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JPH06299188A - Method for improving fats and oils - Google Patents

Method for improving fats and oils

Info

Publication number
JPH06299188A
JPH06299188A JP5091145A JP9114593A JPH06299188A JP H06299188 A JPH06299188 A JP H06299188A JP 5091145 A JP5091145 A JP 5091145A JP 9114593 A JP9114593 A JP 9114593A JP H06299188 A JPH06299188 A JP H06299188A
Authority
JP
Japan
Prior art keywords
oils
fats
oil
colored
filtration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP5091145A
Other languages
Japanese (ja)
Inventor
Takashi Iguchi
喬 井口
Koichi Sugita
浩一 杉田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NIPPON SHIYOKUZAI KAKO KK
Original Assignee
NIPPON SHIYOKUZAI KAKO KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NIPPON SHIYOKUZAI KAKO KK filed Critical NIPPON SHIYOKUZAI KAKO KK
Priority to JP5091145A priority Critical patent/JPH06299188A/en
Publication of JPH06299188A publication Critical patent/JPH06299188A/en
Pending legal-status Critical Current

Links

Landscapes

  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Edible Oils And Fats (AREA)
  • General Preparation And Processing Of Foods (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Fats And Perfumes (AREA)

Abstract

PURPOSE:To decolorize and deodorize fats and oils, colored or having off-flavor or unpleasant smell and produced in a step for thermally extracting the fats and oils from animal tissues. CONSTITUTION:Fats and oils, colored or having off-flavor such as scorch smell are filtered through a polyolefinic micro-filtration membrane to afford decolorized fats and oils without the off-flavor. Thereby, the fats and oils, colored or having the scorch smell can be decolorized and deodorized.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は油脂の改良方法に関す
る。動物から採取した油脂は、採取時の加熱や原料の種
類、鮮度により、着色したり、異臭がついたりするの
で、膜処理により着色とこれらの異臭を除去した油脂を
製造する。
FIELD OF THE INVENTION The present invention relates to a method for improving fats and oils. Since oils and fats collected from animals are colored and have an offensive odor depending on the heating at the time of extraction, the type of raw material, and the freshness, oils and fats that are colored and have these offensive odors removed by a membrane treatment are produced.

【0002】[0002]

【従来の技術】油脂はタンパク質、炭水化物と並んで重
要な食品成分であり、栄養とおいしさに果たす役割は大
きく、植物、動物などから製造されている。
2. Description of the Related Art Oils and fats are important food ingredients as well as proteins and carbohydrates, and play a large role in nutrition and deliciousness, and are produced from plants and animals.

【0003】一般に、動物油脂は動物脂肪組織を加熱す
ることにより得られる。この加熱工程で油脂が茶色に着
色したり、油脂がもともともっていない、こげ臭などの
フレーバーが生じる。また、油脂自体に不快臭が存在す
ることもある。
Animal fats and oils are generally obtained by heating animal adipose tissue. In this heating step, the fats and oils are colored brown, or the fats and oils are not accompanied, and flavors such as burnt odor occur. In addition, unpleasant odor may be present in the oil or fat itself.

【0004】油脂を食品用途に使用する場合、そのかお
りや色がしばしば問題になることが多い。
When oils and fats are used for food applications, their scent and color are often a problem.

【0005】例えばインスタントラーメンのスープやス
ナックに使用する油脂には素材の特色のいかされたフレ
ーバーが好まれ、場合によっては各種シーズニングフレ
ーバーが添加され、官能的に改良されることが多い。し
かし、使用する油脂に不快なコゲ臭があると油脂そのも
のが持つフレーバーを損なうばかりか、シーズニングフ
レーバーによる香味づけを妨げることがある。
For example, for the fats and oils used for instant ramen soups and snacks, flavors with the characteristics of the raw materials are preferred, and in some cases various seasoning flavors are added to improve the taste in many cases. However, if the fats and oils used have an unpleasant burnt odor, not only the flavors of the fats and oils themselves are impaired, but also the flavoring by the seasoning flavors may be disturbed.

【0006】また、色についても、油脂をスープ、ドレ
ッシングなどに使用して、それらを著しく着色してしま
う時は、食品としての価値を減少させてしまう。
[0006] Regarding the color, when oils and fats are used for soups, dressings, etc. and they are markedly colored, their value as food is reduced.

【0007】そこで、食用油の製造においては脱色、不
快臭の脱臭は重要な課題である。
Therefore, decolorization and deodorization of unpleasant odors are important problems in the production of edible oil.

