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JP6835487B2 - Stirrer - Google Patents

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JP6835487B2
JP6835487B2 JP2016116501A JP2016116501A JP6835487B2 JP 6835487 B2 JP6835487 B2 JP 6835487B2 JP 2016116501 A JP2016116501 A JP 2016116501A JP 2016116501 A JP2016116501 A JP 2016116501A JP 6835487 B2 JP6835487 B2 JP 6835487B2
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stirring
stirring tank
shape
wall
tank
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JP2017217635A (en
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幸雄 江田
幸雄 江田
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Denka Co Ltd
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Denka Co Ltd
Denki Kagaku Kogyo KK
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Description

本発明は、撹拌装置に関する。 The present invention relates to a stirrer.

熱交換することにより被撹拌物の温度を調整しながら撹拌する撹拌装置として、伝熱特性向上の目的で撹拌槽内に伝熱コイルを配置し、上記伝熱コイルへの電力を調整して被撹拌物の昇温速度を制御するもの(例えば、特許文献1参照)、撹拌槽の外部に熱源を配置し撹拌槽を介して内部の被撹拌物の温度を調整するもの(例えば、特許文献2、3参照)が開示されている。また、被撹拌物の温度均一化等の目的で被撹拌物を強制的に撹拌する撹拌装置として、撹拌槽内にバッフル(邪魔板)を設けるもの(例えば、特許文献4、5参照)が提案されている。 As a stirring device that stirs while adjusting the temperature of the object to be agitated by exchanging heat, a heat transfer coil is arranged in the stirring tank for the purpose of improving the heat transfer characteristics, and the power to the heat transfer coil is adjusted to be covered. Those that control the temperature rise rate of the agitated material (see, for example, Patent Document 1), those that arrange a heat source outside the agitating tank and adjust the temperature of the agitated object inside via the agitating tank (for example, Patent Document 2). 3, 3) is disclosed. Further, as a stirring device for forcibly stirring the material to be agitated for the purpose of making the temperature of the material to be agitated uniform, a device provided with a baffle (jamming plate) in the stirring tank (see, for example, Patent Documents 4 and 5) has been proposed. Has been done.

これらのうち、伝熱コイルを配置するものは直接的な伝熱により温度調整能に優れ、撹拌槽の外部に熱源を配置するものは撹拌槽内への被撹拌物の収容量に優れている。また、撹拌槽内にバッフルを設けるものは、被撹拌物の反応によって生じた反応生成物や発生した熱エネルギーの拡散を促進して撹拌槽内の被撹拌物の温度および濃度ムラを抑制することができる点で優れている。 Of these, the one in which the heat transfer coil is arranged is excellent in temperature control ability by direct heat transfer, and the one in which the heat source is arranged outside the stirring tank is excellent in the capacity of the object to be agitated in the stirring tank. .. In addition, if a baffle is provided in the stirring tank, the reaction product generated by the reaction of the material to be stirred and the generated thermal energy are diffused to suppress the temperature and concentration unevenness of the material to be stirred in the stirring tank. It is excellent in that it can be done.

特開2001―224951号公報Japanese Unexamined Patent Publication No. 2001-224951 特許第5220544号公報Japanese Patent No. 5220544 特許第5249419号公報Japanese Patent No. 5249419 特開2009−18274号公報Japanese Unexamined Patent Publication No. 2009-18274 特開2013−151621号公報Japanese Unexamined Patent Publication No. 2013-151621

しかしながら、上述した撹拌装置のうち、伝熱コイルを配置するものは、伝熱コイルとの物理的な接触を避けるために撹拌翼のサイズが制限されたり、伝熱コイル近傍で被撹拌物の滞留により温度や濃度ムラが生じたり、伝熱コイルの腐食(酸化劣化など)防止のために被撹拌物および伝熱コイルの組合せが制限されるという難点がある。 However, among the above-mentioned stirring devices, those in which the heat transfer coil is arranged have a limitation in the size of the stirring blade in order to avoid physical contact with the heat transfer coil, or the object to be agitated stays in the vicinity of the heat transfer coil. This causes uneven temperature and concentration, and there is a problem that the combination of the object to be agitated and the heat transfer coil is restricted in order to prevent corrosion (oxidation deterioration, etc.) of the heat transfer coil.

また、撹拌槽の外部に熱源を配置するものは撹拌槽のスケールアップに伴い伝熱効率が低下する傾向にあり、これにより高容量の熱源が必要になったり、温調に時間が掛かったりするという難点がある。さらに、撹拌槽内にバッフルを設けるものは、濃度および温度分布の均一化や、未反応部の低減が期待できるものの、バッフルの背面などにおいて局所的に被撹拌物の滞留部が発生する虞があり、加えてバッフルが設けられている分、撹拌翼の自由な形状選定の障害にもなり易い。 In addition, if the heat source is placed outside the stirring tank, the heat transfer efficiency tends to decrease as the stirring tank is scaled up, which requires a high-capacity heat source and takes time to control the temperature. There are drawbacks. Further, in the case where the baffle is provided in the stirring tank, it is expected that the concentration and temperature distribution will be uniform and the unreacted part will be reduced, but there is a possibility that the stagnant part of the material to be agitated is locally generated on the back surface of the baffle. In addition, since the baffle is provided, it tends to be an obstacle to the free shape selection of the stirring blade.

本発明は、以上のような事情に基づいてなされたものであり、その目的は、被撹拌物の温度を迅速かつ確実に調整することができると共に、上記被撹拌物の温度および濃度の均一化に優れる撹拌装置を提供することにある。 The present invention has been made based on the above circumstances, and an object of the present invention is to be able to quickly and surely adjust the temperature of the agitated object and to make the temperature and concentration of the agitated object uniform. It is an object of the present invention to provide an excellent stirring device.

