JP3496459B2 - Rolling method of ferritic stainless steel sheet - Google Patents
Rolling method of ferritic stainless steel sheetInfo
- Publication number
- JP3496459B2 JP3496459B2 JP15703497A JP15703497A JP3496459B2 JP 3496459 B2 JP3496459 B2 JP 3496459B2 JP 15703497 A JP15703497 A JP 15703497A JP 15703497 A JP15703497 A JP 15703497A JP 3496459 B2 JP3496459 B2 JP 3496459B2
- Authority
- JP
- Japan
- Prior art keywords
- rolling
- stainless steel
- steel sheet
- ferritic stainless
- rough
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000005096 rolling process Methods 0.000 title claims description 78
- 229910001220 stainless steel Inorganic materials 0.000 title claims description 23
- 238000000034 method Methods 0.000 title claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 23
- 238000005098 hot rolling Methods 0.000 claims description 11
- 239000010935 stainless steel Substances 0.000 claims description 8
- 229910000831 Steel Inorganic materials 0.000 description 16
- 239000010959 steel Substances 0.000 description 16
- 238000007788 roughening Methods 0.000 description 10
- 230000007547 defect Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 230000003746 surface roughness Effects 0.000 description 3
- 206010013786 Dry skin Diseases 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910000859 α-Fe Inorganic materials 0.000 description 2
- 101100233050 Caenorhabditis elegans ima-1 gene Proteins 0.000 description 1
- 238000005422 blasting Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 238000005554 pickling Methods 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
Landscapes
- Metal Rolling (AREA)
Description
【発明の詳細な説明】
【0001】
【発明の属する技術分野】本発明は、フェライト系ステ
ンレス鋼の熱間圧延時のスケールに起因する表面欠陥や
ロール面荒れを防止し、ロール原単位を向上すると共
に、表面の良好なフェライト系ステンレス熱間圧延鋼板
を圧延する方法に関する。
【0002】
【従来の技術】フェライト系ステンレス鋼は、熱間圧延
時にスケール疵が発生すると重要な特性である表面品質
が損なわれ、このため次工程で再酸洗や表面研磨を要す
るので製品コストが上昇し、生産性が低下する弊害があ
る。ステンレス鋼の熱間圧延時のスケール疵は表面酸化
膜(スケール)が剥離して発生するもので、加熱温度を
高くして二次スケールを厚くすると肌荒れの防止に効果
があることが知られている。
【0003】従来、ステンレス鋼の肌荒れ防止対策とし
て特開平7−284804号公報などが開示されてい
る。これは、フェライト系ステンレス鋼を熱間圧延する
ためにスラブ加熱炉に装入する前に、グラインダーある
いはショットブラストによる研削、もしくはバイトやフ
ライスによる切削の少なくとも1種類の方法により、ス
ラブの表面粗度をRmaxで20μm以上にすることに
より、スラブ加熱中に均一で厚いスケールを容易に形成
せしめ、しかる後に熱間圧延を行うことを特徴とする表
面疵の少ないフェライト系ステンレス鋼の製造方法であ
る。
【0004】
【発明が解決しようとする課題】しかし、このような方
法では、加熱炉からスラブが抽出された直後では確かに
平滑なスラブよりもスケールの生成量は多くなるが、加
熱炉内で生成された一次スケールを除去するスラブ出側
のスケールブレーカによりその多くは除去されてしま
い、粗圧延の後段スタンドや仕上圧延の前段スタンドで
生じるロール面荒れ及びそれに伴う鋼板の表面荒れを防
止することは不可能であるという問題があった。
【0005】本発明は、粗圧延のみならずスラブの加熱
から仕上圧延までを通して肌荒れを発生させずに安定的
に表面の良好な鋼板を製造することを目的とする。
【0006】
【課題を解決するための手段】本発明は、前記問題点を
解決するもので、連続鋳造したフェライト系ステンレス