【0008】食用油の製造において、脱色は一般的に活
性白土によって行われている。また、油脂(幸書房、19
91年、44巻、522号、61ページ)に記載があるとおり、
活性白土と活性炭の併用によって脱色効率を上昇させる
方法も知られている。ここでは、活性白土、活性炭を8
5:15に混合し、90℃で処理する方法が紹介されてい
る。
In the production of edible oils, decolorization is generally carried out with activated clay. In addition, fats and oils (Koshobo, 19
(1991, 44, 522, p. 61)
There is also known a method of increasing decolorization efficiency by using activated clay and activated carbon in combination. Here, activated clay and activated carbon 8
The method of mixing at 5:15 and treating at 90 ℃ is introduced.

【0009】また、脱臭については活性炭を使用して行
う事が可能である。
Deodorization can be performed using activated carbon.

【0010】[0010]

【本発明が解決しようとする問題点】しかしながら、活
性炭や活性炭と活性白土の混合の使用後には大量の廃物
が出来、廃棄に手間がかかる。また、廃棄した活性炭に
よる環境汚染の心配もある。しかも、処理した油脂が廃
棄物のケーキに大量に吸収されるので歩留りが悪くなる
欠点を有する。そこで、廃棄物が出ず、歩留のよい油脂
の脱色、脱臭の方法が望まれている。
[Problems to be Solved by the Invention] However, a large amount of waste is produced after use of activated carbon or a mixture of activated carbon and activated clay, and it takes time to dispose. In addition, there is concern about environmental pollution due to discarded activated carbon. In addition, the treated oil and fat is absorbed in a large amount in the waste cake, resulting in a poor yield. Therefore, a method of decolorizing and deodorizing fats and oils that does not produce waste and has a good yield is desired.

【0011】[0011]

【課題を解決するための手段】本発明者らは、上記課題
を解決するために種々検討した結果、本発明を完成する
にいたった。
As a result of various studies to solve the above-mentioned problems, the inventors of the present invention have completed the present invention.

【0012】本発明は、廃棄物のでない、効率のよい油
脂の脱色、脱臭方法に関する。
The present invention relates to an efficient method for decolorizing and deodorizing fats and oils which is not waste.

【0013】すなわち、本発明においてはポリオレフィ
ン系の精密濾過膜で濾過を行うことにより濾過液側にこ
げ臭のない、脱色された油脂を得ることができる。
That is, in the present invention, a decolorized oil or fat having no burning odor on the filtrate side can be obtained by performing filtration with a polyolefin-based microfiltration membrane.

【0014】使用する精密濾過膜としては旭化成工業製
の精密濾過モジュールPSP-003、PSP-013,PMP-003,PMP-0
13,PSP-103,PSP-113、PMP-102,PMP-113,PSV-303,PSV-31
3,PMV-302,PMV-313,PMP-302,PMP-313などが使用できる
が、他社製品でもポリオレフィン系の膜であれば使用で
きる。
The microfiltration membrane used is a microfiltration module PSP-003, PSP-013, PMP-003, PMP-0 manufactured by Asahi Kasei.
13, PSP-103, PSP-113, PMP-102, PMP-113, PSV-303, PSV-31
3, PMV-302, PMV-313, PMP-302, PMP-313, etc. can be used, but products of other companies can also be used as long as they are polyolefin-based membranes.

【0015】また、膜の形態も平膜型、中空糸型、スパ
イラル型のいずれでも使用できる。
The form of the membrane may be any of flat membrane type, hollow fiber type and spiral type.

【0016】[0016]

【実施例1】以下、実施例により本発明を具体的に説明
する。豚の脂身(内臓脂を含む)3tを、敷油としてポー
クオイル1tを予め入れておいた釜に入れ、140℃になる
まで約3.5時間かけて加熱した。加熱終了後、パーコレ
ーターで粗カスと抽出した油脂を分離し、油脂中に含ま
れる細かい残渣を除去するためにフィルタープレスで濾
過を行い、ポークオイル1.5tを得た。
[Embodiment 1] The present invention will be described in detail below with reference to an embodiment. 3 t of pork fat (including visceral fat) was placed in a kettle in which 1 t of pork oil was added beforehand as bedding oil, and heated to 140 ° C for about 3.5 hours. After the heating was completed, the coarse dust was separated from the extracted fats and oils by a percolator, and filtration was performed by a filter press to remove fine residues contained in the fats and oils to obtain 1.5 t of pork oil.

