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JP2013000095A - Emulsified seasoning liquid - Google Patents

Emulsified seasoning liquid Download PDF

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JP2013000095A
JP2013000095A JP2011137317A JP2011137317A JP2013000095A JP 2013000095 A JP2013000095 A JP 2013000095A JP 2011137317 A JP2011137317 A JP 2011137317A JP 2011137317 A JP2011137317 A JP 2011137317A JP 2013000095 A JP2013000095 A JP 2013000095A
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seasoning liquid
content
emulsified seasoning
egg yolk
lactic acid
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JP5758712B2 (en
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Yuko Kurihara
佑子 栗原
Nozomi Miyata
のぞみ 宮田
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Kewpie Corp
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QP Corp
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Abstract

【課題】肉や野菜、パスタ類などの食材と和えて料理に仕上げるための調味液であって、酸の刺激を抑えながら、食材に爽やかでマイルドな酸味を付与し、それを持続させることができる乳化調味液を提供する。
【解決手段】乳酸、卵黄及び食用油脂を含有する乳化状調味液であって、ナトリウム含有量が2〜10%であり、水分活性が0.75〜0.90である乳化液状調味液。
【選択図】 なし
[PROBLEMS] A seasoning liquid for finishing a dish by mixing with ingredients such as meat, vegetables, pasta, etc., and suppressing the stimulation of acid while imparting a fresh and mild acidity to the ingredients and sustaining them. An emulsified seasoning liquid is provided.
An emulsified seasoning liquid containing lactic acid, egg yolk and edible oil and fat, having a sodium content of 2 to 10% and a water activity of 0.75 to 0.90.
[Selection figure] None

Description

本発明は、例えば、肉や野菜、パスタ類などの食材と和えて料理に仕上げるための調味液として用いることができ、酸の刺激を抑えながら、食材に爽やかでマイルドな酸味を付与し、それを持続させることができる乳化調味液に関する。 The present invention, for example, can be used as a seasoning liquid to finish cooking with ingredients such as meat, vegetables, pasta, etc., and gives a fresh and mild acidity to the ingredients while suppressing acid irritation. It is related with the emulsified seasoning liquid which can be maintained.

肉や野菜などの食材に酸味を付与した炒め物や和え物などは、特有の刺激や爽やかさがあることから人気のあるメニューであり、主にマヨネーズや食酢など酸味のある調味料と和えて調理されている。近年では酸味を付与した料理のレパートリーも拡大しており、パスタ料理などのメニューにも用いられるようになってきている。 Stir-fried foods and seasonings that add sourness to ingredients such as meat and vegetables are popular because of their unique irritation and freshness, and are cooked mainly with sour seasonings such as mayonnaise and vinegar. Has been. In recent years, the repertoire of sour-flavored dishes has been expanded, and it has come to be used for menus such as pasta dishes.

このような料理の酸味は、特有の味としてあまり違和感を感じていない消費者がいる一方で、幼児・年少児を含む若年層を中心に、そのような刺激的な酸味を好ましくないものとして感じている消費者も多く存在する。このため、酸味を付与した料理を幅広い消費者に受け入れてもらうためには、酸の刺激を抑えながら、食材に爽やかでマイルドな酸味を付与することが求められている。 While there are consumers who do not feel a sense of incongruity as a peculiar taste, such a sour taste of such dishes is felt as undesirable by such a stimulating sour taste mainly in young people including infants and young children. There are many consumers. For this reason, in order for a wide range of consumers to accept dishes with a sour taste, it is required to impart a refreshing and mild sourness to the ingredients while suppressing acid stimulation.

ところで、惣菜売場などでこのような酸味を付与した料理を提供する場合、調理後に時間が経過してから食することが多いため、喫食時には酸味が弱くなってしまうという問題があった。このような経時変化による酸味の減少を防止するには、酸味を付与する調味料を料理に一定量以上配合する必要があり、この場合、これらの調味料が有する刺激的な酸味が強すぎて好まれないという問題がある。これに対し、これら種々の酸味を付与する調味料を刺激が強すぎない範囲で少量配合しても、今度は充分な酸味を持続させることができないという問題が起こる。つまり、酸の刺激を抑えながら、食材に爽やかでマイルドな酸味を付与し、それを持続させることは困難であった。 By the way, when providing a dish with such acidity at a side dish shop or the like, there is a problem that the acidity is weakened at the time of eating because it is often eaten after a long time after cooking. In order to prevent a decrease in sourness due to such a change over time, it is necessary to add a certain amount or more of a seasoning that imparts sourness. In this case, the stimulating sourness of these seasonings is too strong. There is a problem of not being liked. On the other hand, even if a small amount of these seasonings for imparting various sourness is added within a range where the irritation is not too strong, there is a problem that sufficient acidity cannot be maintained. In other words, it was difficult to impart a refreshing and mild acidity to the food while maintaining the acid stimulation, and to maintain it.

