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JPH0647479B2 - Method for producing lightweight inorganic fiber - Google Patents

Method for producing lightweight inorganic fiber

Info

Publication number
JPH0647479B2
JPH0647479B2 JP62305568A JP30556887A JPH0647479B2 JP H0647479 B2 JPH0647479 B2 JP H0647479B2 JP 62305568 A JP62305568 A JP 62305568A JP 30556887 A JP30556887 A JP 30556887A JP H0647479 B2 JPH0647479 B2 JP H0647479B2
Authority
JP
Japan
Prior art keywords
fibers
fiber
adhesive
inorganic fiber
blowing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP62305568A
Other languages
Japanese (ja)
Other versions
JPS63274641A (en
Inventor
廣 清水
利勝 加治
昭 片島
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Chemical and Materials Co Ltd
Original Assignee
Nippon Steel Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Steel Chemical Co Ltd filed Critical Nippon Steel Chemical Co Ltd
Priority to JP62305568A priority Critical patent/JPH0647479B2/en
Publication of JPS63274641A publication Critical patent/JPS63274641A/en
Publication of JPH0647479B2 publication Critical patent/JPH0647479B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A30/00Adapting or protecting infrastructure or their operation
    • Y02A30/24Structural elements or technologies for improving thermal insulation
    • Y02A30/244Structural elements or technologies for improving thermal insulation using natural or recycled building materials, e.g. straw, wool, clay or used tires

Landscapes

  • Building Environments (AREA)
  • Manufacture, Treatment Of Glass Fibers (AREA)
  • Surface Treatment Of Glass Fibres Or Filaments (AREA)
  • Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
  • Nonwoven Fabrics (AREA)

Description

【発明の詳細な説明】 〔産業上の利用分野〕 本発明は住宅等の建造物へのブローイング工法に適した
軽量な無機繊維の製造方法に関する。
TECHNICAL FIELD The present invention relates to a method for producing a lightweight inorganic fiber suitable for a blowing method for a building such as a house.

〔従来の技術〕[Conventional technology]

住宅の天井裏や断熱材としてグラスファィバーやロック
ウールの成形品を使用することは知られており、これら
は繊維化後又は繊維の集綿後に接着剤を噴霧又は塗布等
の方法によりマット状に成型し、接着剤を完全に硬化さ
せるために圧縮や加熱処理によって製造されている。
It is known to use molded products of glass fiber and rock wool for the ceilings of houses and heat insulation materials, and these are formed into a mat by spraying or applying an adhesive after fiberization or fiber collection. It is molded and manufactured by compression or heat treatment to completely cure the adhesive.

しかしながら、これらの成型品は100mm以上の厚い製
品がなく、施工の結果隙間ができるので断熱性能上問題
があり、また、結露などの発生原因となっている。
However, these molded products do not have a thick product of 100 mm or more, and a gap is formed as a result of the construction, so that there is a problem in heat insulation performance, and it causes dew condensation.

そのため、ブローイング工法(吹き込み工法)によりロ
ックウールを任意の厚さに吹き込むことが行われている
が、この際に、通常のロックウールを使用し、住宅の天
井裏や壁に吹き込んで断熱施工とすると、通常40〜6
0kg/m3の密度となる。これは、単位面積当たりの重量
にすると、例えば100mmの厚さに吹き込むと4〜6kg
/m2となり、天井を構成する材料、即ち野縁や天井板、
吊り木の補強が必要となる他、ロックウールの使用量が
多くなり経済的ではないという問題点があった。
For this reason, rock wool is blown to a desired thickness by the blowing method (blowing method), but at this time, ordinary rock wool is used to blow it into the ceiling and walls of the house for insulation. Then usually 40-6
The density is 0 kg / m 3 . This is 4-6 kg when blown into a thickness of 100 mm, for example, in terms of weight per unit area.
/ M 2, and the material constituting the ceiling, i.e. ceiling joists and the ceiling board,
In addition to the need to reinforce the hanging tree, there was a problem that the amount of rock wool used was large and it was not economical.

