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JP3621372B2 - Bamboo fiber and carbonized bamboo fiber manufacturing method - Google Patents

Bamboo fiber and carbonized bamboo fiber manufacturing method Download PDF

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Publication number
JP3621372B2
JP3621372B2 JP2001350965A JP2001350965A JP3621372B2 JP 3621372 B2 JP3621372 B2 JP 3621372B2 JP 2001350965 A JP2001350965 A JP 2001350965A JP 2001350965 A JP2001350965 A JP 2001350965A JP 3621372 B2 JP3621372 B2 JP 3621372B2
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JP
Japan
Prior art keywords
bamboo
pressure
bamboo fiber
heating
fiber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2001350965A
Other languages
Japanese (ja)
Other versions
JP2003155677A (en
Inventor
隆行 近藤
稔 安島
光幸 明神
藤井  透
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
YASUJIMA CO., LTD.
Original Assignee
YASUJIMA CO., LTD.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Priority to JP2001350965A priority Critical patent/JP3621372B2/en
Priority to CN 02123038 priority patent/CN1287044C/en
Publication of JP2003155677A publication Critical patent/JP2003155677A/en
Application granted granted Critical
Publication of JP3621372B2 publication Critical patent/JP3621372B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Chemical And Physical Treatments For Wood And The Like (AREA)