本発明は、
(1)温度を調整しながら被撹拌物を撹拌する撹拌装置であって、
前記被撹拌物を内部に収容する撹拌槽と、
前記撹拌槽の外部に設けられ、前記撹拌槽を介して前記被撹拌物の温度を調整する温調手段と、
前記撹拌槽内に配置され、前記被撹拌物を回転しながら撹拌する撹拌翼と、
撹拌軸を介して前記撹拌翼に接続され、前記撹拌翼を回転駆動する駆動手段とを備え、
前記撹拌槽の内壁の少なくとも一部が所定の凹凸形状に形成されていることを特徴とする撹拌装置、
(2)撹拌槽の内壁の表面積が、前記内壁が平坦であると仮定したときの仮想内壁の表面積の1.1倍超である前記(1)に記載の撹拌装置、
(3)撹拌槽の内壁の少なくとも一部の粗さが、算術平均粗さ(Ra)で1.0μm以下である前記(1)または(2)に記載の撹拌装置、
(4)凹凸形状が撹拌軸方向に周期的に形成されている前記(1)から(3)のいずれか1項に記載の撹拌装置、
(5)凹凸形状における凹部と凸部との高低差が10mm以上40mm以下であり、かつ前記凹凸形状の周期が100mm以上である前記(4)に記載の撹拌装置、
(6)撹拌槽を撹拌軸に直交する投影面に投影したときの投影像において、前記撹拌軸を横断する内壁間の寸法の最小値が、凹凸形状における凹部と凸部との高低差の最大値の4倍超である前記(1)から(5)のいずれか1項に記載の撹拌装置、
(7)凹凸形状における凹部および凸部のそれぞれの形状が、球面形状、楕円面形状、円錐面形状および多角錐面形状からなる群より選ばれる少なくとも1種の形状の一部を含んでいる前記(1)から(6)のいずれか1項に記載の撹拌装置、並びに
(8)撹拌槽が、ステンレス鋼、銅またはアルミニウムを主成分とする金属材料で形成されている前記(1)から(7)のいずれか1項に記載の撹拌装置
に関する。
The present invention
(1) A stirring device that stirs an object to be agitated while adjusting the temperature.
A stirring tank that houses the material to be agitated and
A temperature control means provided outside the stirring tank and adjusting the temperature of the object to be stirred via the stirring tank.
A stirring blade arranged in the stirring tank and stirring the object to be agitated while rotating,
It is connected to the stirring blade via a stirring shaft and includes a driving means for rotationally driving the stirring blade.
A stirring device, characterized in that at least a part of the inner wall of the stirring tank is formed in a predetermined uneven shape.
(2) The stirring device according to (1) above, wherein the surface area of the inner wall of the stirring tank is more than 1.1 times the surface area of the virtual inner wall assuming that the inner wall is flat.
(3) The stirring device according to (1) or (2) above, wherein the roughness of at least a part of the inner wall of the stirring tank is 1.0 μm or less in arithmetic average roughness (Ra).
(4) The stirring device according to any one of (1) to (3) above, wherein the uneven shape is periodically formed in the stirring axis direction.
(5) The stirring device according to (4) above, wherein the height difference between the concave portion and the convex portion in the concave-convex shape is 10 mm or more and 40 mm or less, and the period of the concave-convex shape is 100 mm or more.
(6) In the projected image when the stirring tank is projected on the projection plane orthogonal to the stirring axis, the minimum value of the dimension between the inner walls crossing the stirring axis is the maximum height difference between the concave portion and the convex portion in the concave-convex shape. The stirring device according to any one of (1) to (5) above, which is more than four times the value.
(7) The shape of the concave portion and the convex portion in the concave-convex shape includes a part of at least one shape selected from the group consisting of a spherical shape, an ellipsoidal surface shape, a conical surface shape, and a polygonal pyramid surface shape. The stirring device according to any one of (1) to (6) and (8) the stirring tank are made of a metal material containing stainless steel, copper or aluminum as a main component, from (1) to (1). 7) The stirring device according to any one of the items.

なお、本明細書において「内壁」とは、撹拌槽の胴部表面のうちの被撹拌物に接液する表面を意味する。また、「凹部と凸部との高低差」とは、隣り合う凹部および凸部において、内壁に垂直な方向における凸部(最頂部)と凹部(最低部)との距離を意味する。また、「所定の凹凸形状」とは、特定の周期を有するあらかじめ定められた凹凸形状を意味し、「内壁の粗さ」とは、不規則に形成された内壁の形状を意味する。上記所定の凹凸形状と内壁の粗さとは異なる概念である。 In the present specification, the "inner wall" means the surface of the body surface of the stirring tank that comes into contact with the material to be agitated. Further, the "height difference between the concave portion and the convex portion" means the distance between the convex portion (top portion) and the concave portion (lowest portion) in the direction perpendicular to the inner wall in the adjacent concave portion and convex portion. Further, the "predetermined uneven shape" means a predetermined uneven shape having a specific period, and the "roughness of the inner wall" means the shape of an irregularly formed inner wall. The above-mentioned predetermined uneven shape and the roughness of the inner wall are different concepts.

本発明は、撹拌槽内壁における被撹拌物への接液面積を増加させることができ、被撹拌物の温度を迅速かつ確実に調整することができると共に、凹凸形状に起因する乱流の発生により被撹拌物の撹乱を促進することができ、上記被撹拌物の温度および濃度の均一化に優れる撹拌装置を提供することができる。 According to the present invention, the area of contact with the agitated object on the inner wall of the agitating tank can be increased, the temperature of the agitated object can be adjusted quickly and surely, and turbulence due to the uneven shape is generated. It is possible to promote the disturbance of the material to be agitated, and it is possible to provide a stirring device excellent in uniforming the temperature and concentration of the material to be agitated.

本発明の第1の実施形態を示す概略断面図である。It is the schematic sectional drawing which shows the 1st Embodiment of this invention. 図1の撹拌槽の内壁の凹凸形状を示す概略図であって、(a)は撹拌槽を切り出した一部の斜視図、(b)は(a)の端面近傍の斜視図、(c)は(b)の端面の輪郭の一部を示す図である。It is a schematic view which shows the uneven shape of the inner wall of the stirring tank of FIG. 1, (a) is the perspective view of a part cut out of the stirring tank, (b) is the perspective view near the end face of (a), (c). Is a figure showing a part of the outline of the end face of (b). 図1の撹拌槽の内壁の輪郭を拡大して示す概略図である。It is the schematic which shows the outline of the inner wall of the stirring tank of FIG. 1 enlarged. 本発明の第2の実施形態を示す概略断面図である。It is a schematic sectional drawing which shows the 2nd Embodiment of this invention. 本発明の第3の実施形態を示す概略断面図である。It is a schematic sectional drawing which shows the 3rd Embodiment of this invention. 比較例を示す概略断面図である。It is the schematic sectional drawing which shows the comparative example. 図1、図4〜図5の各部の寸法を説明するための概略断面図である。1 is a schematic cross-sectional view for explaining the dimensions of each part of FIGS. 1 and 4 to 5.