酸味の持続性を維持する方法としては、特許文献1(特開2007−190018)に、酢酸発酵物の濃縮物を含有させることにより、すし飯の酸味のもちを長くする等の呈味を改善する方法、呈味改善したすし飯が提案されている。しかしながら、この方法でも、酸の刺激を抑えながら、食材に爽やかでマイルドな酸味を付与し、それを持続させることは困難であった。 As a method of maintaining sourness persistence, Patent Document 1 (Japanese Patent Application Laid-Open No. 2007-190018) contains a concentrate of an acetic acid fermented product to improve taste such as lengthening the sourness of sushi rice. A sushi rice with improved taste and taste has been proposed. However, even with this method, it was difficult to impart a refreshing and mild sourness to the food while suppressing the stimulation of the acid, and to maintain it.

特開2007−190018号公報JP 2007-190018 A

そこで、本発明の目的は、例えば、肉や野菜、パスタ類などの食材と和えて料理に仕上げるための調味液、酸の刺激を抑えながら、食材に爽やかでマイルドな酸味を付与し、それを持続させることができる乳化調味液を提供するものである。 Therefore, the object of the present invention is to add a refreshing and mild sourness to the ingredients while suppressing the stimulation of acids, for example, a seasoning liquid to finish cooking with ingredients such as meat, vegetables and pasta. An emulsified seasoning liquid that can be sustained is provided.

本発明者等は、上記目的を達成すべく調味液の配合原料等について鋭意研究を重ねた結果、特定の原料を含有し、ナトリウム含量と水分活性を特定範囲に調整した乳化調味液は、食材とからめて使用すると、意外にも酸の刺激を抑えながら、食材に爽やかでマイルドな酸味を付与することができ、しかも、それを持続させることを見出し遂に本発明を完成するに至った。 As a result of intensive studies on the ingredients of the seasoning liquid in order to achieve the above-mentioned object, the inventors of the present invention contain an emulsified seasoning liquid containing a specific raw material and adjusting the sodium content and water activity within a specific range. When used in a tandem manner, it was surprisingly found that a fresh and mild acidity can be imparted to the food while suppressing the stimulation of the acid, and that it has been sustained, and the present invention has been completed.

すなわち、本発明は、
(1)乳酸、卵黄及び食用油脂を含有し、ナトリウム含有量が2〜10%であり、水分活性が0.75〜0.90である乳化調味液、
(2)前記乳酸の含有量(固形分換算)1部に対し、前記卵黄の含有量(固形分換算)が0.1〜50部である(1)記載の乳化調味液、
(3)乳化調味液に対して、乳酸の含有量(固形分換算)が0.01〜3%、卵黄の含有量(固形分換算)が0.01〜15%、食用油脂の含有量が1〜70%である(1)又は(2)記載の乳化調味液、
である。
That is, the present invention
(1) An emulsified seasoning liquid containing lactic acid, egg yolk and edible oil and fat, having a sodium content of 2 to 10% and a water activity of 0.75 to 0.90,
(2) The emulsified seasoning liquid according to (1), wherein the egg yolk content (in terms of solid content) is 0.1 to 50 parts relative to 1 part of the content of lactic acid (in terms of solid content),
(3) With respect to the emulsified seasoning liquid, the content of lactic acid (in terms of solid content) is 0.01 to 3%, the content of egg yolk (in terms of solid content) is 0.01 to 15%, and the content of edible fats and oils is The emulsified seasoning liquid according to (1) or (2), which is 1 to 70%,
It is.

本発明によれば、酸の刺激を抑えながら、食材に爽やかでマイルドな酸味を付与し、それを持続させることができる乳化調味液を提供することができる。したがって、惣菜売場などでこの調味液で例えば、肉や野菜、パスタ類などの食材と和えて仕上げた料理を幅広い消費者に受け入れてもらうことができ、調味液の更なる需要の拡大が期待される。 ADVANTAGE OF THE INVENTION According to this invention, the emulsification seasoning liquid which can provide a refreshing and mild acidity to a foodstuff and can maintain it, suppressing the irritation | stimulation of an acid can be provided. Therefore, a wide range of consumers can accept dishes prepared with ingredients such as meat, vegetables, and pasta using this seasoning liquid at sugar beet departments, and further expansion of demand for seasoning liquid is expected. The

以下本発明を詳細に説明する。なお、本発明において「%」は「質量%」を、「部」は「質量部」を意味する。 The present invention will be described in detail below. In the present invention, “%” means “mass%” and “part” means “part by mass”.

本発明の乳化調味液は、例えば、肉や野菜、パスタ類などの食材と和えて料理に仕上げるための調味液、食用油脂が油滴として水相中に略均一に分散して水中油型の乳化状態が維持された調味料をいう。 The emulsified seasoning liquid of the present invention is, for example, a seasoning liquid for finishing with a food such as meat, vegetables and pasta, and an oil-in-water type in which edible fats and oils are dispersed almost uniformly in the aqueous phase as oil droplets. A seasoning in which the emulsified state is maintained.