鋼のスラブを、加熱炉で加熱し、粗圧延、仕上圧延を行
い、ステンレス鋼板を製造する一連の熱間圧延におい
て、加熱炉出側温度を1200〜1300℃とし、粗圧
延時の各パスの圧下率を35%以下とし、仕上圧延の前
半(F1 〜F3 スタンド)の各スタンドの圧下率を30
%以下とし、仕上げ最終スタンドの圧延速度を700m
/min以上とすることを特徴とするフェライト系ステ
ンレス鋼板の熱間圧延方法を提案するものである。
【0007】以下、本発明のフェライト系ステンレス鋼
の肌荒れを防止するための熱間圧延方法について詳細に
説明する。焼付(以下肌荒れと称す)は、例えばCAM
P ISIJ Vol.6(1996)−1346にも
示されているように、スケールが厚く均一にできる場合
には発生しないが、加熱温度が低くてスケールが薄い場
合には圧延されると鋼板とロールとが焼き付いて(肌荒
れ)となる。
【0008】加熱炉出側における温度が1200℃未満
であると、鋼板表面のスケール厚が薄く、鋼板とロール
の間で焼付が発生するので好ましくない。1300℃を
越えると鋼板の粒界割れに起因する線状の疵が発生する
ため不可である。したがって本発明では加熱炉出側温度
を1200〜1300℃とした。粗圧延および仕上げ圧
延の規制の理由は次のとおりである。
【0009】フェライト系ステンレス鋼に発生する肌荒
れは粗圧延の圧下率が35%を越えるか、又は仕上げ圧
延の圧下率が30%を越え仕上圧延の最終スタンドの圧
延速度が700m/min未満の場合に発生しやすい。
粗圧延で圧下率が35%を越えると鋼板表面のスケール
が剪断されたり、スケールが割れて材料の新生面の割合
が大きくなり、地鉄がロールと接しやすくなって焼き付
きが生じるものと考えられる。従って、粗圧延の各パス
での圧下率は35%以下とする。
【0010】仕上げ圧延で、圧下率が30%を越える
と、粗圧延の場合と同じ理由によって焼付が発生する。
また、最終スタンド出側で、圧延速度が700m/mi
nよりも遅い場合、圧延材がロールと接触する時間が長
くなり、金属の拡散時間が長くなるため焼き付きを生じ
易くなる。従って、仕上圧延の圧下率は30%以下、仕
上げ圧延の最終スタンドの圧延速度は700m/min
以上とする。
【0011】なお、フェライト系ステンレス鋼の成分の
含有重量%は、C:0.05%以下、Mn:0.15〜
0.3%、Cr:16〜20%を含むステンレス鋼であ
る。さらにMo:2.0%以下、Nb:0.5%以下、
Ti:0.3%以下の内から選ばれた少なくとも1種以
上を添加した肌荒れの発生しやすいステンレス鋼でも効
果を得ることができる。
【0012】
【発明の実施の形態】表1に示す成分を有する厚さ20
0mm、長さ6m、板幅1300mmのフェライト系ス
テンレス鋼スラブを用い、熱間圧延を行った例について
説明する。用いた圧延機の圧延機列を図1に示した。図
1において、加熱炉1で加熱されたスラブは、スケール
ブレーカ2でスケールを剥離した後、R1 〜R3 スタン
ドを有する粗圧延機3で粗圧延され、次いで、F1 から
F7 で示す各スタンドを持つ仕上げ圧延機4で仕上圧延
され、ランアウトテーブル5を経てダウンコイラ6に巻
き取られる。粗圧延機3のワークロール径は1500m
m、仕上圧延機4のワークロール径はF1 〜F3 スタン
ドが820mm、F4 〜F7 スタンドが700mmであ
る。
【0013】上記フェライト系ステンレス鋼スラブを1
200℃に2時間加熱し、粗圧延機3により、厚さ20
0mmのスラブを厚さ30.3mmのシートバーまで圧
延した。粗圧延スタンドR1 、R2 では3パスのリバー
ス圧延を行い、R3 では1パスの圧延を行った。その
後、7スタンドの仕上圧延機4を用いてタンデム圧延を
行い、板厚3.5mmまで圧延した。
【0014】粗圧延条件とシートバーの表面性状の関係
を調査するため表2、表3のように加熱温度、粗圧延の
圧下率設定を変更した。表2は、加熱温度(加熱炉出側
温度)、仕上圧延機入側温度、圧下率とF1 入側の鋼板
(シートバー)表面性状を示す表、表3は、圧延を行う
際の本発明と従来条件の粗圧延の圧下率配分を示す表で
ある。結果を図2に示す。加熱温度が1300℃を越え
る条件では線疵が発生し、1200℃未満の条件では肌
荒れが発生し、これらの表面欠陥の発生は圧下率の設定
の如何によらなかった。また、加熱温度が1200〜1
300℃の条件では、粗圧下率の条件、B−1、B−2
の圧下率設定で圧延を行った場合には肌荒れの発生は見
られなかったが、従来条件Aの圧下率の設定ではいずれ
も肌荒れが発生することがわかった。また、加熱温度は
1200〜1300℃のシートバーの表面性状が良好な
とき、仕上圧延機入側の鋼板温度は1000〜1100
℃となることがわかった。
【0015】次に、仕上げ圧延条件と仕上げ圧延終了後
の鋼板表面の状態を調べる実験を行った。実験条件と結
果を表4、表5に示す。表4は、圧下率設定、仕上圧延
機最終スタンドF7 の出側圧延速度と圧延終了後の鋼板
表面性状の関係を示す。表5は、表4で圧延を行う際の
仕上圧延の圧下率配分を示す表である。この時の、仕上
げ圧延機入側の鋼板温度は、いずれも1050℃で、シ
ートバーの状態では肌荒れの発生は見られなかった。結
果を図3に示す。実験の結果、鋼板表面が良好であった
のは表5の条件のうち、P、R、S、Tの圧下率条件
で、かつ圧延速度が700m/min以上の組合で、P
の圧下率条件でも圧延速度が690m/minと低速の
場合や、圧延速度が速くても、仕上スタンドF1 、F2
の圧下率が32%と大きなQの圧下率条件になっている
条件では、肌荒れが発生することがわかった。
【0016】
【表1】
【0017】
【表2】【0018】
【表3】
【0019】
【表4】【0020】
【表5】
【0021】
【発明の効果】フェライト系ステンレス鋼板の肌荒れ防
止の対策として、従来は加熱温度の高温化やスラブの手
入れなどがあったが、高温での加熱は線疵が発生しやす
