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JPH04142061A - Formation of tungsten plug - Google Patents

Formation of tungsten plug

Info

Publication number
JPH04142061A
JPH04142061A JP26451890A JP26451890A JPH04142061A JP H04142061 A JPH04142061 A JP H04142061A JP 26451890 A JP26451890 A JP 26451890A JP 26451890 A JP26451890 A JP 26451890A JP H04142061 A JPH04142061 A JP H04142061A
Authority
JP
Japan
Prior art keywords
tungsten
film
wiring
interconnection
layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP26451890A
Other languages
Japanese (ja)
Inventor
Toshiaki Hasegawa
利昭 長谷川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sony Corp
Original Assignee
Sony Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sony Corp filed Critical Sony Corp
Priority to JP26451890A priority Critical patent/JPH04142061A/en
Publication of JPH04142061A publication Critical patent/JPH04142061A/en
Pending legal-status Critical Current

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Abstract

PURPOSE:To make the coverage of an upper-layer interconnection good, to prevent the upper-layer interconnection from becoming thin at an opening part for interconnection and to prevent a void by a method wherein tungsten is grown selectively on tungsten which is left inside the opening part for interconnection use. CONSTITUTION:A contact hole 11a as an opening part for interconnection is made in an layer insulating film 11 deposited on a silicon substrate 10 and composed of SiO2. After that, a titanium nitride (TiN) film 12 as a close contact layer is applied to be thin; then, blanket tungsten 13A is formed so as to be filled into the contact hole 11a and to be applied onto the layer insulating film 11. The tungsten film 13A and the titanium nitride film 12 are etched back; the tungsten film 13A inside the contact hole 11a is overetched; selective tungsten 13B is grown selectively on the tungsten film 13A; an aluminum interconnection 14 is formed. Thereby, the coverage of an upper-layer interconnection is made good.

Description

【発明の詳細な説明】 [産業上の利用分野] 本発明は、半導体装置製造における配線技術に関し、特
に、コンタクトホール等に埋め込まれるタングステンプ
ラグの形成方法に係わる。
DETAILED DESCRIPTION OF THE INVENTION [Field of Industrial Application] The present invention relates to wiring technology in semiconductor device manufacturing, and particularly to a method for forming tungsten plugs embedded in contact holes and the like.

[発明の概要: 本発明は、タングステンプラグの形成方法において、 絶縁膜に配線用開口部を形成する工程と、前記絶縁膜」
−及び前記配線用開口部内にタングステンをブランケッ
ト成長させて該配線用開口部を密に埋め込む工程と、前
記タングステンにエッチバックを施し前記配線用開口部
の開口縁よりも下方にタングステンが残留するようにオ
ーバーエツチングする工程と、前記配線用開口部内のタ
ングステン上にさらにタングステンを選択成長させて該
配線用開口部を埋め込む工程を備えることにより、配線
用開口部の開口面に対して窪みのないタングステンプラ
グを形成し、上層配線の被覆性(カバレッジ)を良好に
して配線の信頼性を向上し得るようにしたものである。
[Summary of the Invention: The present invention provides a method for forming a tungsten plug, comprising: a step of forming a wiring opening in an insulating film; and a step of forming a wiring opening in an insulating film.
- a step of blanket growing tungsten in the wiring opening to densely bury the wiring opening, and etching back the tungsten so that the tungsten remains below the edge of the wiring opening. By over-etching the tungsten in the wiring opening, and further selectively growing tungsten on the tungsten in the wiring opening to fill the wiring opening, tungsten can be formed without making a depression with respect to the opening surface of the wiring opening. A plug is formed to improve the coverage of the upper layer wiring, thereby improving the reliability of the wiring.