本発明の乳化調味液は、乳酸、卵黄及び食用油脂を含有し、ナトリウム含有量が2〜10%、好ましくは2〜6%であり、水分活性が0.75〜0.90であることを特徴とする。このような本発明の乳化調味液は、例えば、肉や野菜、パスタ類などの食材と和えて使用することで、酸の刺激を抑えながら、当該食材に爽やかでマイルドな酸味を付与し、それを持続させることができる。これに対して、卵黄を配合しない乳化調味液、あるいは、食用油脂を配合しない乳化調味液は、酸の刺激が強く爽やかでマイルドな酸味を付与しにくい。また、乳酸を配合せず、酢酸のみを配合した乳化調味液、あるいは、ナトリウム含有量が前記範囲よりも低く水分活性が前記範囲よりも高い乳化調味液は、酸味を持続させにくい。なお、ナトリウム含有量が前記範囲よりも高く水分活性が前記範囲よりも低い乳化調味液は、風味の点から好ましくない。 The emulsified seasoning liquid of the present invention contains lactic acid, egg yolk and edible oil and fat, has a sodium content of 2 to 10%, preferably 2 to 6%, and a water activity of 0.75 to 0.90. Features. Such an emulsified seasoning liquid of the present invention is used in combination with ingredients such as meat, vegetables and pasta, for example, and gives a fresh and mild acidity to the ingredients while suppressing acid stimulation. Can be sustained. On the other hand, an emulsified seasoning liquid that does not contain egg yolk or an emulsified seasoning liquid that does not contain edible oils and fats has a strong acid stimulus and is difficult to impart a fresh and mild acidity. Moreover, the emulsified seasoning liquid which does not mix | blend lactic acid but mix | blended only acetic acid, or the emulsified seasoning liquid whose sodium content is lower than the said range and whose water activity is higher than the said range cannot maintain sourness easily. An emulsified seasoning liquid having a sodium content higher than the above range and a water activity lower than the above range is not preferable from the viewpoint of flavor.

本発明で用いる乳酸としては、天然の乳酸、あるいは合成の乳酸のいずれであっても良いが、一般的に食品に用いられる天然の乳酸、例えば発酵乳酸を用いると良い。市販されている50%発酵乳酸、あるいは乳酸に賦形剤を添加して乾燥させた粉末乳酸などを使用しても良い。 The lactic acid used in the present invention may be either natural lactic acid or synthetic lactic acid, but natural lactic acid generally used in foods, such as fermented lactic acid, may be used. Commercially available 50% fermented lactic acid or powdered lactic acid obtained by adding an excipient to lactic acid and drying it may be used.

乳化調味液に対する乳酸の含有量(固形分換算)は、好ましくは0.01〜3%、より好ましくは0.05〜2%である。乳酸の含有量が前記特定範囲であることにより、マイルドな酸味を付与して持続させる本発明の効果が得られやすい。前記特定範囲外である場合は、本発明の効果が得られにくくなるため好ましくない。 The content (in terms of solid content) of lactic acid with respect to the emulsified seasoning liquid is preferably 0.01 to 3%, more preferably 0.05 to 2%. When the content of lactic acid is in the specific range, the effect of the present invention that imparts and maintains a mild acidity is easily obtained. When it is out of the specific range, the effect of the present invention is hardly obtained, which is not preferable.

また、本発明で用いる前記卵黄としては、例えば、鶏卵を割卵し卵白と分離して得られた生卵黄、当該生卵黄に殺菌処理、冷凍処理、濾過処理、スプレードライ又はフリーズドライ等の乾燥処理、ホスフォリパーゼA1、ホスフォリパーゼA2、ホスフォリパーゼC、ホスフォリパーゼD又はプロテアーゼ等による酵素処理、酵母またはグルコースオキシダーゼ等による脱糖処理、超臨界二酸化炭素処理又は亜臨界二酸化炭素処理等の脱コレステロール処理、食塩又は糖類等の混合処理等の1種または2種以上の処理を施したものを使用することができる。また、卵黄としては、鶏卵を割卵して得られる全卵、もしくは卵黄と卵白とを任意の割合で混合したもの、又はこれらに上述の処理を施したものなどを用いてもよい。このように全卵、あるいは卵黄と卵白を混合したものを使用する場合、卵黄部分が本発明の卵黄に相当する。 Examples of the egg yolk used in the present invention include, for example, raw egg yolk obtained by splitting a chicken egg and separating it from egg white, and sterilizing, freezing, filtering, spray drying, freeze drying, etc. Treatment, Phospholipase A1, Phospholipase A2, Phospholipase C, Phospholipase D or enzyme treatment with protease, desugaring treatment with yeast or glucose oxidase, supercritical carbon dioxide treatment or subcritical carbon dioxide treatment, etc. Those subjected to one or more treatments such as decholesterolization treatment, mixed treatment of salt or saccharide, and the like can be used. Moreover, as an egg yolk, you may use the whole egg obtained by dividing a chicken egg, what mixed egg yolk and egg white in arbitrary ratios, or what performed the above-mentioned process to these. In this way, when using a whole egg or a mixture of egg yolk and egg white, the egg yolk portion corresponds to the egg yolk of the present invention.

乳化調味液に対する卵黄含有量(固形分換算)は、好ましくは0.01〜15%であり、より好ましくは0.1〜5%である。卵黄の含有量が前記特定範囲であることにより、マイルドな酸味を付与して持続させる本発明の効果が得られやすい。卵黄の配合量が前記特定範囲よりも多い場合、卵黄の風味が強くなりすぎて好ましくなく、前記範囲よりも少ない場合、酸味がたちやすく好ましくない。 The egg yolk content (in terms of solid content) with respect to the emulsified seasoning liquid is preferably 0.01 to 15%, more preferably 0.1 to 5%. When the content of egg yolk is within the specific range, the effect of the present invention that imparts and maintains a mild acidity is easily obtained. When the blending amount of egg yolk is larger than the above specific range, the flavor of egg yolk becomes too strong, which is not preferable.