【0017】このようにして製造したポークオイルはポ
リオレフィン系の精密濾過膜で濾過した。はじめに、ペ
ンシル型モジュール専用の卓上型濾過装置「PS-24001」
(旭化成工業製)にペンシル型モジュールPMP-013を装
着し、エチルアルコール100mlを系内に通し、モジュー
ル内、装置系内をアルコールに置換した。このエチルア
ルコールの処理は繰り返し3回行った。その後ヘキサン
でモジュール内と系内を置換した。
The pork oil thus produced was filtered through a polyolefin-based microfiltration membrane. First, a desktop type filtration device for pencil type modules "PS-24001"
A pencil type module PMP-013 was attached to (Asahi Kasei Co., Ltd.), 100 ml of ethyl alcohol was passed through the system, and the inside of the module and the system of the apparatus were replaced with alcohol. This treatment with ethyl alcohol was repeated 3 times. After that, the inside of the module and the inside of the system were replaced with hexane.

【0018】ポークオイルを50℃に加熱溶解し、モジュ
ール、系内をヘキサンの臭いが完全にとれるまでポーク
オイルで洗浄し、ポークオイル100gを入口圧力1.0kgf/c
m2、出口圧力を0.5kgf/cm2で50℃で濾過した。濾過液が
50gになってから濾過を停止した。
Melt the pork oil at 50 ° C., wash the inside of the module and system with pork oil until the odor of hexane is completely removed, and add 100 g of pork oil to an inlet pressure of 1.0 kgf / c.
It was filtered at 50 ° C. with m 2 and outlet pressure of 0.5 kgf / cm 2 . The filtrate is
The filtration was stopped after reaching 50 g.

【0019】濾過終了後、脱色の程度を評価したとこ
ろ、脱色率は43%であった。ここでいう脱色率とは、(1
-濾過液の430nmのOD/濾過前液の430nmのOD)×100で表
される指標である。
After the completion of filtration, the degree of decolorization was evaluated, and the decolorization rate was 43%. The decolorization rate here is (1
-OD at 430 nm of filtered solution / OD at 430 nm of unfiltered solution) x 100.

【0020】また、臭いは、5人のパネラーによって評
価し、濾過前液と濾過液を比較したところ、表1に示し
た通り、全員が濾過前液のコゲ臭が濾過液では除去され
ていると評価した。
The odor was evaluated by five panelists and the pre-filtration liquid and the filtration liquid were compared. As shown in Table 1, all the kogation odors of the pre-filtration liquid were removed by the filtration liquid. It was evaluated.

【表1】 [Table 1]

【0021】[0021]

【実施例2】鶏の尻部脂肪3tを、チキンオイル1tを予め
入れておいた釜に入れ、140℃になるまで約3.5時間かけ
て加熱した。加熱終了後、パーコレーターで粗カスと抽
出した油脂を分離し、油脂中に含まれる細かい残渣を除
去するためにフィルタープレスで濾過を行い、チキンオ
イル鶏脂1.6tを得た。
[Example 2] 3 t of chicken buttocks fat was placed in a kettle in which 1 t of chicken oil had been placed in advance and heated to 140 ° C for about 3.5 hours. After the heating was completed, the coarse dust and the extracted fat and oil were separated by a percolator, and filtered with a filter press to remove fine residues contained in the fat and oil to obtain 1.6 t of chicken oil chicken fat.

【0022】このようにして製造したチキンイルはポリ
オレフィン系の精密濾過膜で濾過した。はじめに、ペン
シル型モジュール専用の卓上型濾過装置「PS-24001」
(旭化成工業製)にペンシル型モジュールPMP-013を装
着し、エチルアルコール100mlを系内に通し、モジュー
ル内、装置系内をアルコールに置換した。このエチルア
ルコールの処理は繰り返し3回行った。その後ヘキサン
でモジュール内と系内を置換した。
The chicken il thus produced was filtered through a polyolefin-based microfiltration membrane. First, a desktop type filtration device for pencil type modules "PS-24001"
A pencil type module PMP-013 was attached to (Asahi Kasei Co., Ltd.), 100 ml of ethyl alcohol was passed through the system, and the inside of the module and the system of the apparatus were replaced with alcohol. This treatment with ethyl alcohol was repeated 3 times. After that, the inside of the module and the inside of the system were replaced with hexane.