〔発明が解決しようとする問題点〕[Problems to be solved by the invention]

本発明の目的はブローイング工法に好適な軽量な無機繊
維の製造方法を提供することにある。
An object of the present invention is to provide a method for producing a lightweight inorganic fiber suitable for a blowing method.

〔問題点を解決するための手段〕[Means for solving problems]

本発明者らは上記のような問題点を解決するため研究を
行い、繊維化された繊維が冷却される前に少量の接着剤
を吹きつけ繊維が保有する熱により繊維同志を部分的に
固着させることにより、外力に対して変形しにくく軽量
な密度のブローイング用ロックウールが得られることを
見出し、本発明を完成した。
The present inventors have conducted research to solve the above-mentioned problems, and spray a small amount of adhesive before the fiberized fiber is cooled to partially fix the fibers by heat held by the fiber. It was found that by doing so, it is possible to obtain a rocking wool for blowing, which is hard to be deformed by an external force and has a light weight, and completed the present invention.

すなわち、本発明は高温の無機質溶融体を遠心力や気流
の作用により繊維化する際に、繊維化された繊維が冷却
される前に少量の接着剤を吹きつけ、加熱、圧縮するこ
となく繊維が保有する熱により接着剤の硬化および/ま
たは脱溶剤を行わせしめることにより繊維同志を部分的
に接着したバルク状又はマット状とすることを特徴とす
る軽量な無機繊維の製造方法である。
That is, the present invention, when fibrating the high temperature inorganic melt by the action of centrifugal force or air flow, spray a small amount of adhesive before the fibrous fibers are cooled, and heat and compress the fibers without compression. Is a method for producing a lightweight inorganic fiber, characterized in that the adhesive is cured and / or the solvent is removed by the heat retained therein to form a partially bonded bulk or matted fiber.

高温の無機質溶融体とは無機質繊維の原料を溶融したも
のであり、例えばロックウールは製鉄所等で副生するス
ラグあるいは安山岩や玄武岩等の天然鉱石をキュポラ、
電気炉等で溶解したものである。次にこの高温の無機質
溶融体は蒸気等の圧力気体又は遠心力により吹製して繊
維化される。繊維化と同時に、又は後であって、まだ冷
却しない内に公知の方法により接着剤を噴霧する。
The high temperature inorganic melt is a melt of the raw material of the inorganic fiber, for example rockwool is a slag by-produced in a steel mill or a natural ore such as andesite or basalt cupola,
It is melted in an electric furnace. Next, this high-temperature inorganic melt is blown into a fiber by pressure gas such as steam or centrifugal force. At the same time as or after the fiberization, the adhesive is sprayed by a known method while not cooling.

接着剤としては熱硬化性樹脂、水溶性でない熱可塑性樹
脂が使用できる。熱硬化性樹脂としてはフェノール樹
脂、尿素−ホルムアルデヒド樹脂、アクリル酸エステル
共重合体、メラミン−ホルムアルデヒド樹脂、エポキシ
樹脂等が、熱可塑性樹脂としてはポリ酢酸ビニル系のも
のが挙げられる。これらの接着剤のうち固形のものは溶
剤溶液、エマルジョンの形で使用してもよい。
A thermosetting resin or a water-insoluble thermoplastic resin can be used as the adhesive. Examples of the thermosetting resin include phenol resin, urea-formaldehyde resin, acrylic acid ester copolymer, melamine-formaldehyde resin and epoxy resin, and examples of the thermoplastic resin include polyvinyl acetate type. Of these adhesives, solid ones may be used in the form of solvent solution or emulsion.

接着剤の付着量は一般の成型品の場合は1〜3%である
が、本発明ではその1/10〜1/3 程度の0.1 〜1.0 %、好
ましくは0.1 〜0.5 %である。付着量が0.1 %以下では
繊維同志が強固に固着されず、また1.0 %以上では繊維
と繊維の間に接着剤が入り込み、密度が高くなるために
好ましくない。
The amount of adhesive adhered is 1 to 3% in the case of a general molded product, but in the present invention, it is 0.1 to 1.0%, preferably 1 to 0.5%, which is about 1/10 to 1/3 of that. If the adhered amount is 0.1% or less, the fibers are not firmly fixed to each other, and if the adhered amount is 1.0% or more, the adhesive enters between the fibers to increase the density, which is not preferable.