更に、前記卵黄の含有量(固形分換算)は、前述した乳酸の合計含有量(固形分換算)1部に対し、好ましくは0.1〜50部であり、より好ましくは1〜30部である。乳酸含有量に対する卵黄含有量が前記特定範囲であることにより、マイルドな酸味を付与して持続させる本発明の効果が特に得られ易くなる。 Further, the egg yolk content (in terms of solid content) is preferably 0.1 to 50 parts, more preferably 1 to 30 parts, relative to 1 part of the total content of lactic acid (in terms of solid content) described above. is there. When the egg yolk content with respect to the lactic acid content is within the specific range, the effect of the present invention that imparts and maintains a mild acidity is particularly easily obtained.

また、本発明の乳化調味液に用いる食用油脂としては、トリアシルグリセロール又はジアシルグリセロールを主成分とする脂質のことである。前記本発明の食用油脂としては、従来の乳化調味料で使用される種々の食用油脂であれば特に制限は無く、具体的には、例えば、菜種油、大豆油、コーン油、サフラワー油、ひまわり油、綿実油、ごま油、こめ油、パーム油、パームオレイン、オリーブ油、落花生油、やし油、しそ油、乳脂、牛脂、ラード、魚油等の動植物油又はこれらの精製油、MCT(中鎖脂肪酸トリグリセリド)、エステル交換油等のような化学的あるいは酵素処理等を施して得られる油脂等の1種又は2種以上を組み合わせて含有させることができる。また、これら食用油脂としては、牛乳、生クリーム、バター、チーズ等の乳製品、あるいは、マヨネーズ等の酸性水中油型乳化調味料等の食用油脂を含む原料を配合することにより調味液に含有させてもよい。 The edible fat used in the emulsified seasoning liquid of the present invention is a lipid mainly composed of triacylglycerol or diacylglycerol. The edible fat of the present invention is not particularly limited as long as it is various edible fats and oils used in conventional emulsified seasonings. Specifically, for example, rapeseed oil, soybean oil, corn oil, safflower oil, sunflower Oil, cottonseed oil, sesame oil, rice oil, palm oil, palm olein, olive oil, peanut oil, coconut oil, perilla oil, milk fat, beef tallow, lard, fish oil and other refined oils, MCT (medium chain fatty acid triglyceride) ), Fats and oils obtained by chemical or enzymatic treatment such as transesterified oil, etc., or a combination of two or more thereof. In addition, these edible fats and oils are incorporated into the seasoning liquid by blending raw materials containing edible fats and oils such as milk, fresh cream, butter and cheese, or acidic oil-in-water emulsified seasonings such as mayonnaise. May be.

乳化調味液に対する食用油脂の含有量は、マイルドな酸味が程よく調和した味となる点から、乳化調味液に対して、好ましくは1〜70%、より好ましくは5〜60%である。食用油脂の含有量が前記特定範囲であることにより、マイルドな酸味を付与して持続させる本発明の効果が得られやすい。食用油脂の含有量が前記特定範囲より多い場合、食用油脂特有の風味が強くなりすぎて好ましくなく、前記特定範囲より少ない場合、酸味がたちやすく好ましくない。 The content of the edible oil / fat with respect to the emulsified seasoning liquid is preferably 1 to 70%, more preferably 5 to 60% with respect to the emulsified seasoning liquid, from the point that the mild acidity has a moderately harmonious taste. When the content of the edible oil / fat is within the specific range, the effect of the present invention for imparting and maintaining a mild acidity is easily obtained. When the content of the edible oil / fat is greater than the specific range, the flavor unique to the edible oil / fat is not preferable because it is too strong.

本発明に用いるナトリウムとしては、食用に供し得るナトリウムであればいずれのものでもよく、例えば、塩化ナトリウム、塩化ナトリウムを主成分とする食塩、L−グルタミン酸ナトリウム、5´−イノシン酸ナトリウム、5´−グアニル酸ナトリウム等の調味料や酢酸ナトリウム等を用いることができる。なお、ナトリウム含有量の分析方法は、モール法、原子吸光光度法、原料配合量からのナトリウム換算など、常法により分析することができる。また、本明細書中では、原子吸光光度法を用いて分析した数値を使用した。 The sodium used in the present invention may be any sodium as long as it is edible, for example, sodium chloride, sodium chloride as a main component, sodium L-glutamate, 5'-sodium inosinate, 5 ' -Seasonings, such as sodium guanylate, sodium acetate, etc. can be used. In addition, the analysis method of sodium content can be analyzed by a conventional method, such as the Mohr method, the atomic absorption photometry method, or sodium conversion from the raw material blending amount. Moreover, in this specification, the numerical value analyzed using the atomic absorption photometry method was used.

