作る。これに香料0.2 0/2%、イチゴ果汁1%を入
れて、50%乳酸溶液にてPH3.8とし、全量100%
とする。92℃までプレート殺菌機械にて加温し、85
℃で150kg/cm2の均質化をして、容器充填する。これ
を95℃で15分間殺菌し、冷却する。
Example 2 Fermented milk (milk solid content 20%, lactic acid acidity 1.0%) 15% by weight, sugar 10% by weight and HLB11 polyglycerin fatty acid ester 0.03% were added to water to prepare a sugar and an emulsifier. Make a solution. Add 0.20 / 2% of fragrance and 1% of strawberry juice to pH 3.8 with 50% lactic acid solution, total 100%
And Warm up to 92 ° C with a plate sterilization machine, 85
Homogenize at 150 kg / cm 2 at ℃ and fill the container. It is sterilized at 95 ° C. for 15 minutes and cooled.

【0010】[0010]

【発明の効果】前記実施例1及び実施例2のタンパク質
含有酸性飲料を120日間室温で保存した。その結果、
実施例1では凝集もなく、沈澱のない口当たりのさっぱ
りした乳酸菌飲料となった。また実施例2も凝集、沈澱
がなく、口当たりのさっぱりした乳酸菌飲料となった。
The protein-containing acidic beverages of Examples 1 and 2 were stored at room temperature for 120 days. as a result,
In Example 1, there was no aggregation, and there was no precipitation, and the lactic acid bacterium drink had a refreshing mouthfeel. In addition, Example 2 was also a lactic acid bacterium beverage with no aggregation and precipitation and a refreshing mouthfeel.

【0011】また本発明の効果を追確認するための試験
品を以下の要領で作成した。 実験例 発酵乳(水79重量%に脱脂粉乳21重量%を加え、加
熱溶解し、90〜95℃で15分間殺菌し、冷却し、ラ
クトバチラス・ブルガリカスを用いて38℃で24時間
発酵して得られた乳酸酸度1.2重量%の乳固形分20
%のもの)25重量%と砂糖9重量%及びHLBがそれ
ぞれ異なる乳化剤を0.05重量%添加し、50%乳酸
溶液で所定のPHに調製し、水で100重量%とする。
このときのPHは4.2であった。次に90℃まで加熱
攪拌し、殺菌した後、85℃で均質化(150kg/cm2
する。これを容器に充填し、更に90℃で15分間殺菌
をする。この試験品の状態を観察した結果を下記に示
す。
Further, a test product for confirming the effect of the present invention was prepared in the following manner. Experimental Example Fermented milk (21% by weight of skim milk powder was added to 79% by weight of water, dissolved by heating, sterilized at 90 to 95 ° C for 15 minutes, cooled, and fermented at 38 ° C for 24 hours using Lactobacillus bulgaricus. 20 milk solids having a lactic acid content of 1.2% by weight
25% by weight), 9% by weight of sugar, and 0.05% by weight of emulsifiers different in HLB, and adjusted to a predetermined pH with a 50% lactic acid solution, and adjusted to 100% by weight with water.
The PH at this time was 4.2. Next, heat and stir to 90 ° C, sterilize, and homogenize at 85 ° C (150 kg / cm 2 )
To do. This is filled in a container and sterilized at 90 ° C. for 15 minutes. The results of observing the state of this test product are shown below.

【0012】 乳化剤 HLB 状 態 ポリグリセリン脂肪酸エステル 無添加 + 同上 2.6 + 同上 4.5 + 同上 7.0 + 同上 9.0 − 同上 11.6 − 同上 13.5 − 同上 16.0 − ショ糖脂肪酸エステル 3.0 + 同上 5.0 + 同上 7.0 + 同上 9.0 + 同上 11.0 + 同上 13.0 + 同上 19.0 + (表中の記号の意味 +:凝集あり −:凝集なし)Emulsifier HLB state Polyglycerin fatty acid ester not added + Id 2.6 + Id 4.5 + Id 7.0 + Id 9.0 − Id 11.6 − Id 13.5 − Id 16.0 − Sho Sugar fatty acid ester 3.0 + Same as above 5.0 + Same as above 7.0 + Same as above 9.0 + Same as above 11.0 + Same as above 13.0 + Same as above 13.0 + Same as above 19.0 + (Meaning of symbols in the table +: With aggregation −: (No aggregation)