[従来の技術〕 次世代の超々LSIプロセスでの最大の課題は、配線技
術といってよい。第2図に示すように、従来のアルミニ
ウム配線3ては、例えばノリコン基板l−ヒの層間絶縁
膜2に開口したコンタクトホール2a内にボイド4を生
じた状態で形成されるなとの問題を有している。このよ
うな、アルミニウム配線の膜被覆性(ステップカバレッ
ジ)やマイグレーンヨン耐性の低下は、微細化に伴う薄
膜化で著しくなる。このため、ステップカバレッジが良
く、しかも従来のポリンリコンプラグなどと比較してコ
ンタクト抵抗を低くする、ブランケットタングステンC
VDとエッチバックを組み合せたプロセス技術が注目を
集めている。
[Prior Art] The biggest challenge in next-generation ultra-super LSI processes can be said to be wiring technology. As shown in FIG. 2, the conventional aluminum wiring 3 has a problem in that it is formed with voids 4 in the contact holes 2a opened in the interlayer insulating film 2 of the Noricon substrate 1, for example. have. Such decreases in film coverage (step coverage) and migration resistance of aluminum wiring become more significant as the film becomes thinner with miniaturization. For this reason, the blanket tungsten C plug has good step coverage and lower contact resistance compared to conventional polycarbonate plugs.
Process technology that combines VD and etchback is attracting attention.

この方法は、第3図Aに示すように、例えばシリコン基
板1上の層間絶縁膜2にコンタクトホール2aを開口し
た後、窒化チタン、チタンオキシナイトライドなとてな
る密着層4を被着させ、その後、タングステン層5を気
相成長法(CVD)によりブランケット成長させる。
In this method, as shown in FIG. 3A, for example, after a contact hole 2a is opened in an interlayer insulating film 2 on a silicon substrate 1, an adhesion layer 4 made of titanium nitride or titanium oxynitride is deposited. Thereafter, the tungsten layer 5 is blanket grown by vapor phase epitaxy (CVD).

次に、第3図Bに示すようにタングステン層5のエッチ
バックを行ない、コンタクトホール2a内のみにタング
ステン層(タングステンプラグ)5を残し、次いて、第
3図Cに示すように、アルミニウム配線6をスパッタ法
により形成して上層配線とする。
Next, as shown in FIG. 3B, the tungsten layer 5 is etched back to leave the tungsten layer (tungsten plug) 5 only in the contact hole 2a, and then, as shown in FIG. 3C, the aluminum wiring is etched back. 6 is formed by a sputtering method to form an upper layer wiring.

[発明が解決しようとする課題” しかしながら、上記した方法は、エッチバックの終点判
定が難しく、コンタクトホール以外のタングステン層が
エッチバックされたところでエツチングされるタングス
テンの量が急激に減るため、エッチャントがコンタクト
ホール内のタングステンプラグに集中し、第3図Bに示
すように、コンタクトホールの開口縁より下方までオー
バーエツチングされてしまう問題点があった。
[Problems to be Solved by the Invention] However, with the above method, it is difficult to determine the end point of etchback, and the amount of tungsten etched decreases rapidly when the tungsten layer other than the contact hole is etched back. There was a problem in that the tungsten plug in the contact hole was concentrated and overetched to a point below the opening edge of the contact hole, as shown in FIG. 3B.

また、絶縁膜に段差がある場合(例えばゲート電極上方
など)にタングステンが残るため、このタングステンを
除去するためには逆に上記したオーバーエツチングは必
要であるとされている。
Furthermore, since tungsten remains when there is a step in the insulating film (for example, above the gate electrode), the above-mentioned overetching is said to be necessary in order to remove this tungsten.

しかし、第3図Cに示すように、このようにタングステ
ンプラグかオーバーエツチングされた状態で上層配線と
してのアルミニウム配線6をスパッタ法などにより形成
した場合、段差部分のアルミニウム膜厚か薄くなり、ま
1こ、ともするとボイドを生しるため、ストレスマイグ
レーノヨンやエレクトロマイグレーノヨンを起し、配線
の信頼性を悪くする問題点を有している。
However, as shown in FIG. 3C, when the aluminum wiring 6 as the upper layer wiring is formed by sputtering or the like with the tungsten plug over-etched, the thickness of the aluminum film at the stepped portion becomes thinner and the aluminum wiring 6 becomes thinner. First, since voids are often formed, stress migration and electromigration are caused, resulting in poor wiring reliability.