本発明の乳化調味液の水分活性は上述のように0.75〜0.90であり、このような乳化調味液を肉や野菜、パスタ類などの食材と和えて使用することで、酸の刺激を抑えながら、当該食材に爽やかでマイルドな酸味を付与し、それを持続させることができるが、水分活性が0.86以下であると、マイルドな酸味を付与して持続させる本発明の効果が得られやすく特に好ましい。また、前記水分活性が0.80以上であると食味がよくなることから好ましい。水分活性を前記範囲に調整するには、乳化調味液の食味を考慮し、常法により、水飴、デキストリン、還元デキストリン、サイクロデキストリン、ソルビトール、トレハロース等の糖類、あるいは、食塩等のナトリウム量等により調整すればよい。 The water activity of the emulsified seasoning liquid of the present invention is 0.75 to 0.90 as described above. By using such an emulsified seasoning liquid in combination with ingredients such as meat, vegetables and pasta, While suppressing irritation, the food can be given a refreshing and mild acidity and can be sustained. However, if the water activity is 0.86 or less, the effect of the present invention can be imparted with a mild acidity and sustained. Is particularly preferred because it is easy to obtain. In addition, the water activity is preferably 0.80 or more because the taste is improved. In order to adjust the water activity to the above range, the taste of the emulsified seasoning liquid is taken into consideration, and in accordance with conventional methods, depending on the amount of sugar such as syrup, dextrin, reduced dextrin, cyclodextrin, sorbitol, trehalose, or sodium amount such as salt Adjust it.

本発明の乳化調味液は、上述原料を含有させる他に本発明の効果を損なわない範囲で調味液に通常用いられている各種原料を適宜選択し含有させることができる。例えば、トマト、玉葱、セロリ、人参、マッシュルーム、ピーマン、パセリ等の具材、砂糖、醤油、食塩、グルタミン酸ナトリウム等の調味料、カツオやコンブ等の動植物エキス、水飴、デキストリン、キサンタンガム、ゼラチン等の増粘剤、モノグリセリン脂肪酸エステル、ポリグリセリン脂肪酸エステル、ショ糖脂肪酸エステル、レシチン、リゾレシチン等の乳化材、アスコルビン酸又はその塩、ビタミンE等の酸化防止剤、着色料、香料、甘味料、保存料等の原料が挙げられる。 The emulsified seasoning liquid of the present invention can contain various raw materials that are usually used in the seasoning liquid as long as the effects of the present invention are not impaired, in addition to the above-described raw materials. For example, ingredients such as tomatoes, onions, celery, carrots, mushrooms, peppers, parsley, seasonings such as sugar, soy sauce, salt, sodium glutamate, animal and plant extracts such as bonito and kombu, chickenpox, dextrin, xanthan gum, gelatin, etc. Thickeners, monoglycerin fatty acid esters, polyglycerin fatty acid esters, sucrose fatty acid esters, lecithin, lysolecithin and other emulsifiers, ascorbic acid or salts thereof, antioxidants such as vitamin E, coloring agents, flavorings, sweeteners, storage And raw materials such as materials.

本発明の乳化調味液の製造方法は、特に限定するものではなく、前述した調味料原料を、常法により、混合して製すれば良い。すなわち、まず、乳酸、卵黄、食用油脂、ナトリウム含有原料、調味料、更に、水分活性を調整するための糖類等の原料及び清水等の調味液原料を用意する。次に、これらを攪拌装置付きニーダーに投入し、攪拌しながら混合加熱をして調味料を製する。以上のようにして得られた乳化調味液は、ボトルやパウチ、缶等の容器包装に充填・密封することで容器入りの製品とすることができる。また、必要に応じて冷凍処理等を行ってもよい。 The manufacturing method of the emulsified seasoning liquid of this invention is not specifically limited, What is necessary is just to mix and produce the seasoning raw material mentioned above by a conventional method. That is, first, lactic acid, egg yolk, edible oil and fat, sodium-containing raw materials, seasonings, raw materials such as sugars for adjusting water activity, and seasoning liquid raw materials such as fresh water are prepared. Next, these are put into a kneader equipped with a stirrer and mixed and heated while stirring to produce a seasoning. The emulsified seasoning liquid obtained as described above can be made into a product in a container by filling and sealing in a container package such as a bottle, a pouch or a can. Moreover, you may perform a freezing process etc. as needed.

以下、本発明の乳化調味液の製造方法について、実施例、及び試験例に基づき具体的に説明する。なお、本発明は、これらに限定するものではない。 Hereinafter, the manufacturing method of the emulsified seasoning liquid of this invention is demonstrated concretely based on an Example and a test example. The present invention is not limited to these.

[実施例1]
下記の配合割合に準じ、本発明の乳化調味液を製した。すなわち、二重釜に下記配合割合の原料を入れ、均一になるように混合しながら90℃まで加熱した後冷却することにより、乳化調味液を製した。得られた乳化調味液の水分活性は0.81であった。また、得られた乳化調味液の乳酸含有量は0.25%、卵黄の含有量(固形分換算)は1%、食用油脂含有量は40%、ナトリウム含有量は4%であった。また、乳酸含有量1部に対して、卵黄含有量が4部、食用油脂含有量が160部、ナトリウムが含有量16部であった。
[Example 1]
The emulsified seasoning liquid of the present invention was manufactured according to the following blending ratio. That is, an emulsified seasoning liquid was prepared by putting raw materials in the following blending ratio into a double kettle, heating to 90 ° C. with uniform mixing, and then cooling. The water activity of the obtained emulsified seasoning liquid was 0.81. Moreover, the lactic acid content of the obtained emulsified seasoning liquid was 0.25%, the egg yolk content (in terms of solid content) was 1%, the edible fat content was 40%, and the sodium content was 4%. Moreover, egg yolk content was 4 parts, edible fat and oil content was 160 parts, and sodium content was 16 parts with respect to 1 part of lactic acid content.