本発明の撹拌装置は、温度を調整しながら被撹拌物を撹拌する撹拌装置であって、上記被撹拌物を内部に収容する撹拌槽と、上記撹拌槽の外部に設けられ、上記撹拌槽を介して上記被撹拌物の温度を調整する温調手段と、上記撹拌槽内に配置され、上記被撹拌物を回転しながら撹拌する撹拌翼と、撹拌軸を介して上記撹拌翼に接続され、上記撹拌翼を回転駆動する駆動手段とを備え、上記撹拌槽の内壁の少なくとも一部が所定の凹凸形状に形成されていることを特徴とする。 The stirring device of the present invention is a stirring device that stirs an object to be agitated while adjusting the temperature, and includes a stirring tank for accommodating the object to be agitated inside and a stirring tank provided outside the stirring tank. A temperature control means for adjusting the temperature of the object to be agitated, a stirring blade arranged in the stirring tank and stirring the object to be agitated while rotating, and a stirring blade connected to the stirring blade via a stirring shaft. The stirring blade is provided with a driving means for rotationally driving the stirring blade, and at least a part of the inner wall of the stirring tank is formed in a predetermined uneven shape.

以下、本発明の第1〜第3の実施形態について図1〜図5を参照して説明するが、本発明は、当該図面に記載の実施形態にのみ限定されるものではない。 Hereinafter, the first to third embodiments of the present invention will be described with reference to FIGS. 1 to 5, but the present invention is not limited to the embodiments described in the drawings.

[第1の実施形態]
図1は、本発明の第1の実施形態を示す概略断面図である。当該撹拌装置11は、図1に示すように、概略的に、撹拌槽21と、温調手段5と、撹拌翼3と、駆動手段8とにより構成されている。
[First Embodiment]
FIG. 1 is a schematic cross-sectional view showing a first embodiment of the present invention. As shown in FIG. 1, the stirring device 11 is roughly composed of a stirring tank 21, a temperature control means 5, a stirring blade 3, and a driving means 8.

撹拌槽21は、被撹拌物bを内部に収容する。この撹拌槽21は、具体的には、略円筒形状の胴部21aと、この胴部21aの一端を閉塞するように接続された略半回転楕円面形状の槽底部21bとを有している。 The stirring tank 21 houses the object to be agitated b inside. Specifically, the stirring tank 21 has a substantially cylindrical body portion 21a and a substantially semi-rotating ellipsoidal surface-shaped tank bottom portion 21b connected so as to close one end of the body portion 21a. ..

この撹拌槽21は、撹拌槽21の被撹拌物bに接液する内壁61(以下、「接液部」ともいう)が、撹拌槽21の内壁61の少なくとも一部(本実施形態では内壁61の接液部全体)が所定の凹凸形状61aに形成されている。 In the stirring tank 21, the inner wall 61 (hereinafter, also referred to as “contacting portion”) that comes into contact with the object to be agitated b of the stirring tank 21 is at least a part of the inner wall 61 of the stirring tank 21 (in the present embodiment, the inner wall 61). The entire wetted portion of the above) is formed in a predetermined uneven shape 61a.

より具体的には、凹凸形状61aは、当該凹凸形状61aにおける凹部61bおよび凸部61cのそれぞれの形状が球面形状の一部を含んでいる形状、すなわち、図1および図2に示すような撹拌槽21の断面における接液部側の輪郭が曲線となるように山谷状に形成されており、かつ上記凹凸形状61aが撹拌軸4方向に周期的に形成されている。このように凹凸形状61aが撹拌軸4方向に周期的に形成されていることで、被撹拌物bの温度を効果的に調整することができると共に、撹拌槽21の内壁を容易に形成することができる。なお、凹凸形状61aが形成される部位は、接液部の一部であってもよいが、伝熱の促進並びに温度および濃度の均一化向上の観点から、本実施形態のように接液部全体であることが好ましい。 More specifically, the concave-convex shape 61a is a shape in which the respective shapes of the concave portion 61b and the convex portion 61c in the concave-convex shape 61a include a part of the spherical shape, that is, stirring as shown in FIGS. 1 and 2. The contour of the wetted portion side in the cross section of the tank 21 is formed in a mountain valley shape so as to be curved, and the uneven shape 61a is periodically formed in the four directions of the stirring shaft. By periodically forming the concave-convex shape 61a in the four directions of the stirring shaft in this way, the temperature of the object to be agitated b can be effectively adjusted, and the inner wall of the stirring tank 21 can be easily formed. Can be done. The portion where the uneven shape 61a is formed may be a part of the wetted portion, but from the viewpoint of promoting heat transfer and improving the uniformity of temperature and concentration, the wetted portion is as in the present embodiment. It is preferably the whole.

ここで、撹拌槽21の内壁61の凹凸形状61aは、図2に示すように、高低差7aおよび周期長さ7bによって規定することができる。高低差7aと周期長さ7bとの比は、特に限定されるものではないが、撹拌翼3(後述)の形状の自由度を向上させる観点から、下記式(1)で表される関係を満たすことが好ましく、下記式(2)で表される関係を満たすことがより好ましい。
(7b/4)>(7a/2) (1)
(7b/2)>(7a/2) (2)
Here, the uneven shape 61a of the inner wall 61 of the stirring tank 21 can be defined by the height difference 7a and the period length 7b, as shown in FIG. The ratio between the height difference 7a and the period length 7b is not particularly limited, but from the viewpoint of improving the degree of freedom in the shape of the stirring blade 3 (described later), the relationship represented by the following equation (1) is established. It is preferable to satisfy, and it is more preferable to satisfy the relationship represented by the following formula (2).
(7b / 4)> (7a / 2) (1)
(7b / 2)> (7a / 2) (2)

また、凹凸形状61aにおける凹部61bと凸部61cとの高低差は、上記比と同様に撹拌翼3の形状自由度向上の観点から、10mm以上40mm以下が好ましく、20mm以上30mm以下がより好ましい。また、凹凸形状61aの周期は、製作容易性向上の観点から、100mm以上が好ましく、150mm以上がより好ましく、乱流を効率よく発生させかつ十分な接液面積の確保して伝熱性を向上させる観点から、300mm以下が好ましく、200mm以下がより好ましい。 Further, the height difference between the concave portion 61b and the convex portion 61c in the concave-convex shape 61a is preferably 10 mm or more and 40 mm or less, and more preferably 20 mm or more and 30 mm or less from the viewpoint of improving the degree of freedom in the shape of the stirring blade 3 as in the above ratio. Further, the period of the concave-convex shape 61a is preferably 100 mm or more, more preferably 150 mm or more, from the viewpoint of improving ease of manufacturing, to efficiently generate turbulent flow and secure a sufficient wetted area to improve heat transfer. From the viewpoint, 300 mm or less is preferable, and 200 mm or less is more preferable.