【0023】チキンオイルを50℃に加熱溶解し、モジュ
ール、系内をヘキサンの臭いが完全にとれるまでチキン
オイルで洗浄し、チキンイル100gを入口圧力1.0kgf/c
m2、出口圧力を0.5kgf/cm2で濾過を行った。濾過液が50
gになってから濾過を停止した。
[0023] Chicken oil was dissolved by heating at 50 ° C, and the module and system were washed with chicken oil until the odor of hexane was completely removed, and 100 g of chicken yl was introduced at an inlet pressure of 1.0 kgf / c.
Filtration was performed at m 2 and outlet pressure of 0.5 kgf / cm 2 . 50 filtrate
The filtration was stopped after reaching g.

【0024】濾過終了後、脱色の程度を評価したとこ
ろ、脱色率は32%であった。ここでいう脱色率とは、(1
-濾過液の430nmのOD/濾過前液の430nmのOD)×100で表
される指標である。
After the completion of filtration, the degree of decolorization was evaluated and the rate of decolorization was 32%. The decolorization rate here is (1
-OD at 430 nm of filtered solution / OD at 430 nm of unfiltered solution) x 100.

【0025】また、臭いは、5人のパネラーによって評
価し、濾過前液と濾過液比較したところ、表2に示した
通り、全員が濾過前液のコゲ臭が濾過液では除去されて
いると評価した。
Further, the odor was evaluated by five panelists, and the pre-filtration liquid and the filtration liquid were compared, and as shown in Table 2, it was found that the kogation odor of the pre-filtration liquid was removed by the filtration liquid in all of them. evaluated.

【表2】 [Table 2]

【0026】[0026]

【発明の効果】以上説明したように本発明によれば着
色、コゲ臭のある油脂を精密濾過膜を使用して、活性炭
や活性炭と活性白土混合物を使用したときの様に、新た
な廃棄物を生成することなくを脱色、コゲ臭除去ができ
る。
As described above, according to the present invention, a colored waste oil having a burnt odor is used as a new waste material by using a microfiltration membrane and activated carbon or a mixture of activated carbon and activated clay. It is possible to decolorize and remove kogation odor without producing.

───────────────────────────────────────────────────── フロントページの続き (51)Int.Cl.5 識別記号 庁内整理番号 FI 技術表示箇所 C11B 3/10 2115−4H ─────────────────────────────────────────────────── ─── Continuation of the front page (51) Int.Cl. 5 Identification code Office reference number FI technical display location C11B 3/10 2115-4H

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】油脂をポリオレフィン系の精密濾過膜で濾
過することを特徴とする脱色方法。
1. A decolorizing method, which comprises filtering oils and fats through a polyolefin-based microfiltration membrane.
【請求項2】油脂をポリオレフィン系の精密濾過膜で濾
過することを特徴とするフレーバーの改良方法
2. A method for improving flavor, which comprises filtering an oil or fat with a polyolefin microfiltration membrane.
JP5091145A 1993-04-19 1993-04-19 Method for improving fats and oils Pending JPH06299188A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP5091145A JPH06299188A (en) 1993-04-19 1993-04-19 Method for improving fats and oils

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP5091145A JPH06299188A (en) 1993-04-19 1993-04-19 Method for improving fats and oils

Publications (1)

Publication Number Publication Date
JPH06299188A true JPH06299188A (en) 1994-10-25

Family

ID=14018364

Family Applications (1)

Application Number Title Priority Date Filing Date
JP5091145A Pending JPH06299188A (en) 1993-04-19 1993-04-19 Method for improving fats and oils

Country Status (1)

Country Link
JP (1) JPH06299188A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014508806A (en) * 2011-03-25 2014-04-10 クーパーラブス リミテッド Thermally extracted net extract, composition thereof, method of preparation and use thereof
JP2015501851A (en) * 2011-11-09 2015-01-19 エボニック メンブレイン イクストラクション テクノロジー リミテッドEvonik Membrane Extraction Technology Ltd. Membrane-based method and composition resulting therefrom for producing a concentrate comprising a non-marine fatty acid oil mixture for reducing at least one impurity and comprising at least one natural ingredient

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014508806A (en) * 2011-03-25 2014-04-10 クーパーラブス リミテッド Thermally extracted net extract, composition thereof, method of preparation and use thereof
JP2015501851A (en) * 2011-11-09 2015-01-19 エボニック メンブレイン イクストラクション テクノロジー リミテッドEvonik Membrane Extraction Technology Ltd. Membrane-based method and composition resulting therefrom for producing a concentrate comprising a non-marine fatty acid oil mixture for reducing at least one impurity and comprising at least one natural ingredient

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