Description

【0001】
【発明の属する技術分野】
本発明は、消臭作用、脱臭作用、抗菌作用があり、高級繊維として和紙、壁紙、美術品、バリアフリー用品、薬品、オイル製品代替品等の幅広い使用用途を持つ竹繊維及び炭化竹繊維の製造方法に関するもので、天然の竹材から竹繊維及び炭化竹繊維を容易に取り出す技術に関するものである。
【0002】
【従来の技術】
従来の竹繊維の製造方法は、所定長さに切断した丸い竹材を粉竹機により10〜20本に縦割りし、更にそれを粉砕機にかけて繊維を取り出すという方法である。この方法で製造される竹繊維の繊維長さは最長でも2〜3cmであり、1ロットの製造に必要な所要時間は1〜2時間である。この方法で多量の竹繊維を取り出すには、上記の方法を何回も行う必要がある。またこの従来方法では、竹材を粉砕機にかけるために、繊維方向に長い竹繊維を取り出すことは不可能である。
【0003】
【発明が解決しようとする課題】
この発明は、上記のような従来手段の様々な問題点を解決することを目的とするものであって、天然の竹材から長さの長短を問わず、竹繊維を容易かつ1回の処理で多量に取り出し可能にすること、更に、爆砕操作のの条件により、竹繊維だけでなく炭化した竹繊維も取り出し可能にすることである。
【0004】
すなわちこの発明は、従来方法のように粉竹から粉砕という作業工程を必要とせず、圧力缶体に1度に多量の竹をセットするだけで、長さの長短を問わず、竹繊維を取り出すことが簡便に可能で、従って竹繊維製造コストも廉価になる新たな技術手段を得ることを課題としている。
【0005】
【課題を解決するための手段】
上記課題を解決したこの発明の竹繊維の製造方法は、圧力缶体1に竹材11を入れて当該圧力缶体内に水蒸気を噴出し、処理する圧力缶体内の温度を100℃以上にし、竹材中の繊維と繊維とをつなぎ止める役割をしているリグニン層に熱を与え、次に水蒸気温度に対応する缶内圧力を瞬間的に大気開放することで、竹繊維を痛めることなくリグニン層だけを分解し、竹繊維を取り出すというものである。
【0006】
すなわちこの発明は、天然の竹材から竹繊維を採取するとき、圧力缶体を用いて100℃以上の水蒸気とそれに対応する圧力に竹材を晒す操作と、瞬時に圧力缶体内の圧力を大気開放する操作とを数回〜数十回行うことで、長さの長短を問わず数時間で容易に竹繊維を取り出すことを特徴とするものである。
【0007】
この発明の製造方法の特徴は、竹材を収容した圧力缶体内の処理温度と、圧力を瞬間的に大気開放する回数等の処理条件を変化させることで、竹繊維だけにとどまらず、炭化した竹繊維も取り出すことができることである。1回の工程時間は2〜3時間であり、繊維方向に長い竹繊維及び炭化竹繊維が取り出せることが、この発明の発明者らの実験により認められた。
【0008】
この発明の竹繊維及び炭化竹繊維の製造方法によれば、従来の粉竹機による竹の縦割り工程及び繊維を取り出す粉砕工程という工程数を踏む必要がなく、簡便で作業者の操作も簡単であり、作業時間が短縮されることに加えて、所望長さの竹繊維ないし炭化竹繊維を1度に多量に取り出せるため、竹繊維や炭化竹繊維の製造コストを低減することが可能になる。
【0009】
【発明の実施の形態】
この発明の竹繊維の製造方法の実施例を以下に示す。実施例で使用した装置は、図2に示されている。図中、1は横置き円筒形の圧力タンクで、耐圧は10kg/cmのものである。この圧力タンク1の一端には、内容物の出し入れのための扉10が設けられている。圧力タンク1には、その内圧を急速に大気開放するための開放弁2が設けられている。図の装置では、圧力開放を速やかに行うため、開放弁2としてバタフライ弁を用いている。開放弁2の吐出口には、圧力開放時の大きな流体音を消すためのサイレンサー3が接続されており、圧力タンク1内の水蒸気は、このサイレンサー3を経て大気開放される。
【0010】
圧力タンク1の底部には、多数の蒸気吹出孔を備えた蒸気吹出管7が配置され、この蒸気吹出管は、蒸気弁4を介して蒸気ボイラ8に接続されている。蒸気弁4の開度は、圧力タンク1に設置した図示しない温度センサないし圧力センサの検出信号により制御されている。なお、図中、6は自動制御盤、9は圧力タンク1のドレン配管である。
【0011】
竹繊維を取り出そうとする竹材11は、竹材支持枠を備えた台車5に搭載して圧力タンク1に挿入される。台車5は車輪12を備えており、圧力タンク1内のレールとタンク外のレールとの間を移動して、圧力タンク1への竹材の出し入れを行う。
【0012】
次に、上記装置を用いて行った実施例を図1の符号(1)ないし(8)及び図2を参照して説明する。
【0013】
まず、丸いままの竹材を台車5に搭載し、ベルトなどで適宜固定して、台車5を圧力タンク1に入れ、扉10を閉める(1)。そして蒸気弁4を開き、蒸気ボイラ8の蒸気を圧力タンク1内に吹き出して、圧力タンク1内を加熱する(2)。第一回目の加熱サイクルでは、タンク内温度を摂氏170〜175度に維持し、30〜60分間の加熱を行う(3)。タイマーがタイムアップした後、開放弁2を開きタンク内蒸気を大気放出する(4)。図の装置では、開放弁2の開閉に要する時間はそれぞれ約5秒である。
【0014】
次に開放弁2を閉じ、蒸気弁4を開いて圧力タンク1に再度加熱蒸気を供給する(5)。第二回目以降の加熱サイクルでは、タンク内温度が所定の摂氏170〜175度に上昇するのに約5分かかり(6)、温度上昇後、摂氏170〜175度で2〜3分保持する(7)。タイマーがタイムアップ後、開放弁2を開いてタンク内圧力を大気開放する(8)。以下、この第二回目以降の加熱・減圧サイクル(6)〜(8)を所定回数繰り返す。
【0015】
繰り返し回数は、処理する竹の大きさにより5〜15回で、直径100mm以上の竹材で10〜15回、直径75〜100mmの竹材で7〜10回、直径50〜75mmの竹材で5〜7回程度の繰り返し回数が適当であった。
【0016】
試験例1として、長さ3000mm、直径約120mmの竹材を加熱温度173℃、加熱・減圧回数15回の条件で処理した結果、長さ3000mmの竹繊維が取り出せた。試験例2として長さ3000mm、直径約50〜120mmの竹材11本を加熱温度171℃、加熱・減圧回数10回の条件で同時に処理した結果、すべての竹材から長さ3000mmの竹繊維が取り出せた。試験例2において得られた竹材の総重量は80kgであり、この発明の方法を用いて1度に多量かつ廉価にて繊維方向に長い竹繊維が取り出せることが確認できた。
【図面の簡単な説明】
【図1】加熱・減圧サイクルの例を示すタイムチャート
【図2】実施例で使用した装置の模式的な斜視図
【符号の説明】
1 圧力タンク
11 竹材
[0001]
BACKGROUND OF THE INVENTION
The present invention has a deodorizing action, a deodorizing action, an antibacterial action, and bamboo fibers and carbonized bamboo fibers having a wide range of uses such as Japanese paper, wallpaper, fine arts, barrier-free goods, chemicals, and oil product substitutes as high-grade fibers. The present invention relates to a manufacturing method, and relates to a technique for easily extracting bamboo fibers and carbonized bamboo fibers from natural bamboo materials.
[0002]
[Prior art]
A conventional method for manufacturing bamboo fiber is a method in which a round bamboo material cut into a predetermined length is vertically divided into 10 to 20 pieces by a powder bamboo machine, and further, the fiber is taken out through a pulverizer. The fiber length of bamboo fiber manufactured by this method is 2 to 3 cm at the longest, and the time required for manufacturing one lot is 1 to 2 hours. In order to take out a large amount of bamboo fiber by this method, it is necessary to perform the above method many times. Also, with this conventional method, it is impossible to take out bamboo fibers that are long in the fiber direction in order to apply the bamboo material to a pulverizer.