上記凹凸形状61aを形成する方法としては、例えば、機械加工、エッチング、鋳造、鍛造、溶接、研摩、冶金、打ち出し板金、叩き出し板金、金型成型プレスなどの方法を単独でまたは組み合わせて用いることができる。 As a method for forming the uneven shape 61a, for example, methods such as machining, etching, casting, forging, welding, polishing, metallurgy, punched sheet metal, punched sheet metal, and die forming press may be used alone or in combination. Can be done.

また、図3に示すように、撹拌槽21の内壁61の少なくとも一部の粗さが、算術平均粗さ(Ra)で1.0μm以下であることが好ましい。これにより、ダストが内壁に噛み込むのを防止することができ、撹拌槽21の内壁61への汚れの付着を抑制することができる。 Further, as shown in FIG. 3, it is preferable that the roughness of at least a part of the inner wall 61 of the stirring tank 21 is 1.0 μm or less in terms of arithmetic mean roughness (Ra). As a result, it is possible to prevent dust from getting caught in the inner wall, and it is possible to suppress adhesion of dirt to the inner wall 61 of the stirring tank 21.

上記粗さを有する内壁61を形成する方法としては、例えば、電解研磨、メッキ、エッチングなどにより化学研摩を行う方法;砥石、バフなどにより研磨加工を行う方法;サンドペーパー処理、レーザー加工などにより物理研摩を行う方法、またはこれらを組み合わせた方法等が挙げられる。なお、Raが1.0μm以下の粗さを有する内壁は、例えば、JIS R 6010に規定されているP400相当の粒度を有する研磨剤を用いて研磨した後、電解研磨を施すことによって得ることができる。 As a method of forming the inner wall 61 having the above roughness, for example, a method of performing chemical polishing by electrolytic polishing, plating, etching or the like; a method of polishing by a grindstone, a buff or the like; physical by sandpaper processing, laser processing or the like. Examples include a method of polishing and a method of combining these. The inner wall having a roughness of Ra of 1.0 μm or less can be obtained by, for example, polishing with an abrasive having a particle size equivalent to P400 specified in JIS R 6010 and then performing electrolytic polishing. it can.

ここで、撹拌槽21の内壁61の表面積は、内壁61が平坦であると仮定したときの仮想内壁の表面積の1.1倍超であることが好ましく、1.5倍超であることがより好ましく、2倍超であることがさらに好ましい。これにより、被撹拌物bの温度をより迅速かつ確実に調整することができる。 Here, the surface area of the inner wall 61 of the stirring tank 21 is preferably more than 1.1 times, more preferably more than 1.5 times, the surface area of the virtual inner wall when the inner wall 61 is assumed to be flat. It is preferable, and more preferably more than twice. As a result, the temperature of the object to be agitated b can be adjusted more quickly and reliably.

また、撹拌槽21を撹拌軸4に直交する投影面に投影したときの投影像において、撹拌軸4を横断する内壁61間の寸法の最小値が、凹凸形状61aにおける凹部61bと凸部61cとの高低差の最大値の4倍超であることが好ましい。これにより、撹拌翼3を配置可能な空間を広くとることができ、当該撹拌翼3の形状自由度を向上させることができる。 Further, in the projected image when the stirring tank 21 is projected on the projection plane orthogonal to the stirring shaft 4, the minimum value of the dimensions between the inner walls 61 crossing the stirring shaft 4 is the concave portion 61b and the convex portion 61c in the concave-convex shape 61a. It is preferable that the height difference is more than 4 times the maximum value of. As a result, the space in which the stirring blade 3 can be arranged can be widened, and the degree of freedom in the shape of the stirring blade 3 can be improved.

温調手段5は、撹拌槽21の外部に設けられ、撹拌槽21を介して被撹拌物bの温度を調整する。この温調手段5としては、撹拌槽21の加熱冷却が可能であれば特に限定されず、例えば、ジャケット、ラバーヒータ、ペルチェ素子等を採用することができる。なお、ジャケットなどを採用して撹拌槽21の外周から温度を調整する場合、上記撹拌槽21の外周の少なくともジャケットなどが接する表面を、例えば上述した所定の凹凸形状のような形状に形成することで、可能な限り伝熱面積(ジャケットなどと撹拌槽との接触面積)を広くすることが好ましい。これにより、上記ジャケットなどと撹拌槽21との間の伝熱を促進させることができる。 The temperature control means 5 is provided outside the stirring tank 21 and adjusts the temperature of the object to be agitated b via the stirring tank 21. The temperature controlling means 5 is not particularly limited as long as the stirring tank 21 can be heated and cooled, and for example, a jacket, a rubber heater, a Peltier element, or the like can be adopted. When the temperature is adjusted from the outer circumference of the stirring tank 21 by using a jacket or the like, at least the surface of the outer circumference of the stirring tank 21 in contact with the jacket or the like is formed into a shape such as the above-mentioned predetermined uneven shape. Therefore, it is preferable to make the heat transfer area (contact area between the jacket or the like and the stirring tank) as wide as possible. As a result, heat transfer between the jacket or the like and the stirring tank 21 can be promoted.

本実施形態の温調手段5は、ジャケット51が採用されている。このジャケット51は、具体的には、図1に示すように撹拌槽21の外周にスパイラル状に捲かれるものであり、ジャケット51の内部に流路52が設けられ、熱媒体cがジャケット51の下方に位置する入口53を介して流路52に投入され、この流路52を流通しながら被撹拌物bと熱交換(被撹拌物bを加熱または冷却)した後にジャケット51の上方に位置する出口54から排出される。 A jacket 51 is adopted as the temperature control means 5 of the present embodiment. Specifically, as shown in FIG. 1, the jacket 51 is spirally wound around the outer periphery of the stirring tank 21, a flow path 52 is provided inside the jacket 51, and the heat medium c is the jacket 51. It is introduced into the flow path 52 through the inlet 53 located below, and is located above the jacket 51 after heat exchange (heating or cooling the agitated object b) with the agitated object b while flowing through the flow path 52. It is discharged from the outlet 54.

熱媒体cは、入口53での温度が一定であれば使い捨ての流体(一過水など)または再使用可能な流体(循環水など)のいずれであってもよい。この熱媒体cとしては、流路52等の腐食劣化を防止する観点から、エチレングリコール、プロピレングリコールなどのグリコール類、水、塩水、シリコーンオイル、熱風、蒸気を好適に用いることができる。これらは、単独でまたは組み合わせて用いてもよい。 The heat medium c may be either a disposable fluid (such as hydrogen peroxide) or a reusable fluid (such as circulating water) as long as the temperature at the inlet 53 is constant. As the heat medium c, glycols such as ethylene glycol and propylene glycol, water, salt water, silicone oil, hot air, and steam can be preferably used from the viewpoint of preventing corrosion deterioration of the flow path 52 and the like. These may be used alone or in combination.

