[go: up one dir, main page]

JPH02277527A - Filter of liquid chemical - Google Patents

Filter of liquid chemical

Info

Publication number
JPH02277527A
JPH02277527A JP1098024A JP9802489A JPH02277527A JP H02277527 A JPH02277527 A JP H02277527A JP 1098024 A JP1098024 A JP 1098024A JP 9802489 A JP9802489 A JP 9802489A JP H02277527 A JPH02277527 A JP H02277527A
Authority
JP
Japan
Prior art keywords
filter
carbon dioxide
pure water
valve
valves
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP1098024A
Other languages
Japanese (ja)
Other versions
JPH088978B2 (en
Inventor
Seiichi Kumagai
誠一 熊谷
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NEC Kyushu Ltd
Original Assignee
NEC Kyushu Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NEC Kyushu Ltd filed Critical NEC Kyushu Ltd
Priority to JP1098024A priority Critical patent/JPH088978B2/en
Publication of JPH02277527A publication Critical patent/JPH02277527A/en
Publication of JPH088978B2 publication Critical patent/JPH088978B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Landscapes

  • Separation Using Semi-Permeable Membranes (AREA)
  • Filtration Of Liquid (AREA)
  • Cleaning Or Drying Semiconductors (AREA)

Abstract

PURPOSE:To smoothly allow liquid chemical to permeate through a filter medium by equipping a feed port and a discharge port of gaseous carbon dioxide so that gaseous carbon dioxide is passed through the filter and discharged. CONSTITUTION:The valves A, C and the valves E, F are closed and a filter 1 is replaced. Thereafter the valves E, F are opened and gaseous carbon dioxide is passed until the air of the inside has been completely substituted with gaseous carbon dioxide and the valve E is closed. Then the valve C is opened to introduce pure water. After the primary-side inside of the filter 1 has been completely filled with pure water, the valve F is closed and a valve D is opened. At this time, pure water reaches the secondary side of the filter because the gaseous carbon dioxide in a filter medium is dissolved into pure water. Gaseous carbon dioxide in the secondary side is discharged together with pure water through the valve D. Thereafter the valves C, D are closed and the valves A, B are opened and liquid chemical is allowed to flow. Thereby the filter medium is efficiently utilized.

Description

【発明の詳細な説明】 〔産業上の利用分野〕 本発明は薬液濾過装置に関し、特に半導体基板処理に使
用する無機薬液の微粒子除去を行なう薬液濾過装置に関
する。
DETAILED DESCRIPTION OF THE INVENTION [Field of Industrial Application] The present invention relates to a chemical liquid filtration apparatus, and more particularly to a chemical liquid filtration apparatus for removing particulates from an inorganic chemical liquid used in semiconductor substrate processing.

〔従来の技術〕[Conventional technology]

従来、この種の濾過器は、濾材を内蔵し、薬液の流入口
及び流出口を有し、この流入口、流出口に接続する配管
により構成されていた。
Conventionally, this type of filter has a built-in filter medium, has an inlet and an outlet for the chemical liquid, and is configured by piping connected to the inlet and the outlet.

〔発明が解決しようとする課題〕[Problem to be solved by the invention]

上述した従来の濾過器は、交換に際し、濾材が弗素樹脂
膜でできているため疎水性となっており、無機薬液の濾
過を行なう場合は、あらかじめ濾材をアルコールで浸漬
し、純水でアルコールを洗浄する作業を行なった後、薬
液配管を接続する様になっているので、薬液配管を接続
する作業の過程で濾材が乾燥し、薬液の濾材透過が円滑
に行なわれないという欠点がある。
When replacing the conventional filter described above, the filter medium is made of a fluororesin membrane and is therefore hydrophobic, so when filtering an inorganic chemical solution, soak the filter medium in alcohol in advance and remove the alcohol with pure water. Since the chemical liquid piping is connected after the cleaning operation is performed, there is a drawback that the filter medium dries during the process of connecting the chemical liquid piping, and the chemical liquid cannot pass through the filter medium smoothly.

本発明の目的は、弗素樹脂膜の濾材を有する濾過器の交
換に際し、直ちに薬液配管を行ない、薬液の透過を行な
うことができる薬液濾過装置を提供することにある。
An object of the present invention is to provide a chemical liquid filtration device that allows the chemical liquid to be permeated by immediately connecting chemical liquid piping when replacing a filter having a fluororesin membrane filter medium.