【0013】この実験の結果から、ポリグリセリン脂肪
酸エステルのHLB8以上の乳化剤を使用することで乳
酸菌飲料の凝集を防止できた。従って本発明によって、
タンパク質による凝集、分離、沈澱を生ずることなく、
従来の安定剤やその他の乳化剤で防止できなかった風味
の良い、外観の良い乳酸菌飲料を製造できた。
From the results of this experiment, it was possible to prevent aggregation of the lactic acid bacterium beverage by using an emulsifier having a polyglycerin fatty acid ester of HLB 8 or higher. Therefore, according to the present invention,
Without protein aggregation, separation or precipitation
It was possible to produce a lactic acid bacterium beverage with a good taste and good appearance that could not be prevented by conventional stabilizers and other emulsifiers.

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 発酵乳の乳固形分が0.1〜5 重量%で
あり、PH4.5以下の酸性飲料において、HLB8以
上で重合度6〜10のポリグリセリン脂肪酸エステルが
0.005〜0.2重量%添加されて成ることを特徴と
するタンパク質含有酸性飲料。
1. A fermented milk having a milk solid content of 0.1 to 5% by weight and a pH of 4.5 or less, an HLB of 8 or more and a degree of polymerization of 6 to 10 of polyglycerin fatty acid ester is 0.005 to 0. A protein-containing acidic beverage characterized by being added at 2% by weight.
JP3358731A 1991-12-26 1991-12-26 Protein-containing acidic drink Pending JPH0686633A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP3358731A JPH0686633A (en) 1991-12-26 1991-12-26 Protein-containing acidic drink

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP3358731A JPH0686633A (en) 1991-12-26 1991-12-26 Protein-containing acidic drink

Publications (1)

Publication Number Publication Date
JPH0686633A true JPH0686633A (en) 1994-03-29

Family

ID=18460825

Family Applications (1)

Application Number Title Priority Date Filing Date
JP3358731A Pending JPH0686633A (en) 1991-12-26 1991-12-26 Protein-containing acidic drink

Country Status (1)

Country Link
JP (1) JPH0686633A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5715388A (en) * 1992-09-25 1998-02-03 Kohki Co., Ltd. Computer system for controlling an industrial robot subsystem which can monitor and detect abnormalities therein
WO2011115135A1 (en) * 2010-03-16 2011-09-22 三菱化学フーズ株式会社 Fat-containing acidic beverage
JP2017112995A (en) * 2015-12-18 2017-06-29 アサヒ飲料株式会社 Beverages containing microbial cells

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5715388A (en) * 1992-09-25 1998-02-03 Kohki Co., Ltd. Computer system for controlling an industrial robot subsystem which can monitor and detect abnormalities therein
WO2011115135A1 (en) * 2010-03-16 2011-09-22 三菱化学フーズ株式会社 Fat-containing acidic beverage
CN102791139A (en) * 2010-03-16 2012-11-21 三菱化学食品株式会社 Fat-containing acidic beverage
JP2016082988A (en) * 2010-03-16 2016-05-19 三菱化学フーズ株式会社 Fat-containing acidic beverage
JP5956924B2 (en) * 2010-03-16 2016-07-27 三菱化学フーズ株式会社 Fat-containing acidic beverage
JP2018174940A (en) * 2010-03-16 2018-11-15 三菱ケミカルフーズ株式会社 Fat-containing acidic beverage
JP2017112995A (en) * 2015-12-18 2017-06-29 アサヒ飲料株式会社 Beverages containing microbial cells
JP2022009095A (en) * 2015-12-18 2022-01-14 アサヒ飲料株式会社 Microbial bacterial cell-containing beverage

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