<実施例1のソースの配合割合>
キサンタンガム 0.1%
砂糖 3%
グルタミン酸ナトリウム 5%
食塩 10%
サラダ油 40%
発酵乳酸(酸度50%) 0.5%
生卵黄 2%
醸造酢(酸度4%) 10%
清水 残余
――――――――――――――――
合計 100%
<Combination ratio of sauce of Example 1>
Xanthan gum 0.1%
3% sugar
Sodium glutamate 5%
Salt 10%
40% salad oil
Fermented lactic acid (acidity 50%) 0.5%
Raw egg yolk 2%
Brewing vinegar (acidity 4%) 10%
Shimizu Residue ――――――――――――――――
Total 100%

[比較例1]
実施例1において、乳酸を配合せず、代わりに食酢を配合した以外は同様にして乳化調味液を調製した。
[Comparative Example 1]
In Example 1, an emulsified seasoning liquid was prepared in the same manner except that lactic acid was not blended and vinegar was blended instead.

[比較例2]
実施例1において、卵黄を配合しなかった以外は同様にして調味液を調製した。
[Comparative Example 2]
A seasoning liquid was prepared in the same manner as in Example 1 except that egg yolk was not blended.

[比較例3]
実施例1において、食用油脂を配合しなかった以外は同様にして乳化調味液を調整した。
[Comparative Example 3]
In Example 1, an emulsified seasoning liquid was prepared in the same manner except that the edible fat / oil was not blended.

[試験例1]
実施例1、並びに比較例1乃至3の乳化調味液を使用して、下記方法でそれぞれパスタを調製し、パスタの保存後の食味について下記方法で評価した。結果を表2に示す。
[Test Example 1]
Using the emulsified seasoning liquid of Example 1 and Comparative Examples 1 to 3, pasta was prepared by the following method, and the taste after storage of the pasta was evaluated by the following method. The results are shown in Table 2.

<パスタの調製方法>
フライパンに得られた乳化調味液50gを入れて加熱し、これに茹でたての温かいスパゲティ300gを加えてよく混ぜてからめパスタを調製した。
<Preparation method of pasta>
A pasta was prepared by adding 50 g of the emulsified seasoning liquid obtained in a frying pan and heating, adding 300 g of hot spaghetti freshly boiled and mixing well.

<保存後の食味の評価方法>
パスタを一食ずつ蓋付きの容器に入れ、20℃の室内に1時間保管した後喫食し、その食味を評価した。
<Method for evaluating taste after storage>
Each pasta was put in a container with a lid, stored in a room at 20 ° C. for 1 hour, and then eaten to evaluate the taste.

Figure 2013000095
Figure 2013000095

表1より、乳酸、卵黄及び食用油脂を含有し、ナトリウム含有量、水分活性が上記数値である乳化調味液(実施例1)を用いた料理は、食材とからめて時間が経過した後に喫食しても、食材に爽やかでマイルドな酸味が維持されており大変好ましいことが理解される。これに対して、乳酸を配合せず、酢酸のみを配合した場合(比較例1)、酸味が弱く好ましくなかった。更に、卵黄を配合しない場合(比較例2)、あるいは、食用油脂を配合しない場合(比較例3)は、酸味がたち好ましくなかった。 From Table 1, the dish using the emulsified seasoning liquid (Example 1) containing lactic acid, egg yolk and edible fats and oils and having the above-mentioned values for the sodium content and water activity is eaten after a lapse of time from the ingredients. However, it is understood that the fresh and mild acidity of the food is maintained, which is very preferable. On the other hand, when lactic acid was not blended but only acetic acid was blended (Comparative Example 1), the acidity was weak and not preferred. Furthermore, when the egg yolk was not blended (Comparative Example 2) or when the edible fat / oil was not blended (Comparative Example 3), the acidity was not preferable.

[試験例2]
実施例1において、ナトリウム含有量、及び水分活性が表2に示す割合となるように食塩含有量を変更した以外は、実施例1と同様の方法で4種類の乳化調味液を製した。次いで、実施例1と同様の方法で、得られた各乳化状調味液を用いてパスタを調製し、保存後の食味について、下記評価基準により評価した。結果を表2に示す。
[Test Example 2]
In Example 1, four types of emulsified seasoning liquids were manufactured by the same method as Example 1 except having changed the salt content so that sodium content and the water activity might become the ratio shown in Table 2. Next, pasta was prepared in the same manner as in Example 1 using each of the obtained emulsified seasonings, and the taste after storage was evaluated according to the following evaluation criteria. The results are shown in Table 2.

パスタの食味の評価基準
A:パスタにマイルドな酸味が感じられ大変好ましいものであった。
B:パスタのマイルドな酸味がやや弱いが問題のない程度であり好ましい。
C:パスタのマイルドな酸味が弱く好ましくない。
D:パスタにマイルドな酸味が感じられず、好ましくない。
Evaluation criteria A of pasta taste : The pasta had a mild acidity and was very preferable.
B: Mild sour taste of pasta is slightly weak, but it is not problematic and preferable.
C: The mild sour taste of pasta is weak and not preferred.
D: The pasta does not feel a mild acidity, which is not preferable.