本発明は、このような問題点に着目して創案されたもの
であって、配線用開口部とタングステンプラグによる段
差をなくし、上層配線の信頼性を向上させるタングステ
ンプラグの形成方法を提供するものである。
The present invention was devised in view of these problems, and provides a method for forming a tungsten plug that eliminates the level difference between the wiring opening and the tungsten plug and improves the reliability of the upper layer wiring. It is.

1課題を解決するための手段で そこで、本発明は、絶縁膜に配線用開口部を形成する工
程と、前記絶縁膜上及び前記配線用開口部内にタングス
テンをブランケット成長させて該配線用開口部を密に埋
め込む工程と、前記タングステンにエッチバックを施し
前記配線用開口部の開口縁よりも下方にタングステンが
残留するようにオーバーエツチングする工程と、前記配
線用開口部内のタングステン上にさらにタングステンを
選択成長させて該配線用開口部を埋め込む工程を備える
ことを、その解決方法としている。
In order to solve the above problems, the present invention includes a step of forming a wiring opening in an insulating film, and blanket growing tungsten on the insulating film and in the wiring opening. a step of etch-backing the tungsten and over-etching so that tungsten remains below the opening edge of the wiring opening; A solution to this problem is to include a step of selectively growing and burying the wiring opening.

1作用− 配線用開口部内に残留するタングステン上にタングステ
ンを選択成長させることにより、配線用開口部を埋め込
み、上層配線のカバレッジを良好にし、上層配線が配線
用開口部で薄膜化やボイドを生ずるのを防止する。この
ため、上層配線にストレスマイグレーノヨンやエレクト
ロマイグレーンヨンを生しることが防止でき、配線の信
頼性が向上する。
1 Effect - By selectively growing tungsten on the tungsten remaining in the wiring opening, the wiring opening is filled, the coverage of the upper layer wiring is improved, and the upper layer wiring becomes thinner and voids occur in the wiring opening. to prevent Therefore, it is possible to prevent stress migration or electromigration from occurring in the upper layer wiring, and the reliability of the wiring is improved.

[実施伊に 以下、本発明に係るタングステンプラグの形成方法の詳
細を図面に示す実施例に基づいて説明する。
[Practice] The details of the method for forming a tungsten plug according to the present invention will be explained below based on examples shown in the drawings.

本実施例は、先ず、第1図Aに示すように、シリコン基
板1上に堆積したSi’Oyでなる層間絶縁膜11に、
配線用開口部であるコンタクトポールIlaを開口した
後、密着層としての窒化チタン(T i N)膜12を
CVD法もしくはスパッタ法により薄く被着させ、次に
、CVD法によりブランケットタングステン(以下タン
グステン膜と称する)13Aを形成し、コンタクトポー
ル11a内を埋め込むと共に層間絶縁膜ll上に被着さ
せる。
In this embodiment, first, as shown in FIG. 1A, an interlayer insulating film 11 made of Si'Oy deposited on a silicon substrate 1 is
After opening the contact pole Ila, which is an opening for wiring, a thin titanium nitride (T i N) film 12 as an adhesion layer is deposited by CVD or sputtering, and then blanket tungsten (hereinafter referred to as tungsten) is deposited by CVD. A film (referred to as a film) 13A is formed, embedding the inside of the contact pole 11a, and depositing it on the interlayer insulating film ll.

このCVD条件は、2段階の工程を行なった。Under these CVD conditions, a two-step process was performed.

以下、その条件を示す。The conditions are shown below.

(第1段階の条件) 雰囲気ガス及びその流量 六フッ化タングステン(WF’8)・・・255ccx
シラン(S i H4)       −15scc。
(First stage conditions) Atmospheric gas and its flow rate Tungsten hexafluoride (WF'8)...255ccx
Silane (S i H4) -15scc.

温度        ・・・475℃ 圧力        −80T o r r(第2段階
の条件) 雰囲気ガス及びその流量 六フッ化タングステン(WFe)・・・60 SCCM
水素(H7)         ・36osCCイ温度
         ・475℃ 圧力        ・・80TOrr次に、第1図B
に示すように、タングステン膜13A及び窒化チタン膜
12をエッチバックする。
Temperature...475℃ Pressure -80T o r r (second stage conditions) Atmospheric gas and its flow rate Tungsten hexafluoride (WFe)...60 SCCM
Hydrogen (H7) ・36osCC Temperature ・475℃ Pressure ・・80TOrr Next, Figure 1 B
As shown in FIG. 2, the tungsten film 13A and the titanium nitride film 12 are etched back.