くなる問題があり、鋼板の温度条件の管理のみでは防止
しきれず、また、スラブの手入れは行っても完全に肌荒
れを防止はできないとともに、製造コストの上昇につな
がる弊害があった。
【0022】本発明によれば、フェライト系ステンレス
鋼を圧延する際の圧延条件を最適にすることができ、安
定して良好な鋼板表面を得ることができる。Description: BACKGROUND OF THE INVENTION [0001] 1. Field of the Invention [0002] The present invention prevents surface defects and roll surface roughness caused by scale during hot rolling of ferritic stainless steel, and improves the basic unit of roll. And a method for rolling a hot-rolled ferritic stainless steel sheet having a good surface. [0002] Ferritic stainless steel suffers from surface flaws, an important characteristic, when scale flaws are generated during hot rolling, so that re-pickling and surface polishing are required in the next step, so that product cost is reduced. And the productivity is reduced. Scale flaws during hot rolling of stainless steel are caused by peeling of the surface oxide film (scale), and it is known that increasing the heating temperature and increasing the thickness of the secondary scale is effective in preventing skin roughness. I have. Conventionally, Japanese Unexamined Patent Publication No. 7-284804 discloses a countermeasure for preventing roughening of stainless steel. This is because the surface roughness of the slab is determined by at least one method of grinding with a grinder or shot blasting or cutting with a tool or mill before charging the ferritic stainless steel to the slab heating furnace for hot rolling. Is set to 20 μm or more by Rmax to easily form a uniform and thick scale during slab heating, followed by hot rolling, which is a method for producing a ferritic stainless steel with few surface defects. [0004] In such a method, however, the amount of scale generated is larger than that of a smooth slab immediately after the slab is extracted from the heating furnace. Many of them are removed by the scale breaker on the slab exit side that removes the generated primary scale, and to prevent the roll surface roughening and the accompanying steel plate surface roughening that occurs in the later stage of rough rolling and the former stage of finish rolling. Had the problem that it was impossible. [0005] An object of the present invention is to produce a steel sheet having a good surface stably without roughening not only through rough rolling but also from slab heating to finish rolling. SUMMARY OF THE INVENTION The present invention solves the above-mentioned problems, and heats a continuously cast ferritic stainless steel slab in a heating furnace, and performs rough rolling and finish rolling. In a series of hot rolling for producing a stainless steel sheet, the exit temperature of the heating furnace is set to 1200 to 1300 ° C., the rolling reduction of each pass during the rough rolling is set to 35% or less, and the first half of the finish rolling (F 1 to F 3 stand) ) The rolling reduction of each stand is 30