〔発明が解決しようとする課題〕[Problem to be solved by the invention]

本発明の薬液濾過装置は、弗素樹脂膜を濾材とする濾過
器と、炭酸ガスが濾過器を通って排出する様配管接続し
た炭酸ガス供給口及び排出口と、濾過器の薬液流入口に
接続した純水供給口及び薬液流出口に接続した純水排出
口とを有している。
The chemical liquid filtration device of the present invention includes a filter using a fluororesin membrane as a filter medium, a carbon dioxide gas supply port and a discharge port connected to pipes so that carbon dioxide gas passes through the filter, and a chemical liquid inlet of the filter. and a pure water outlet connected to the chemical solution outlet.

〔実施例〕〔Example〕

次に、本発明について図面を参照して説明する。第1図
は本発明の一実施例の配管系統図である。濾過器1の薬
液流入口1aに接続するバルブA及びCと、薬液流出口
1bに接続するバルブB及びDと、濾過器2次側へ通ず
る接続口ICに接続するバルブE及び1次側へ通ずる接
続口1dに接続するバルブFを閉じ、濾過器1を交換し
た後、バルブE及びFを開は炭酸ガスを内部の空気か完
全に炭酸ガスと置換するまで通じ、バルブEひ閉める。
Next, the present invention will be explained with reference to the drawings. FIG. 1 is a piping system diagram of one embodiment of the present invention. Valves A and C connected to the chemical inlet 1a of the filter 1, valves B and D connected to the chemical outlet 1b, and valve E connected to the connection port IC leading to the secondary side of the filter and to the primary side. After closing the valve F connected to the connecting port 1d and replacing the filter 1, the valves E and F are opened until the carbon dioxide gas is completely replaced with the air inside, and the valve E is closed.

次にバルブCを開け、純水を導入し、濾過器1の1次側
内が完全に純水で満たされた後、バルブFを閉じバルブ
Dを開ける。この時濾材内の炭酸ガスが純水に溶解する
事により純水が濾過器2次側に達する。2次側内炭酸ガ
スをバルブDより純水とともに排出した後、バルブC及
びDを閉じ、バルブA及びBを開は薬液を流す。
Next, valve C is opened, pure water is introduced, and after the primary side of filter 1 is completely filled with pure water, valve F is closed and valve D is opened. At this time, the carbon dioxide gas in the filter medium is dissolved in the pure water, and the pure water reaches the secondary side of the filter. After the carbon dioxide gas in the secondary side is discharged from valve D along with pure water, valves C and D are closed, and valves A and B are opened to allow the chemical solution to flow.

第2図は本発明の他の実施例の配管系統図である。濾過
器1の、ハウジング部を下側に取付は濾過器1の1次側
へ通ずる接続口1dにバルブEを接続し、2次側へ通ず
る接続口1cにバルブFを接続し、第1の実施例と同手
順により炭酸カスをバルブEを開は導入し、バルブFよ
り排出し、純水及び薬液と順次置換する。この実施例で
は、炭酸ガスを濾過器1の1次側より導入する構造であ
るため、炭酸ガス中の微粒子が2次側にはいらないとい
う利点がある。
FIG. 2 is a piping system diagram of another embodiment of the present invention. To install the filter 1 with the housing part on the lower side, connect the valve E to the connection port 1d leading to the primary side of the filter 1, connect the valve F to the connection port 1c leading to the secondary side, and connect the valve F to the connection port 1c leading to the secondary side. Following the same procedure as in the example, carbon dioxide sludge is introduced by opening valve E, is discharged from valve F, and is sequentially replaced with pure water and a chemical solution. In this embodiment, since the structure is such that carbon dioxide gas is introduced from the primary side of the filter 1, there is an advantage that fine particles in the carbon dioxide gas do not enter the secondary side.

〔発明の効果〕〔Effect of the invention〕

以上説明したように本発明は、薬液配管を接続した状態
で、空気から炭酸ガスに完全に置換し、炭酸ガスが純水
に溶解しやすい事を利用し、濾材の細孔内に純水を浸透
させて、炭酸ガスと純水を完全に置換し、無機薬液が純
水に溶解する事により、無機薬液と純水が完全に置換し
、弗素崩脂膜の濾材を効率良く使用できる効果がある。
As explained above, the present invention completely replaces air with carbon dioxide gas while the chemical pipe is connected, and takes advantage of the fact that carbon dioxide gas easily dissolves in pure water to fill the pores of the filter medium with pure water. By permeating the water, the carbon dioxide gas and pure water are completely replaced, and the inorganic chemical solution is dissolved in the pure water.The inorganic chemical solution and pure water are completely replaced, and the filter medium of the fluoride fat-breaking membrane can be used efficiently. be.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は本発明の一実施例の薬液濾過装置の配管系統図
、第2図は本発明の他の実施例の配管系統図である。 1・・・濾過器、1a・・・薬液流入口、1b・・・薬
液流出口、IC・・・2次側接続口、1d・・・1次側
接続口、A・・・薬液流入バルブ、B・・・薬液流出バ
ルブ、C・・・純水供給バルブ、D・・・純水排出バル
ブ、E・・・炭酸ガス供給バルブ、F・・・炭酸ガス排
出バルブ。
FIG. 1 is a piping system diagram of a chemical liquid filtration apparatus according to one embodiment of the present invention, and FIG. 2 is a piping system diagram of another embodiment of the present invention. 1...Filter, 1a...Medical solution inlet, 1b...Medical solution outlet, IC...Secondary side connection port, 1d...Primary side connection port, A...Medical solution inflow valve , B... Chemical solution outflow valve, C... Pure water supply valve, D... Pure water discharge valve, E... Carbon dioxide gas supply valve, F... Carbon dioxide gas discharge valve.