熱媒体cの流速としては、熱伝達性向上の観点から、0.3m/秒〜3.0m/秒であることが好ましく、1.0m/秒〜2.0m/秒であることがより好ましい。また、流路52内における熱媒体cの流れの方向としては特に限定されないが、熱交換を効率よく行う観点から、撹拌翼3の回転方向と反対の方向であることが好ましい。また、流路52内での熱媒体cの充填性向上の観点から、熱媒体cが撹拌槽21の下方(入口53)から上方(出口54)に向かって流れるようにすることも好ましい。 The flow velocity of the heat medium c is preferably 0.3 m / sec to 3.0 m / sec, more preferably 1.0 m / sec to 2.0 m / sec, from the viewpoint of improving heat transferability. .. The direction of flow of the heat medium c in the flow path 52 is not particularly limited, but is preferably the direction opposite to the rotation direction of the stirring blade 3 from the viewpoint of efficient heat exchange. Further, from the viewpoint of improving the filling property of the heat medium c in the flow path 52, it is also preferable that the heat medium c flows from the lower side (inlet 53) to the upper side (outlet 54) of the stirring tank 21.

撹拌翼3は、撹拌槽21内に配置され、被撹拌物bを回転しながら撹拌する。この撹拌翼3は、被撹拌物bの混合(混合、撹拌、分散などを総称して「混合」と称する)および濃度分布の均一化や、温調手段5と被撹拌物bと間の伝熱を促進させる。撹拌翼3は板状の部材であり、後述する駆動手段8の動力を伝搬させるための撹拌軸4の一端側に垂直に固定されている。駆動手段8は、撹拌軸4を介して撹拌翼3に接続され、撹拌翼3を回転駆動する。駆動手段8としては、例えば、図1に示すモータ81等を採用することができる。 The stirring blade 3 is arranged in the stirring tank 21 and stirs the object to be agitated b while rotating. The stirring blade 3 is used to mix the material b to be agitated (mixing, stirring, dispersion, etc. are collectively referred to as "mixing"), to make the concentration distribution uniform, and to transfer the temperature control means 5 to the material b to be agitated. Promotes heat. The stirring blade 3 is a plate-shaped member, and is vertically fixed to one end side of the stirring shaft 4 for propagating the power of the driving means 8 described later. The driving means 8 is connected to the stirring blade 3 via the stirring shaft 4 and rotationally drives the stirring blade 3. As the drive means 8, for example, the motor 81 shown in FIG. 1 or the like can be adopted.

上述した撹拌槽21、撹拌翼3および撹拌軸4を構成する材料としては、特に限定されず、例えば、ステンレス鋼、鉄、銅、真鍮、アルミニウム、超硬などの金属系材料等を用いることができる。これらの中で、撹拌槽21としては、ステンレス鋼、銅またはアルミニウムを主成分とする金属材料で形成されていることが好ましい。これにより、撹拌槽21自体の伝熱を促進することができ、被撹拌物bの温度をより迅速に調整することができる。 The material constituting the stirring tank 21, the stirring blade 3, and the stirring shaft 4 is not particularly limited, and for example, a metal-based material such as stainless steel, iron, copper, brass, aluminum, or cemented carbide may be used. it can. Among these, the stirring tank 21 is preferably formed of a metal material containing stainless steel, copper or aluminum as a main component. As a result, heat transfer of the stirring tank 21 itself can be promoted, and the temperature of the object to be agitated b can be adjusted more quickly.

また、これら撹拌槽21、撹拌翼3および撹拌軸4の接液部には、上記金属系材料の表面にホワイトアルミナ、グレイアルミナ、アルミナ−チタニア、アルミナ−マグネシア、ジルコニア−カルシア、ジルコニア−イットリア、ジルコニア−マグネシア、クロミア−チタニア、クロミア−シリカ−チタニア、タングステン、チタニア、クロミア、イットリア、ジルコニア、クロムカーバイト、マグネシア、セリア、タングステンカ−バイトなどのセラミックスを溶射により表面処理したものや、フッ素系素材によりライニングしたもの等を採用してもよい。 Further, in the wetted portions of the stirring tank 21, the stirring blade 3 and the stirring shaft 4, white alumina, gray alumina, alumina-titania, alumina-magnesia, zirconia-calcia, zirconia-yttria, etc. are provided on the surfaces of the metal-based materials. Surface-treated ceramics such as zirconia-magnesia, chromia-titania, chromia-silica-titania, tungsten, titania, chromia, yttria, zirconia, chrome carbide, magnesia, ceria, tungsten carbide, and fluorine-based A material lined or the like may be adopted.

以上のように、本実施形態では、上述した撹拌槽21と温調手段5と撹拌翼3と駆動手段8とを備え、撹拌槽21の内壁61の少なくとも一部が凹凸形状61aに形成されているので、撹拌槽内壁61における被撹拌物bへの接液面積を増加させることができ、被撹拌物bの温度を迅速かつ確実に調整することができると共に、凹凸形状61aに起因する乱流の発生により被撹拌物bの撹乱を促進することができ、被撹拌物bの温度および濃度の均一化に優れる。 As described above, in the present embodiment, the above-mentioned stirring tank 21, temperature controlling means 5, stirring blade 3 and driving means 8 are provided, and at least a part of the inner wall 61 of the stirring tank 21 is formed in the concave-convex shape 61a. Therefore, the area of contact with the agitated object b on the inner wall 61 of the agitating tank can be increased, the temperature of the agitated object b can be adjusted quickly and surely, and the turbulent flow caused by the uneven shape 61a. The disturbance of the agitated object b can be promoted by the generation of the agitated object b, and the temperature and the concentration of the agitated object b are excellently made uniform.