% And the rolling speed of the final finishing stand is 700 m
The present invention proposes a method for hot rolling a ferritic stainless steel sheet, wherein the rate is not less than / min. Hereinafter, the hot rolling method of the present invention for preventing roughening of ferritic stainless steel will be described in detail. Burning (hereinafter referred to as rough skin) is, for example, CAM
PISIJ Vol. 6 (1996) -1346, this does not occur when the scale can be made thick and uniform, but when the heating temperature is low and the scale is thin, the steel sheet and the roll stick together when rolled. (Rough skin). If the temperature at the exit side of the heating furnace is less than 1200 ° C., the scale thickness on the surface of the steel sheet is so small that seizure occurs between the steel sheet and the roll, which is not preferable. If the temperature exceeds 1300 ° C., linear flaws due to grain boundary cracks of the steel sheet occur, which is not possible. Therefore, in the present invention, the heating furnace outlet side temperature is set to 1200 to 1300 ° C. The reasons for the regulation of rough rolling and finish rolling are as follows. [0009] The roughening of ferritic stainless steel occurs when the rolling reduction of the rough rolling exceeds 35% or the rolling reduction of the finish rolling exceeds 30% and the rolling speed of the final stand of the finish rolling is less than 700 m / min. Easy to occur.
If the rolling reduction exceeds 35% in the rough rolling, it is considered that the scale on the steel sheet surface is sheared, or the scale is cracked to increase the ratio of a new surface of the material, and the ground iron is likely to be in contact with the roll, causing seizure. Therefore, the rolling reduction in each pass of the rough rolling is 35% or less. When the rolling reduction exceeds 30% in finish rolling, seizure occurs for the same reason as in rough rolling.
On the exit side of the final stand, the rolling speed is 700 m / mi.
If it is slower than n, the contact time of the rolled material with the roll becomes longer, and the diffusion time of the metal becomes longer, so that seizure easily occurs. Therefore, the rolling reduction of the finish rolling is 30% or less, and the rolling speed of the final stand of the finish rolling is 700 m / min.