このエッチバックにより、コンタクトホール11a内の
タングステン膜13Aをオーバーエツチングし、層間絶
縁膜Il上のタングステン膜+3A・及び窒化チタン膜
12を確実に除去する。
By this etchback, the tungsten film 13A in the contact hole 11a is overetched, and the tungsten film +3A and the titanium nitride film 12 on the interlayer insulating film Il are reliably removed.

なお、このエッチバックの条件は、以下に示す通りであ
る。
Note that the conditions for this etchback are as shown below.

エツチングガス ・・・六フッ化イオウ(SF3)ガス
流量    ・・・405CCM 圧力      ・I OmT o r rマイクロ波
出力  850W RFバイアス  ・I 00V (2MHz)次に、第
1図Cに示すように、タングステン膜13A上に選択タ
ングステン(以下タングステン膜と称する)13BをC
VD法にて選択成長させる。
Etching gas: Sulfur hexafluoride (SF3) Gas flow rate: 405CCM Pressure: I OmT or r Microwave output: 850W RF bias: I00V (2MHz) Next, as shown in Figure 1C, tungsten Selective tungsten (hereinafter referred to as tungsten film) 13B is deposited on the film 13A.
Selective growth is performed using the VD method.

このCVD条件は、以下に示す通りである。The CVD conditions are as shown below.

雰囲気ガス及びその流量 六フッ化タングステン(WFe)・I O8CrMンラ
ン(S i H4)      −7、CCM水素(H
2)        ・・・1000s。、温度   
         ・・・2608C圧力      
      −200m T orr上記したタングス
テン膜13Bの選択成長は、コンタクトホールllaの
開口縁に至る程度まで行なってコンタクトホールlla
を埋め込み、タングステンプラグ13の形成が完了する
Atmospheric gas and its flow rate Tungsten hexafluoride (WFe) IO8CrM (S i H4)
2) ...1000s. ,temperature
...2608C pressure
-200 m Torr The above-described selective growth of the tungsten film 13B is performed to the extent that it reaches the opening edge of the contact hole lla.
, and the formation of the tungsten plug 13 is completed.

次に、第1図りに示すように、アルミニウム配線14を
スパッタ法等により形成すれば、上層配線が形成できる
Next, as shown in the first diagram, an upper layer wiring can be formed by forming aluminum wiring 14 by sputtering or the like.

本実施例においては、コンタクトホール1 ]、 a内
にタングステンプラグ13を段差を生ぜずに形成できる
ため、上層配線のカバレッジが良好となり、配線の信頼
性が向上する。
In this embodiment, since the tungsten plug 13 can be formed in the contact hole 1], a without creating a step, the coverage of the upper layer wiring is improved and the reliability of the wiring is improved.

以上、実施例について説明したが、本発明は、これに限
られるものではなく、各種の設計変更が可能である。
Although the embodiments have been described above, the present invention is not limited thereto, and various design changes are possible.

[発明の効果1 以−Lの説明から明らかなように、本発明に係るタング
ステンプラグの形成方法によれば、コンタクトホールな
どの配線用開口部においてタングステンプラグによる凹
部が形成されないため、上層配線のカバレッジを良好に
し、配線の信頼性を高める効果がある。
[Effect of the Invention 1] As is clear from the explanation in L below, according to the method for forming a tungsten plug according to the present invention, no recess is formed by the tungsten plug in an opening for wiring such as a contact hole, so that the upper layer wiring is This has the effect of improving coverage and improving wiring reliability.