Figure 2013000095
Figure 2013000095

表2より、ナトリウム含有量が2〜10%であり、水分活性が0.75〜0.90である乳化調味液(試験例2、No.1〜No.3)は、食材とからめて時間が経過した後に喫食しても、食材の爽やかでマイルドな酸味が維持されており大変好ましいことが理解される。一方、ナトリウム含有量が前記範囲よりも低く、また、水分活性が前記範囲よりも高い場合(試験例2、No.4)は、パスタにマイルドな酸味が感じられず、好ましくなかった。 From Table 2, the emulsified seasoning liquid (Test Example 2, No. 1 to No. 3) having a sodium content of 2 to 10% and a water activity of 0.75 to 0.90 is entangled with ingredients and time. It is understood that the refreshing and mild sourness of the food is maintained even if it is eaten after the elapse of time, which is very preferable. On the other hand, when the sodium content was lower than the above range and the water activity was higher than the above range (Test Example 2, No. 4), the pasta did not feel a mild sour taste, which was not preferable.

[試験例3]
実施例1において、乳酸及び卵黄の含有量を表3に示す割合となるように、生卵黄の配合量を変更した以外は、実施例1と同様の方法で5種類の乳化調味液を製した。次いで、実施例1と同様の方法で、得られた各乳化状調味液を用いてパスタを調製し、保存後の食味について、下記評価基準により評価した。結果を表3に示す。
[Test Example 3]
In Example 1, five types of emulsified seasonings were prepared in the same manner as in Example 1 except that the blending amount of raw egg yolk was changed so that the contents of lactic acid and egg yolk became the ratio shown in Table 3. . Next, pasta was prepared in the same manner as in Example 1 using each of the obtained emulsified seasonings, and the taste after storage was evaluated according to the following evaluation criteria. The results are shown in Table 3.

食材の食味の評価基準
A:爽やかでマイルドな酸味であり大変好ましいものであった。
B:やや刺激的な酸味があるが、全体として爽やかでマイルドな酸味であり好ましい。
C:やや刺激的な酸味があり、好ましくない。
D:刺激的な酸味が強く、好ましくない。
Criteria for evaluating the taste of food A: A refreshing, mild acidity and very favorable.
B: Slightly stimulating sourness, but a refreshing and mild sourness as a whole is preferable.
C: A slightly pungent sour taste is not preferable.
D: Strong sour taste is not preferable.

Figure 2013000095
Figure 2013000095

表3より、乳酸1部に対する卵黄含有量(固形分換算)の比率が1〜30部である乳化調味液(試験例3、No.1〜No.4)は、調味液を食材とからめて時間が経過した後に喫食しても、マイルドな酸味が感じられる本発明の効果が特に得られ易く、大変好ましいものとなることが理解される。これに対して、卵黄含有量の比率が0.1〜50部である乳化調味液(試験例3、No.5)は、乳化調味液を食材とからめて時間が経過した後に、やや酸味が弱いが、問題のない範囲であり好ましかった。 From Table 3, the emulsified seasoning liquid (Test Example 3, No. 1 to No. 4) in which the ratio of egg yolk content (solid content conversion) to 1 part of lactic acid is 1 to 30 parts is entangled with the seasoning liquid. It is understood that even if the food is eaten after a lapse of time, the effect of the present invention in which a mild acidity is felt is particularly easily obtained, which is very preferable. On the other hand, the emulsified seasoning liquid (Test Example 3, No. 5) having an egg yolk content ratio of 0.1 to 50 parts has a slightly sour taste after a lapse of time from the emulsified seasoning liquid as a food. It was weak, but there was no problem.

[実施例2]
<炒め物の調製方法>
実施例1、比較例1〜3で得られた調味液を用いて、それぞれ下記方法により炒め物を調製した。まず、フライパンに乳化調味液30gを入れて加熱し、一口大に切った鶏モモ肉100g、5mm幅に切ったゴーヤ80g、パプリカ50gを順に加えてよく炒めて混ぜ、炒め物を調製した。得られた料理を蓋付きの容器に入れ、20℃の室内に1時間保管した後喫食し、その食味を評価したところ、実施例1の調味液を用いて調理した炒め物は、食材とからめて時間が経過した後に喫食しても、食材に爽やかでマイルドな酸味が維持されており大変好ましいものであった。一方、比較例1〜3は食材へマイルドな酸味を付与して持続させる本発明の効果が得られず、好ましくなかった。
[Example 2]
<Method of preparing fried food>
Using the seasonings obtained in Example 1 and Comparative Examples 1 to 3, fried foods were prepared by the following methods. First, 30 g of the emulsified seasoning liquid was put into a frying pan and heated, 100 g of chicken thigh meat cut into bite-sized pieces, 80 g of bitter gourd cut into 5 mm width, and 50 g of paprika were added in order and mixed well to prepare a fried food. The obtained dish was put in a container with a lid, stored in a room at 20 ° C. for 1 hour, and then eaten. The taste was evaluated, and the fried food cooked using the seasoning liquid of Example 1 was entangled with ingredients. Even after eating after a long time, the fresh and mild acidity of the ingredients was maintained, which was very favorable. On the other hand, Comparative Examples 1 to 3 were not preferable because the effect of the present invention for imparting a mild sour taste to the food material and maintaining it was not obtained.