Above. [0011] The content of the ferritic stainless steel is as follows: C: 0.05% or less;
Stainless steel containing 0.3% and Cr: 16 to 20%. Further, Mo: 2.0% or less, Nb: 0.5% or less,
The effect can be obtained even with stainless steel in which rough surface is likely to be generated by adding at least one kind selected from Ti: 0.3% or less. DETAILED DESCRIPTION OF THE INVENTION A thickness 20 having the components shown in Table 1
An example in which hot rolling is performed using a ferrite stainless steel slab having a length of 0 mm, a length of 6 m, and a width of 1300 mm will be described. The rolling mill row of the rolling mill used is shown in FIG. In FIG. 1, a slab heated in a heating furnace 1 is roughly rolled by a rough rolling mill 3 having R 1 to R 3 stands after the scale is peeled off by a scale breaker 2, and then denoted by F 1 to F 7 . It is finish-rolled by a finishing mill 4 having each stand, and is taken up by a down coiler 6 via a run-out table 5. The work roll diameter of the rough rolling mill 3 is 1500 m
m, the work roll diameter of the finishing mill 4 is 820 mm for the F 1 to F 3 stands and 700 mm for the F 4 to F 7 stands. [0013] The ferrite stainless steel slab is
It is heated to 200 ° C. for 2 hours,
A 0 mm slab was rolled to a 30.3 mm thick sheet bar. In the rough rolling stands R 1 and R 2 , three-pass reverse rolling was performed, and in R 3 , one-pass rolling was performed. Thereafter, tandem rolling was performed using a finishing mill 4 having seven stands, and the plate was rolled to a thickness of 3.5 mm. In order to investigate the relationship between the rough rolling conditions and the surface properties of the sheet bar, the heating temperature and the rolling reduction of the rough rolling were changed as shown in Tables 2 and 3. Table 2, the heating temperature (heating furnace exit side temperature), the table showing the finishing mill entry side temperature, rolling reduction and F 1 entry side of the steel sheet (sheet bar) surface texture, Table 3, this in performing the rolling It is a table | surface which shows reduction ratio distribution of rough rolling of invention and conventional conditions. FIG. 2 shows the results. When the heating temperature was higher than 1300 ° C., line flaws were generated, and when the temperature was lower than 1200 ° C., surface roughness was generated. The occurrence of these surface defects did not depend on the setting of the rolling reduction. Moreover, the heating temperature is 1200-1.
Under the condition of 300 ° C., the conditions of the rough rolling reduction, B-1, B-2
No surface roughening was observed when rolling was performed at the rolling reduction setting of, but it was found that roughening occurred at any setting of the rolling reduction under the conventional condition A. When the surface temperature of the sheet bar at a heating temperature of 1200 to 1300 ° C is good, the temperature of the steel sheet on the entrance side of the finishing mill is 1000 to 1100.
° C. Next, an experiment was conducted to examine the finish rolling conditions and the state of the steel sheet surface after the finish rolling. Tables 4 and 5 show the experimental conditions and results. Table 4 shows reduction rate setting, the relationship between the finishing mill final exit side rolling speed and the steel sheet surface texture after rolling completion of the stand F 7. Table 5 is a table showing the reduction ratio distribution of the finish rolling when rolling is performed in Table 4. At this time, the temperature of the steel sheet on the entrance side of the finishing rolling mill was 1050 ° C., and no roughening was observed in the state of the sheet bar. The results are shown in FIG. As a result of the experiment, the steel sheet surface was good under the rolling reduction conditions of P, R, S, and T among the conditions in Table 5 and the rolling speed was 700 m / min or more.
Even if the rolling speed is as low as 690 m / min under the rolling reduction conditions of, or even if the rolling speed is high, the finishing stands F 1 , F 2
It was found that under the condition where the reduction ratio of the sample was 32%, which was a large reduction ratio of Q, skin roughness occurred. [Table 1] [Table 2] [Table 3] [Table 4] [Table 5] As a countermeasure for preventing roughening of a ferritic stainless steel sheet, conventionally, there has been an increase in the heating temperature or care of a slab. However, heating at a high temperature has a problem that line flaws are easily generated. There was a problem that it could not be prevented only by controlling the temperature conditions of the steel sheet, and that even if the slab was cared for, the rough surface could not be completely prevented and the production cost increased. According to the present invention, rolling conditions for rolling ferritic stainless steel can be optimized, and a stable and good steel sheet surface can be obtained.