[第2の実施形態]
図4は、本発明の第2の実施形態を示す概略断面図である。当該撹拌装置12は、図4に示すように、概略的に、撹拌槽22と、温調手段5と、撹拌翼3と、駆動手段8とにより構成されている。第2の実施形態は、撹拌槽22の内壁62における接液部の凹凸形状62aが第1の実施形態と異なっている。なお、温調手段5、撹拌翼3および駆動手段8は、第1の実施形態のものと同じ構成であるので、同一部分には同一符号を付してその詳細な説明を省略する。
[Second Embodiment]
FIG. 4 is a schematic cross-sectional view showing a second embodiment of the present invention. As shown in FIG. 4, the stirring device 12 is roughly composed of a stirring tank 22, a temperature control means 5, a stirring blade 3, and a driving means 8. In the second embodiment, the uneven shape 62a of the wetted portion of the inner wall 62 of the stirring tank 22 is different from that of the first embodiment. Since the temperature control means 5, the stirring blade 3, and the driving means 8 have the same configuration as those of the first embodiment, the same parts are designated by the same reference numerals and detailed description thereof will be omitted.

本実施形態では、撹拌槽22の内壁62における接液部の凹凸形状62aは、図4に示すように、当該凹凸形状62aにおける凹部62bおよび凸部62cのそれぞれの形状が三角錐面形状の一部を含んでいる形状、すなわち、撹拌槽22の断面における接液部側の輪郭が折れ線となるように山谷状に形成されており、かつ上記凹凸形状62aが撹拌軸4方向に周期的に形成されている。 In the present embodiment, as shown in FIG. 4, the concave-convex shape 62a of the wetted portion on the inner wall 62 of the stirring tank 22 has a triangular pyramid shape, respectively, of the concave portion 62b and the convex portion 62c in the concave-convex shape 62a. The shape including the portion, that is, the contour on the wetted portion side in the cross section of the stirring tank 22 is formed in a mountain valley shape so as to be a polygonal line, and the uneven shape 62a is periodically formed in the four directions of the stirring shaft. Has been done.

このように、本実施形態では、撹拌槽22の断面における接液部側の輪郭が折れ線となるように山谷状に形成されているので、上述した第1の実施形態の効果に加え、撹拌槽22の内壁62を容易に形成することができる。なお、凹凸形状62aが形成される部位は、接液部の一部であってもよいが、伝熱の促進並びに温度および濃度の均一化の観点から、本実施形態のように接液部全体であることが好ましい。 As described above, in the present embodiment, the contour of the wetted portion side in the cross section of the stirring tank 22 is formed in a mountain valley shape so as to be a polygonal line. Therefore, in addition to the effect of the first embodiment described above, the stirring tank The inner wall 62 of 22 can be easily formed. The portion where the concave-convex shape 62a is formed may be a part of the wetted portion, but from the viewpoint of promoting heat transfer and making the temperature and concentration uniform, the entire wetted portion as in the present embodiment. Is preferable.

[第3の実施形態]
図5は、本発明の第3の実施形態を示す概略断面図である。当該撹拌装置13は、図5に示すように、概略的に、撹拌槽23と、温調手段5と、撹拌翼3と、駆動手段8とにより構成されている。第3の実施形態は、撹拌槽23の内壁63の凹凸形状63aにおける凹部63bと凸部63cとの高低差が第1の実施形態と異なっている。なお、温調手段5、撹拌翼3および駆動手段8は、第1の実施形態のものと同じ構成であるので、同一部分には同一符号を付してその詳細な説明を省略する。
[Third Embodiment]
FIG. 5 is a schematic cross-sectional view showing a third embodiment of the present invention. As shown in FIG. 5, the stirring device 13 is roughly composed of a stirring tank 23, a temperature control means 5, a stirring blade 3, and a driving means 8. In the third embodiment, the height difference between the concave portion 63b and the convex portion 63c in the concave-convex shape 63a of the inner wall 63 of the stirring tank 23 is different from that of the first embodiment. Since the temperature control means 5, the stirring blade 3, and the driving means 8 have the same configuration as those of the first embodiment, the same parts are designated by the same reference numerals and detailed description thereof will be omitted.

本実施形態では、撹拌槽23の内壁63の凹凸形状63aにおける凹部63bと凸部63cとの高低差は、図5に示すように、撹拌槽23の厚み以下となるように形成されている。なお、凹凸形状63aは、当該凹凸形状63aにおける凹部63bおよび凸部63cのそれぞれの形状が球面形状の一部を含んでいる形状、すなわち、第1の実施形態と同様に撹拌槽23の断面における接液部側の輪郭が曲線となるように山谷状に形成されており、かつ上記凹凸形状63aが撹拌軸4方向に周期的に形成されている。 In the present embodiment, the height difference between the concave portion 63b and the convex portion 63c in the concave-convex shape 63a of the inner wall 63 of the stirring tank 23 is formed so as to be equal to or less than the thickness of the stirring tank 23, as shown in FIG. The concave-convex shape 63a is a shape in which each of the concave portion 63b and the convex portion 63c in the concave-convex shape 63a includes a part of the spherical shape, that is, in the cross section of the stirring tank 23 as in the first embodiment. The contour on the wetted part side is formed in a mountain valley shape so as to be curved, and the uneven shape 63a is periodically formed in the four directions of the stirring shaft.

このように、本実施形態では、撹拌槽23の内壁63の凹凸形状63aにおける凹部63bと凸部63cとの高低差が撹拌槽23の厚み以下となるように形成されているので、撹拌槽23の厚みを凹凸形状63aに対して厚くして撹拌槽23の強度(堅牢性)を高めることができ、その結果、槽容量の大型化を図ったり、比重の高い被撹拌物の撹拌を確実に行うことができる。 As described above, in the present embodiment, the height difference between the concave portion 63b and the convex portion 63c in the concave-convex shape 63a of the inner wall 63 of the stirring tank 23 is formed so as to be equal to or less than the thickness of the stirring tank 23. The strength (robustness) of the stirring tank 23 can be increased by increasing the thickness of the stirring tank 23 with respect to the uneven shape 63a, and as a result, the tank capacity can be increased and the agitated object having a high specific gravity can be reliably stirred. It can be carried out.

なお、本発明は、上述した実施形態の構成に限定されるものではなく、特許請求の範囲によって示され、特許請求の範囲と均等の意味および範囲内での全ての変更が含まれることが意図される。 It should be noted that the present invention is not limited to the configuration of the above-described embodiment, but is indicated by the scope of claims, and is intended to include all modifications within the meaning and scope equivalent to the scope of claims. Will be done.