【図面の簡単な説明】[Brief explanation of drawings]

第1図A〜第1図りは本発明に係るタングステンプラグ
の形成方法の実施例を示す断面図、第2図はアルミニウ
ムを用いた従来例の断面図、第3図A〜第3図Cはタン
グステンを用いた従来例の断面図である。 11 ・層間絶縁膜、lla・コンタクトホール、13
 ・タングステンプラグ、+3A、13B・・タングス
テン膜、14・・アルミニウム配線(上層配線)。 110コンタクト庁、−ル 丈3乞1夕11の工)1Σ斤、10Jv面 口第1図A (亨二 万t 1り11) 第1図B (支脆1y11) 第1図C (笑止1夕11) 第1図D 20コンタクト汀\−ル アルミニウムΣ用いた4乏来うダ10?面図第2図 20コンタクト汀、−ル 第3図C
1A to 1D are cross-sectional views showing an embodiment of the method for forming a tungsten plug according to the present invention, FIG. 2 is a cross-sectional view of a conventional example using aluminum, and FIGS. 3A to 3C are FIG. 2 is a cross-sectional view of a conventional example using tungsten. 11 ・Interlayer insulating film, lla・contact hole, 13
- Tungsten plug, +3A, 13B...Tungsten film, 14...Aluminum wiring (upper layer wiring). 110 Contact Agency, - Length 3 years 1 night 11 work) 1Σ cat, 10 Jv side Mouth Figure 1 A (Kyo 2 million tons 1ri 11) Figure 1 B (support 1y11) Figure 1 C (lol stop 1 E11) Fig. 1D 20 contacts using aluminum Σ4 less than 10? Top view Figure 2 20 Contact base Figure 3 C

Claims (1)

【特許請求の範囲】[Claims] (1)絶縁膜に配線用開口部を形成する工程と、前記絶
縁膜上及び前記配線用開口部内にタングステンをブラン
ケット成長させて該配線用開口部を密に埋め込む工程と
、 前記タングステンにエッチバックを施し前記配線用開口
部の開口縁よりも下方にタングステンが残留するように
オーバーエッチングする工程と、前記配線用開口部内の
タングステン上にさらにタングステンを選択成長させて
該配線用開口部を埋め込む工程を備えることを特徴とす
るタングステンプラグの形成方法。
(1) forming a wiring opening in an insulating film; blanket-growing tungsten on the insulating film and in the wiring opening to densely fill the wiring opening; and etching back the tungsten. a step of over-etching so that tungsten remains below the opening edge of the wiring opening, and a step of selectively growing tungsten on the tungsten in the wiring opening to fill the wiring opening. A method for forming a tungsten plug, comprising:
JP26451890A 1990-10-02 1990-10-02 Formation of tungsten plug Pending JPH04142061A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP26451890A JPH04142061A (en) 1990-10-02 1990-10-02 Formation of tungsten plug

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP26451890A JPH04142061A (en) 1990-10-02 1990-10-02 Formation of tungsten plug

Publications (1)

Publication Number Publication Date
JPH04142061A true JPH04142061A (en) 1992-05-15

Family

ID=17404365

Family Applications (1)

Application Number Title Priority Date Filing Date
JP26451890A Pending JPH04142061A (en) 1990-10-02 1990-10-02 Formation of tungsten plug

Country Status (1)

Country Link
JP (1) JPH04142061A (en)

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US5633201A (en) * 1992-11-30 1997-05-27 Hyundai Electronics Industries, Co., Ltd. Method for forming tungsten plugs in contact holes of a semiconductor device
KR100321141B1 (en) * 1994-12-30 2002-05-13 박종섭 Method for fabricating semiconductor device
CN104272441A (en) * 2012-03-27 2015-01-07 诺发系统公司 Tungsten feature fill
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US10256142B2 (en) 2009-08-04 2019-04-09 Novellus Systems, Inc. Tungsten feature fill with nucleation inhibition
US10381266B2 (en) 2012-03-27 2019-08-13 Novellus Systems, Inc. Tungsten feature fill with nucleation inhibition
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US11437269B2 (en) 2012-03-27 2022-09-06 Novellus Systems, Inc. Tungsten feature fill with nucleation inhibition
US11549175B2 (en) 2018-05-03 2023-01-10 Lam Research Corporation Method of depositing tungsten and other metals in 3D NAND structures
US11972952B2 (en) 2018-12-14 2024-04-30 Lam Research Corporation Atomic layer deposition on 3D NAND structures
US11978666B2 (en) 2018-12-05 2024-05-07 Lam Research Corporation Void free low stress fill
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Cited By (42)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
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