[0003]
[Problems to be solved by the invention]
The object of the present invention is to solve various problems of the conventional means as described above, and it is easy to process bamboo fibers from natural bamboo materials regardless of the length. In addition to making it possible to take out a large amount, it is also possible to take out not only bamboo fibers but also carbonized bamboo fibers depending on the conditions of the explosion operation.
[0004]
That is, the present invention does not require the work process of pulverizing from powdered bamboo unlike the conventional method, and only by setting a large amount of bamboo at once in the pressure can body, the bamboo fiber can be taken out regardless of the length. Therefore, it is an object to obtain a new technical means that can be easily performed, and hence the manufacturing cost of bamboo fiber is low.
[0005]
[Means for Solving the Problems]
In the method for producing bamboo fiber according to the present invention which has solved the above problems, the bamboo material 11 is put into the pressure can body 1 and water vapor is jetted into the pressure can body so that the temperature inside the pressure can body is 100 ° C. or higher. Heat is applied to the lignin layer, which plays a role in keeping the fibers in contact with each other, and then the pressure inside the can corresponding to the water vapor temperature is momentarily released to the atmosphere, so that only the lignin layer is decomposed without damaging the bamboo fiber. The bamboo fiber is taken out.
[0006]
That is, in the present invention, when collecting bamboo fiber from natural bamboo material, the pressure can body is used to expose the bamboo material to water vapor of 100 ° C. or higher and the corresponding pressure, and the pressure can body pressure is instantaneously released to the atmosphere . By performing the operation several times to several tens of times, the bamboo fiber can be easily taken out in a few hours regardless of the length.
[0007]
The feature of the manufacturing method of the present invention is that not only the bamboo fiber but also carbonized bamboo is changed by changing the treatment temperature in the pressure can containing the bamboo material and the treatment conditions such as the number of times the pressure is instantaneously released to the atmosphere. The fiber can also be taken out. One process time is 2 to 3 hours, and it has been confirmed by experiments of the inventors of the present invention that long bamboo fibers and carbonized bamboo fibers can be taken out in the fiber direction.
[0008]
According to the method for producing bamboo fiber and carbonized bamboo fiber according to the present invention, it is not necessary to go through the number of steps of vertical splitting of bamboo by a conventional powder bamboo machine and pulverizing step of taking out the fiber, and it is simple and easy for the operator to operate. In addition to shortening the working time, it is possible to take out a large amount of bamboo fiber or carbonized bamboo fiber of a desired length at a time, so that the manufacturing cost of bamboo fiber or carbonized bamboo fiber can be reduced. .
[0009]
DETAILED DESCRIPTION OF THE INVENTION
The Example of the manufacturing method of the bamboo fiber of this invention is shown below. The apparatus used in the examples is shown in FIG. In the figure, 1 is a horizontal cylindrical pressure tank having a pressure resistance of 10 kg / cm 2 . One end of the pressure tank 1 is provided with a door 10 for taking contents in and out. The pressure tank 1 is provided with an open valve 2 for rapidly releasing the internal pressure to the atmosphere. In the illustrated apparatus, a butterfly valve is used as the release valve 2 in order to quickly release the pressure. A silencer 3 is connected to the discharge port of the release valve 2 to eliminate a large fluid sound when the pressure is released. Water vapor in the pressure tank 1 is released to the atmosphere via the silencer 3.