例えば、上述した第1および第3の実施形態では、撹拌槽21、23の内壁61、63の凹凸形状における凹部および凸部のそれぞれの形状が球面形状の一部を含んでいるような撹拌装置11、13、第2の実施形態では、撹拌槽22の内壁62の上記形状が円錐面形状の一部を含んでいるような撹拌装置12について説明したが、撹拌槽内壁の凹凸形状における凹部および凸部のそれぞれの形状が、楕円面形状、円錐面形状および多角錐面形状からなる群より選ばれる少なくとも1種の形状の一部を含んでいる撹拌装置であってもよい。このように、撹拌槽の内壁を上記形状とすることで、被撹拌物の温度調整、並びに温度および濃度の均一化を効果的に行うことができる。 For example, in the first and third embodiments described above, a stirring device in which the concave and convex portions of the inner walls 61 and 63 of the stirring tanks 21 and 23 each include a part of the spherical shape. In 11, 13, and the second embodiment, the stirring device 12 in which the shape of the inner wall 62 of the stirring tank 22 includes a part of the conical surface shape has been described, but the recesses in the uneven shape of the inner wall of the stirring tank and the recesses A stirring device may be used in which each shape of the convex portion includes a part of at least one shape selected from the group consisting of an elliptical surface shape, a conical surface shape, and a polygonal pyramid surface shape. By forming the inner wall of the stirring tank in the above shape in this way, it is possible to effectively adjust the temperature of the object to be agitated and make the temperature and concentration uniform.

また、上述した実施形態では、内壁61〜63の凹凸形状61a〜63aが球面形状の一部を含んでいるような撹拌装置11、13、および円錐面形状の一部を含んでいるような撹拌装置12について説明したが、上記凹凸形状としては、撹拌時に被撹拌物の流れを阻害し難い形状であればよく、凹部および凸部を一つのユニットとし、このユニットが並列されている構造であればよい。また、凹部および凸部のそれぞれは、対称形状ではなくてもよい。 Further, in the above-described embodiment, the stirring devices 11 and 13 such that the concave-convex shapes 61a to 63a of the inner walls 61 to 63 include a part of the spherical shape, and stirring such that a part of the conical surface shape is included. Although the device 12 has been described, the concave-convex shape may be any shape that does not easily obstruct the flow of the object to be agitated during stirring, and the concave and convex portions may be one unit and the units may be arranged in parallel. Just do it. Further, each of the concave portion and the convex portion does not have to have a symmetrical shape.

また、上述した実施形態では、凹凸形状61a〜63aが撹拌軸4方向に周期的に形成されている撹拌装置について説明したが、上記凹凸形状が非周期的に形成された撹拌装置や、一部のみが周期的に形成されている撹拌装置であってもよい。 Further, in the above-described embodiment, the stirring device in which the uneven shapes 61a to 63a are periodically formed in the four directions of the stirring shaft has been described, but the stirring device in which the uneven shapes are formed aperiodically and some of them. It may be a stirrer in which only agitators are formed periodically.

また、上述した実施形態では、バッフルを備えていない撹拌装置11〜13について示したが、本発明の効果を阻害しない範囲で、バッフルを備えている撹拌装置であってもよい。 Further, in the above-described embodiment, the stirring devices 11 to 13 not provided with the baffle are shown, but the stirring device may be provided with the baffle as long as the effect of the present invention is not impaired.

以下、本発明を実施例に基づいて具体的に説明するが、本発明は、これらの実施例に限定されるものではない。なお、以下に示す撹拌装置の各部位は、図7に示す通りである。 Hereinafter, the present invention will be specifically described based on examples, but the present invention is not limited to these examples. Each part of the stirring device shown below is as shown in FIG. 7.

[実施例1]
実施例1の撹拌装置は、撹拌槽が槽径D=200mm、板厚t=1.5mm、胴部高さB=250mm(有効高さ200mm)の略円筒形状であり、上記撹拌槽の槽底部Aを略半回転楕円面形状とし、撹拌槽全体をSUS316L鋼で作製した。撹拌槽の内壁の凹凸形状は、高低差7a=30mm、周期長さ7b=100mmの、凹部と凸部とが半球面状に連続した周期的な山谷形状、かつ撹拌槽の断面における接液部側の輪郭が曲線であり、撹拌槽内壁の有効高さ200mm内の部位に24組の凹部および凸部を設けた(図1参照)。また、上記内壁は、JIS R 6010に規定のP400相当の粒度を有するバフを用いて研摩した後、電解研磨を施すことでRa=1.0μmに仕上げた。なお、上記有効高さとは、被撹拌物を受け入れ可能な撹拌槽内の胴部下端からの高さを意味する。上記Raは、粗さ測定器(キーエンス社製レーザーマイクロスコープ、型番:VK−X150/160)を用いて測定したものである。
[Example 1]
In the stirring device of the first embodiment, the stirring tank has a substantially cylindrical shape with a tank diameter D = 200 mm, a plate thickness t = 1.5 mm, and a body height B = 250 mm (effective height 200 mm), and the tank of the stirring tank. The bottom portion A had a substantially half-rotated ellipsoidal shape, and the entire stirring tank was made of SUS316L steel. The uneven shape of the inner wall of the stirring tank has a height difference of 7a = 30 mm, a periodic length of 7b = 100 mm, a periodic mountain-valley shape in which concave portions and convex portions are continuous in a hemispherical shape, and a wetted portion in the cross section of the stirring tank. The contour on the side is curved, and 24 sets of recesses and protrusions are provided in a portion within an effective height of 200 mm of the inner wall of the stirring tank (see FIG. 1). Further, the inner wall was polished with a buff having a particle size equivalent to P400 specified in JIS R 6010 and then electropolished to finish Ra = 1.0 μm. The effective height means the height from the lower end of the body portion in the stirring tank that can accept the material to be stirred. The Ra is measured using a roughness measuring device (laser microscope manufactured by KEYENCE CORPORATION, model number: VK-X150 / 160).

また、撹拌軸は、φ10mmとした。撹拌翼は、翼径d=120mm、翼高さb=80mm、板厚1.5mmの2枚翼とし、翼底形状は槽底形状に合わせた。温調手段は、ジャケットを用い、ジャケット幅X=10mm、ジャケット高さY=50mmとした。駆動手段は、モータとした。なお、バッフルは未設置とした。 The stirring shaft was φ10 mm. The stirring blade was a double blade having a blade diameter d = 120 mm, a blade height b = 80 mm, and a plate thickness of 1.5 mm, and the blade bottom shape was matched to the tank bottom shape. A jacket was used as the temperature control means, and the jacket width X = 10 mm and the jacket height Y = 50 mm. The driving means was a motor. The baffle was not installed.

[実施例2]
凹部と凸部とが同一の底面積および高さを有する円錐面形状に連続した周期的な山谷形状、かつ撹拌槽の断面における接液部側の輪郭が直線とした以外、実施例1と同様の構成とした(図4参照)。
[Example 2]
Similar to Example 1 except that the concave portion and the convex portion have a conical surface shape having the same bottom area and height, a continuous periodic mountain valley shape, and the contour on the wetted portion side in the cross section of the stirring tank is straight. (See FIG. 4).