接着剤を噴霧された繊維は移動コンベア上に繊維を連続
的に気流と共に流すことによって集綿されるが、この時
点で繊維は約100〜200℃の温度を有しているた
め、接着剤は硬化および/または脱溶剤され繊維同志を
部分的に接着したバルク状又はマット状として形成され
る。
The fibers sprayed with the adhesive are collected on the moving conveyor by continuously flowing the fibers with an air stream, at which point the fibers have a temperature of about 100-200 ° C. It is cured and / or desolvated and formed as a bulk or mat in which the fibers are partially adhered.

このものは、バルク状の場合にはこのままで、マット状
のものは公知の手段によって切断等を行った後にブロー
イングマシン等によって住宅等の天井裏や壁等に吹き込
み断熱材層を形成される。
This is as it is in the case of a bulk, while the mat is cut by a known means and then blown into a ceiling or wall of a house or the like by a blowing machine or the like to form a heat insulating material layer.

〔作 用〕[Work]

本発明では繊維化時に少量の接着剤を噴霧することによ
り、集綿時の保有熱によって接着剤を硬化させるため、
繊維が部分的に接着し、更に圧縮や加熱の処理をする必
要がなく軽量なブローイング用ロックウールを得ること
ができる。
In the present invention, by spraying a small amount of adhesive at the time of fiberizing, the adhesive is cured by the heat retained during cotton collection,
It is possible to obtain a lightweight rockwool for blowing, in which fibers are partially adhered and there is no need to further perform compression or heating.

〔実施例〕〔Example〕

実施例1 高炉スラグ90%、珪石10%をキュポラ炉で溶融し、
遠心力により繊維化すると同時に、水溶性フェノール樹
脂を固形分として該繊維に対して0.3%付着させた。
集綿時の繊維は約100〜200℃の温度を保有してお
り、フェノール樹脂中の水分は蒸発し、なおかつ樹脂も
硬化しており、特にオーブン等による加熱処理は必要と
しなかった。
Example 1 90% blast furnace slag and 10% silica were melted in a cupola furnace,
At the same time as fiberization by centrifugal force, a water-soluble phenolic resin was attached as solid content to the fiber in an amount of 0.3%.
The fibers at the time of collecting the cotton had a temperature of about 100 to 200 ° C., the water content in the phenol resin was evaporated, and the resin was hardened, so that the heat treatment with an oven or the like was not particularly required.

このバルク状繊維をブローイングマシンで吹き込み施工
した結果、20kg/m3の密度で外力に対して変形しにく
い軽い断熱層を得た。
As a result of blowing the bulk fibers with a blowing machine, a light heat insulating layer having a density of 20 kg / m 3 which is not easily deformed by an external force was obtained.

実施例2 実施例1の原料を溶融して繊維化するときに固形分30
%、粘度4000poise の酢酸ビニルエマルジョンを繊
維に対して0.25%付着させた。
Example 2 When the raw material of Example 1 is melted and made into fiber, the solid content is 30.
%, A vinyl acetate emulsion having a viscosity of 4000 poise was adhered to the fibers in an amount of 0.25%.

得られた繊維は実施例1同様オーブン等の加熱処理を必
要としなかった。
The obtained fiber did not require heat treatment in an oven as in Example 1.

このバルク状繊維をブローイングマシンで吹き込み施工
した結果、22kg/m3の密度で外力に対して変形しにく
い軽い断熱層を得た。
As a result of blowing and applying this bulk fiber with a blowing machine, a light heat-insulating layer having a density of 22 kg / m 3 and being hard to be deformed by an external force was obtained.