[0010]
A steam blowing pipe 7 having a large number of steam blowing holes is disposed at the bottom of the pressure tank 1, and this steam blowing pipe is connected to a steam boiler 8 via a steam valve 4. The opening degree of the steam valve 4 is controlled by a detection signal of a temperature sensor or a pressure sensor (not shown) installed in the pressure tank 1. In the figure, 6 is an automatic control panel, and 9 is a drain pipe of the pressure tank 1.
[0011]
The bamboo material 11 from which the bamboo fiber is to be taken out is mounted on a cart 5 having a bamboo material support frame and inserted into the pressure tank 1. The carriage 5 includes wheels 12 and moves between the rails in the pressure tank 1 and the rails outside the tank, and the bamboo material is taken in and out of the pressure tank 1.
[0012]
Next, an embodiment performed using the above apparatus will be described with reference to reference numerals (1) to (8) in FIG. 1 and FIG.
[0013]
First, the bamboo material which is still round is mounted on the cart 5 and fixed with a belt or the like, the cart 5 is put in the pressure tank 1 and the door 10 is closed (1). Then, the steam valve 4 is opened, the steam from the steam boiler 8 is blown into the pressure tank 1, and the pressure tank 1 is heated (2). In the first heating cycle, the tank internal temperature is maintained at 170 to 175 degrees Celsius, and heating is performed for 30 to 60 minutes (3). After the timer expires, the release valve 2 is opened to release the tank vapor to the atmosphere (4). In the illustrated apparatus, the time required to open and close the release valve 2 is about 5 seconds.
[0014]
Next, the open valve 2 is closed, the steam valve 4 is opened, and the heating steam is supplied again to the pressure tank 1 (5). In the second and subsequent heating cycles, it takes about 5 minutes for the temperature in the tank to rise to a predetermined 170 to 175 degrees Celsius (6), and after the temperature rise, the temperature is maintained at 170 to 175 degrees Celsius for 2 to 3 minutes ( 7). After the timer expires, the release valve 2 is opened to release the tank pressure to the atmosphere (8). Thereafter, the second and subsequent heating / decompression cycles (6) to (8) are repeated a predetermined number of times.
[0015]
The number of repetitions is 5 to 15 times depending on the size of the bamboo to be processed, 10 to 15 times for bamboo materials having a diameter of 100 mm or more, 7 to 10 times for bamboo materials having a diameter of 75 to 100 mm, and 5 to 7 times for bamboo materials having a diameter of 50 to 75 mm. The number of repetitions of about the number of times was appropriate.
[0016]
As Test Example 1, a bamboo material having a length of 3000 mm and a diameter of about 120 mm was treated under the conditions of a heating temperature of 173 ° C. and a heating / depressurization frequency of 15 times. As a result, a bamboo fiber having a length of 3000 mm could be taken out. As Test Example 2, 11 bamboo materials having a length of 3000 mm and a diameter of about 50 to 120 mm were simultaneously processed under the conditions of a heating temperature of 171 ° C. and a heating / depressurization frequency of 10 times. As a result, bamboo fibers having a length of 3000 mm were extracted from all the bamboo materials. . The total weight of the bamboo material obtained in Test Example 2 was 80 kg, and it was confirmed that bamboo fibers that were long in the fiber direction could be taken out at a large amount and at a low cost by using the method of the present invention.
[Brief description of the drawings]
FIG. 1 is a time chart showing an example of a heating / decompression cycle. FIG. 2 is a schematic perspective view of an apparatus used in the examples.
1 Pressure tank 11 Bamboo