[比較例]
撹拌槽の内壁のいずれの部位にも凹凸形状が形成されていないこと以外、実施例1と同様の構成とした(図6参照)。
[Comparison example]
The configuration was the same as that of Example 1 except that no uneven shape was formed on any part of the inner wall of the stirring tank (see FIG. 6).

<評価>
昇温時間および昇温速度比を測定し、その結果を表1に示す。
<Evaluation>
The temperature rise time and temperature rise rate ratio were measured, and the results are shown in Table 1.

[昇温時間および昇温速度比]
ジャケットを温調手段として用いた被撹拌物の加熱において、下記条件下、上記被撹拌物の温度が25℃から60℃になるまでの時間を測定し、この測定値を昇温時間とした。また、昇温速度比は、比較例の昇温速度を100%としたときの各実施例の昇温速度の割合(%)として算出した。
被撹拌物 :純水4L、初期温度20℃
熱媒体 :水とエチレングリコールとの混合液(エチレングリコール75質量%、残部水)、入口温度70℃、流速1.0〜1.5m/秒(0.5〜0.75L/秒)、ジャケット下部から投入
撹拌軸の回転速度 :80rpm
[Raising time and heating rate ratio]
In heating the agitated object using the jacket as a temperature control means, the time until the temperature of the agitated object became 25 ° C. to 60 ° C. was measured under the following conditions, and this measured value was taken as the temperature rising time. Further, the temperature rise rate ratio was calculated as a ratio (%) of the temperature rise rate of each example when the temperature rise rate of the comparative example was 100%.
Material to be agitated: 4 L of pure water, initial temperature 20 ° C
Heat medium: Mixture of water and ethylene glycol (ethylene glycol 75% by mass, residual water), inlet temperature 70 ° C., flow velocity 1.0 to 1.5 m / sec (0.5 to 0.75 L / sec), jacket Input from the bottom Rotation speed of stirring shaft: 80 rpm

なお、撹拌槽内の被撹拌物の液面高さは、凹凸形状における凹部と凸部とが同数であるため、実施例および比較例共に、ほぼ同等であった。 The height of the liquid level of the object to be agitated in the stirring tank was almost the same in both Examples and Comparative Examples because the number of concave portions and convex portions in the concave-convex shape was the same.

Figure 0006835487
Figure 0006835487

11、12、13 撹拌装置
b 被撹拌物
21、22、23 撹拌槽
3 撹拌翼
4 撹拌軸
5 温調手段
61、62、63 内壁
61a、62a、63a 凹凸形状
8 駆動手段
11, 12, 13 Stirrer b Stirring object 21, 22, 23 Stirrer tank 3 Stirrer blade 4 Stirrer shaft 5 Temperature control means 61, 62, 63 Inner wall 61a, 62a, 63a Concavo-convex shape 8 Drive means

Claims (6)

温度を調整しながら被撹拌物を撹拌する撹拌装置であって、
前記被撹拌物を内部に収容する撹拌槽と、
前記撹拌槽の外部に設けられ、前記撹拌槽を介して前記被撹拌物の温度を調整する温調手段と、
前記撹拌槽内に配置され、前記被撹拌物を回転しながら撹拌する撹拌翼と、
撹拌軸を介して前記撹拌翼に接続され、前記撹拌翼を回転駆動する駆動手段とを備え、
前記撹拌槽の内壁の少なくとも一部が所定の凹凸形状に形成され、
前記凹凸形状における凹部および凸部のそれぞれの形状が、同一の底面積および高さを有する円錐面形状であり、
前記凹部および凸部のそれぞれは、前記内壁の少なくとも一部において前記撹拌軸方向に周期的に点在していることを特徴とする撹拌装置。
A stirring device that stirs an object to be agitated while adjusting the temperature.
A stirring tank that houses the material to be agitated and
A temperature control means provided outside the stirring tank and adjusting the temperature of the object to be stirred via the stirring tank.
A stirring blade arranged in the stirring tank and stirring the object to be agitated while rotating,
It is connected to the stirring blade via a stirring shaft and includes a driving means for rotationally driving the stirring blade.
At least a part of the inner wall of the stirring tank is formed into a predetermined uneven shape.
Each shape of the recess and the convex portion of the concavo-convex shape, Ri conical surface shape der having the same bottom area and height,
A stirring device characterized in that each of the concave portion and the convex portion is periodically scattered in the stirring axis direction at least a part of the inner wall.
撹拌槽の内壁の表面積が、前記内壁が平坦であると仮定したときの仮想内壁の表面積の1.1倍超である請求項1に記載の撹拌装置。 The stirring device according to claim 1, wherein the surface area of the inner wall of the stirring tank is more than 1.1 times the surface area of the virtual inner wall when the inner wall is assumed to be flat. 撹拌槽の内壁の少なくとも一部の粗さが、算術平均粗さ(Ra)で1.0μm以下である請求項1または請求項2に記載の撹拌装置。 The stirring device according to claim 1 or 2, wherein the roughness of at least a part of the inner wall of the stirring tank is 1.0 μm or less in arithmetic average roughness (Ra). 凹凸形状における凹部と凸部との高低差が10mm以上40mm以下であり、かつ前記凹凸形状の周期が100mm以上である請求項1から請求項3のいずれか1項に記載の撹拌装置。 The stirring device according to any one of claims 1 to 3, wherein the height difference between the concave portion and the convex portion in the concave-convex shape is 10 mm or more and 40 mm or less, and the period of the concave-convex shape is 100 mm or more. 撹拌槽を撹拌軸に直交する投影面に投影したときの投影像において、前記撹拌軸を横断する内壁間の寸法の最小値が、凹凸形状における凹部と凸部との高低差の最大値の4倍超である請求項1から請求項4のいずれか1項に記載の撹拌装置。 In the projected image when the stirring tank is projected on the projection plane orthogonal to the stirring axis, the minimum value of the dimension between the inner walls crossing the stirring axis is 4 of the maximum value of the height difference between the concave portion and the convex portion in the concave-convex shape. The stirring device according to any one of claims 1 to 4, which is more than doubled. 撹拌槽が、ステンレス鋼、銅またはアルミニウムを主成分とする金属材料で形成されている請求項1から請求項5のいずれか1項に記載の撹拌装置。 The stirring device according to any one of claims 1 to 5, wherein the stirring tank is made of a metal material containing stainless steel, copper or aluminum as a main component.
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