実施例3 溶融スラグ90%、珪石10%を電気炉で溶融し、遠心
力により繊維化する同時に、固形分50%のアクリル酸
エステル共重合体エマルジョンを繊維に対して0.5%
付着させた。
Example 3 90% of molten slag and 10% of silica stone were melted in an electric furnace and were made into fibers by centrifugal force. At the same time, 0.5% of acrylic acid ester copolymer emulsion having a solid content of 50% was added to the fibers.
Attached.

これにより得られたバルク状繊維をブローイングマシン
で吹き込み施工した結果、19kg/m3の密度で外力に対
して変形しにくい軽い断熱層を得た。
The bulk fibers thus obtained were blown with a blowing machine, and as a result, a light heat insulating layer with a density of 19 kg / m 3 which was not easily deformed by external force was obtained.

〔発明の効果〕〔The invention's effect〕

以上の説明から明らかなように、本発明によれば繊維同
志を少量の接着剤により部分的に集綿時の保有熱によっ
て固着することにより、接着剤を硬化させるための圧縮
や加熱の処理をすることなく外力に対して変形しにく
く、軽量なロックウールが得られる。このロックウール
を使用することによって、断熱層を経済的に施工するこ
とができる。
As is clear from the above description, according to the present invention, the fibers are partially fixed by a small amount of the adhesive by the retained heat at the time of collecting the cotton, so that the compression and the heat treatment for curing the adhesive can be performed. Without being deformed, it is hard to be deformed by external force, and lightweight rock wool can be obtained. By using this rock wool, the heat insulation layer can be economically constructed.

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】高温の無機質溶融体を遠心力や気流の作用
により繊維化する際に、繊維化された繊維が冷却される
前に少量(繊維に対し0.1〜1%)の接着剤を吹きつ
け、加熱、圧縮することなく繊維が保有する熱により接
着剤の硬化および/または脱溶剤を行わしめることによ
り繊維同志を部分的に接着したバルク状又はマット状と
することを特徴とするブローイング工法用の軽量な無機
繊維の製造方法。
1. A small amount (0.1 to 1% with respect to the fiber) of the adhesive before the fiberized fiber is cooled when the high-temperature inorganic melt is fiberized by the action of centrifugal force or air flow. Characterized in that the fibers are partially adhered to each other in a bulk or mat shape by curing the adhesive and / or removing the solvent by the heat held by the fibers without spraying, heating and compressing. A method for producing a lightweight inorganic fiber for a blowing method.
JP62305568A 1986-12-16 1987-12-04 Method for producing lightweight inorganic fiber Expired - Fee Related JPH0647479B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP62305568A JPH0647479B2 (en) 1986-12-16 1987-12-04 Method for producing lightweight inorganic fiber

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP29776086 1986-12-16
JP61-297760 1986-12-16
JP62305568A JPH0647479B2 (en) 1986-12-16 1987-12-04 Method for producing lightweight inorganic fiber

Publications (2)

Publication Number Publication Date
JPS63274641A JPS63274641A (en) 1988-11-11
JPH0647479B2 true JPH0647479B2 (en) 1994-06-22

Family

ID=26561223

Family Applications (1)

Application Number Title Priority Date Filing Date
JP62305568A Expired - Fee Related JPH0647479B2 (en) 1986-12-16 1987-12-04 Method for producing lightweight inorganic fiber

Country Status (1)

Country Link
JP (1) JPH0647479B2 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4241514C2 (en) * 1992-12-10 1995-09-07 Freudenberg Carl Fa Method for producing a sheet loaded with dipoles and device for carrying out the method
WO2021175404A1 (en) * 2020-03-03 2021-09-10 Grenzebach Bsh Gmbh Integrated plant for refuse incineration and for producing rock wool, and method for operating the plant

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5153024A (en) * 1974-10-29 1976-05-11 Asahi Fibreglass Co
JPS59102830A (en) * 1982-11-30 1984-06-14 Nitto Boseki Co Ltd Method for applying processing liquid to inorganic short fiber and apparatus therefor

Also Published As

Publication number Publication date
JPS63274641A (en) 1988-11-11

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