【図面の簡単な説明】
【図1】実験に用いた熱間圧延設備を示す図である。
【図2】粗圧延パスの最大圧下率とスラブ加熱温度の関
係を示す図である。
【図3】仕上スタンドの最大圧下率と仕上げ圧延機最終
スタンド出側の鋼板速度との関係を示す図である。
【符号の説明】
1 加熱炉
2 スケールブレーカ
3 粗圧延機
4 仕上げ圧延機
5 ランアウトテーブル
6 ダウンコイラBRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a view showing a hot rolling facility used in an experiment. FIG. 2 is a diagram showing a relationship between a maximum rolling reduction of a rough rolling pass and a slab heating temperature. FIG. 3 is a diagram showing the relationship between the maximum draft of a finishing stand and the speed of a steel sheet on the exit side of a final stand of a finishing mill. [Description of Signs] 1 Heating furnace 2 Scale breaker 3 Rough rolling mill 4 Finish rolling mill 5 Run-out table 6 Down coiler
───────────────────────────────────────────────────── フロントページの続き (72)発明者 今江 敏夫 千葉県千葉市中央区川崎町1番地 川崎 製鉄株式会社 技術研究所内 (72)発明者 鑓田 征雄 千葉県千葉市中央区川崎町1番地 川崎 製鉄株式会社 技術研究所内 (56)参考文献 特開 昭63−162818(JP,A) 特開 昭57−22802(JP,A) 特開 平9−25516(JP,A) 特開 平9−137230(JP,A) 特開 平8−300006(JP,A) 特開 平10−17938(JP,A) (58)調査した分野(Int.Cl.7,DB名) B21B 1/00 - 3/02 ──────────────────────────────────────────────────の Continuing from the front page (72) Inventor Toshio Ima 1 Kawasaki-cho, Chuo-ku, Chiba-shi, Chiba Kawasaki Steel Engineering Co., Ltd. (72) Inventor Yasuo Yarida 1 Kawasaki-cho, Chuo-ku, Chiba-shi, Chiba Kawasaki Steel (56) References JP-A-63-162818 (JP, A) JP-A-57-22802 (JP, A) JP-A-9-25516 (JP, A) JP-A-9-137230 (JP JP, A) JP-A-8-300006 (JP, A) JP-A-10-17938 (JP, A) (58) Fields investigated (Int. Cl. 7 , DB name) B21B 1/00-3/02
Claims (1)
のスラブを、加熱炉で加熱し、粗圧延、仕上げ圧延を行
い、ステンレス鋼板を製造する一連の熱間圧延におい
て、加熱炉出側温度を1200〜1300℃とし、粗圧
延時の各パスの圧下率を35%以下で粗圧延した後、仕
上げ圧延の前半(F1 〜F3 )の各スタンドの圧下率を
30%以下、仕上げ最終スタンドの圧延速度を700m
/min以上で仕上圧延することを特徴とするフェライ
ト系ステンレス鋼板の圧延方法。(57) [Claims 1] In a series of hot rolling, a continuous cast ferritic stainless steel slab is heated in a heating furnace, rough-rolled and finish-rolled to produce a stainless steel sheet. After setting the exit temperature of the heating furnace to 1200 to 1300 ° C. and performing rough rolling at a rolling reduction of 35% or less during rough rolling, the rolling reduction of each stand in the first half (F 1 to F 3 ) of finish rolling is performed. 30% or less, rolling speed of the final finishing stand is 700m
A method for rolling a ferritic stainless steel sheet, comprising finish-rolling at a rate of not less than / min.
Priority Applications (1)
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JP15703497A JP3496459B2 (en) | 1997-06-13 | 1997-06-13 | Rolling method of ferritic stainless steel sheet |
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Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15703497A JP3496459B2 (en) | 1997-06-13 | 1997-06-13 | Rolling method of ferritic stainless steel sheet |
Publications (2)
Publication Number | Publication Date |
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JPH115103A JPH115103A (en) | 1999-01-12 |
JP3496459B2 true JP3496459B2 (en) | 2004-02-09 |
Family
ID=15640754
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JP15703497A Expired - Fee Related JP3496459B2 (en) | 1997-06-13 | 1997-06-13 | Rolling method of ferritic stainless steel sheet |
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Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
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KR20030048810A (en) * | 2001-12-13 | 2003-06-25 | 주식회사 포스코 | Method for Manufacturing Hot-Rolled Ferrite Stainless Steel Sheet |
CN104785521A (en) * | 2015-04-21 | 2015-07-22 | 山东泰山钢铁集团有限公司 | Method and system for rolling 410S ferrite stainless steel |
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1997
- 1997-06-13 JP JP15703497A patent/JP3496459B2/en not_active Expired - Fee Related
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JPH115103A (en) | 1999-01-12 |
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