Claims (1)

【特許請求の範囲】[Claims] 薬液の供給配管、若しくは、薬液貯槽の循環式濾過機構
に於いて使用する弗素樹脂膜を用いた濾過器と、炭酸ガ
スが濾過器を通って排出する様配管接続した炭酸ガス供
給口及び排出口と、濾過器の薬液流入口に接続した純水
供給口及び薬液流出口に接続した純水排出口とを有する
事を特徴とする薬液濾過装置。
A filter using a fluororesin membrane used in the chemical supply piping or the circulation filtration mechanism of the chemical storage tank, and a carbon dioxide gas supply port and discharge port connected to the pipe so that carbon dioxide gas passes through the filter and is discharged. A chemical liquid filtration device comprising: a pure water supply port connected to a chemical liquid inlet of the filter; and a pure water outlet connected to a chemical liquid outlet of the filter.
JP1098024A 1989-04-17 1989-04-17 Chemical filter device Expired - Lifetime JPH088978B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP1098024A JPH088978B2 (en) 1989-04-17 1989-04-17 Chemical filter device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP1098024A JPH088978B2 (en) 1989-04-17 1989-04-17 Chemical filter device

Publications (2)

Publication Number Publication Date
JPH02277527A true JPH02277527A (en) 1990-11-14
JPH088978B2 JPH088978B2 (en) 1996-01-31

Family

ID=14208350

Family Applications (1)

Application Number Title Priority Date Filing Date
JP1098024A Expired - Lifetime JPH088978B2 (en) 1989-04-17 1989-04-17 Chemical filter device

Country Status (1)

Country Link
JP (1) JPH088978B2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04246828A (en) * 1991-02-01 1992-09-02 Nec Kyushu Ltd Cleaning device of semiconductor wafer

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04246828A (en) * 1991-02-01 1992-09-02 Nec Kyushu Ltd Cleaning device of semiconductor wafer

Also Published As

Publication number Publication date
JPH088978B2 (en) 1996-01-31

Similar Documents

Publication Publication Date Title
US5507959A (en) Apparatus for wetting, flushing and performing integrity checks on encapsulated PTFE filters
US4961759A (en) Closed loop gas dehydration process and apparatus
TWI690941B (en) Method of removing radioactive gases and hydrogen gas from a nuclear reactor coolant
KR20190005843A (en) Starting method of ultrapure water producing device
CN205164515U (en) Membrane module
JP2003299937A (en) Performance evaluation method for reverse osmosis membrane element
JPH02277527A (en) Filter of liquid chemical
JP4867180B2 (en) Immersion membrane separator and chemical cleaning method therefor
US6210646B1 (en) Permanganate feeder for iron filter
JPS60183018A (en) Specimen water filtering apparatus for water quality measuring instrument
JPS62149304A (en) Filter
KR20150079091A (en) High-Flux Pressured Membrane Module Water-Purifying Apparatus and Water-Purifying Apparatus and the method of inspecting membrane break
KR20140071660A (en) A gravity ballasting system and a method of back-flushing a filter using the same
JP2004074091A (en) Cleaning method of filtration membrane
TWI869621B (en) Ultrapure water supply system, control device, and ultrapure water supply program
JP2012239936A (en) Water treatment method and apparatus
KR102395961B1 (en) Eco-friendly cleaning apparatus submurged tubular filtration membrane and the cleaning method using this
CN221760793U (en) Tower-free water supply device
JPH11137978A (en) Membrane contaminant removing method of membrane separation device
CN221607883U (en) A soft water production system
CN118888278A (en) Carrier gas injection oscillation negative pressure oil-gas separation device for transformers
JPH0999226A (en) Washing method of membrane
JPS6287205A (en) Method for washing hollow yarn membrane filter
KR20030042428A (en) Method for treating power plant heater drain water
JPS60500560A (en) Pre-primed filter device and method of manufacturing the same