Claims (2)

所定長さに切断した天然の竹材(11)を圧力缶体(1)に入れ、当該圧力缶体(1)内に100℃以上の温度水蒸気を供給する加熱加圧操作と、圧力缶体(1)内の圧力を急速に大気開放する減圧操作とを繰り返すことにより、竹繊維相互を分離させることを特徴とする、竹繊維の製造方法。Predetermined placed natural bamboo material was cut into lengths (11) to the pressure can body (1), the pressure can body (1) and the heating and pressurizing operation supplies 100 ° C. or more temperature of the steam in the pressure can body (1) A method for producing bamboo fibers, wherein the bamboo fibers are separated from each other by repeating a pressure reducing operation for rapidly releasing the pressure in the atmosphere . 所定長さに切断した天然の竹材(11)を圧力缶体(1)に入れ、当該圧力缶体(1)内に100℃以上の温度水蒸気を供給する加熱加圧操作と、圧力缶体内の圧力を急速に大気開放する減圧操作とを繰り返すことにより竹繊維相互を分離し、前記加熱操作時に竹材を炭化させるのに必要な温度以上の高温の水蒸気を供給することを特徴とする、炭化竹繊維の製造方法。Put natural bamboo material was cut into a predetermined length (11) to the pressure can body (1), and heating and pressurizing operation for supplying steam of the pressure can body (1) above 100 ° C. in temperature, pressure can body bamboo fiber cross separated by repeated rapidly and depressurization to atmospheric release the pressure, and supplying a temperature above the hot steam required to carbonize the bamboo during the heating operation, carbonized Bamboo fiber manufacturing method.
JP2001350965A 2001-11-16 2001-11-16 Bamboo fiber and carbonized bamboo fiber manufacturing method Expired - Fee Related JP3621372B2 (en)

Priority Applications (2)

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JP2001350965A JP3621372B2 (en) 2001-11-16 2001-11-16 Bamboo fiber and carbonized bamboo fiber manufacturing method
CN 02123038 CN1287044C (en) 2001-11-16 2002-06-12 Bamboo fibre and method for carbonizing bamboo fibre

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JP3621372B2 true JP3621372B2 (en) 2005-02-16

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KR100864812B1 (en) * 2007-02-01 2008-10-23 주식회사 민건 Method of manufacturing structural material using bamboo
KR100847071B1 (en) 2007-02-01 2008-07-17 주식회사 민건 Bamboo filter manufacturing method
JP4938638B2 (en) * 2007-12-26 2012-05-23 株式会社竹中工務店 Bamboo fiber rope manufacturing method and bamboo fiber rope
CN103046150A (en) * 2012-12-18 2013-04-17 苏州展华纺织有限公司 Manufacturing method for bamboo fiber
JP5713413B2 (en) * 2013-02-04 2015-05-07 国立大学法人九州工業大学 Bamboo heat treatment equipment
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007154366A (en) * 2005-12-06 2007-06-21 Noritaka Okada Continuous monocotyledon fiber and method for producing the same

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CN1287044C (en) 2006-11-29
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