[実施例3]
<サラダの調製方法>
実施例1、比較例1〜3で得られた調味液を用いて、それぞれ下記方法によりサラダを調製した。まず、ボウルに乳化調味液30gを入れ、茹でたブロッコリー150g、剥きエビ100gと混合し、ブロッコリーと剥きエビのサラダを調製した。得られた料理を蓋付きの容器に入れ、20℃の室内に1時間保管した後喫食し、その食味を評価したところ、実施例1の調味液を用いて調理したサラダは、食材とからめて時間が経過した後に喫食しても、食材に爽やかでマイルドな酸味が維持されており大変好ましいものであった。一方、比較例1〜3は食材へマイルドな酸味を付与して持続させる本発明の効果が得られず、好ましくなかった。
[Example 3]
<Method for preparing salad>
Salads were prepared by the following methods using the seasonings obtained in Example 1 and Comparative Examples 1 to 3, respectively. First, 30 g of the emulsified seasoning liquid was put in a bowl and mixed with 150 g of boiled broccoli and 100 g of peeled shrimp to prepare a salad of broccoli and peeled shrimp. The obtained dish was placed in a container with a lid, stored for 1 hour in a room at 20 ° C., and then eaten. The taste was evaluated. The salad prepared using the seasoning liquid of Example 1 was entangled with ingredients. Even when eating after a lapse of time, the fresh and mild acidity of the ingredients was maintained, which was very favorable. On the other hand, Comparative Examples 1 to 3 were not preferable because the effect of the present invention for imparting a mild sour taste to the food material and maintaining it was not obtained.

Claims (3)

乳酸、卵黄及び食用油脂を含有し、ナトリウム含有量が2〜10%であり、水分活性が0.75〜0.90であることを特徴とする乳化調味液。 An emulsified seasoning liquid containing lactic acid, egg yolk and edible oil and fat, having a sodium content of 2 to 10% and a water activity of 0.75 to 0.90. 前記乳酸の含有量(固形分換算)1部に対し、前記卵黄の含有量(固形分換算)が0.1〜50部である請求項1記載の乳化調味液。 The emulsified seasoning liquid according to claim 1, wherein the egg yolk content (in terms of solid content) is 0.1 to 50 parts per 1 part of the content of lactic acid (in terms of solid content). 乳化調味液に対して、乳酸の含有量(固形分換算)が0.01〜3%、卵黄の含有量(固形分換算)が0.01〜15%、食用油脂の含有量が1〜70%である請求項1又は2記載の乳化調味液。 With respect to the emulsified seasoning liquid, the content of lactic acid (in terms of solid content) is 0.01 to 3%, the content of egg yolk (in terms of solid content) is 0.01 to 15%, and the content of edible fats and oils is 1 to 70. The emulsified seasoning liquid according to claim 1 or 2, wherein the emulsified seasoning liquid is%.
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JP2015104332A (en) * 2013-11-29 2015-06-08 キユーピー株式会社 Method for producing stir-fried dish
JP2015154736A (en) * 2014-02-20 2015-08-27 キユーピー株式会社 Acidic oil-in-water type emulsion seasoning
JP5996732B1 (en) * 2015-07-07 2016-09-21 株式会社Mizkan Holdings Seasoning for stewed dishes, cooking method for stewed dishes, seasoning for heated dishes
WO2019009217A1 (en) * 2017-07-04 2019-01-10 株式会社Mizkan Holdings Emulsified liquid seasoning containing ingredient material
CN113383937A (en) * 2021-06-23 2021-09-14 佛山市海天(高明)调味食品有限公司 Method for predicting water activity of food and application thereof
JP7654384B2 (en) 2020-01-07 2025-04-01 キユーピー株式会社 Liquid seasoning

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01141570A (en) * 1987-11-06 1989-06-02 Curtis Barnes Inc Microbiologically stable food and method for its manufacture
JPH0343059A (en) * 1989-07-10 1991-02-25 Kagome Kk Mayonnaise-like food and its production
JPH0349661A (en) * 1989-07-17 1991-03-04 Kagome Kk Mayonnaise-like food and its preparation
JP2004215539A (en) * 2003-01-14 2004-08-05 Q P Corp Oil-in-water emulsified pasta sauce packed in a container
JP2004535793A (en) * 2001-05-03 2004-12-02 ユニリーバー・ナームローゼ・ベンノートシヤープ Edible oil-in-water emulsions with low oil content
JP2010051192A (en) * 2008-08-26 2010-03-11 Q P Corp Acidic oil-in-water emulsified food and use of the same
JP2010051191A (en) * 2008-08-26 2010-03-11 Q P Corp Acidic oil-in-water emulsified food and use of the same
JP2010227070A (en) * 2009-03-30 2010-10-14 Mitsukan Group Honsha:Kk Neutral egg yolk-containing liquid seasoning
JP2011177153A (en) * 2010-03-03 2011-09-15 Q P Corp Method for producing liquid food
JP2011177152A (en) * 2010-03-03 2011-09-15 Q P Corp Seasoned liquid food, and method for producing seasoned solid food using the same
JP2012039954A (en) * 2010-08-19 2012-03-01 Q P Corp Emulsified pasta sauce
JP2012178995A (en) * 2011-02-28 2012-09-20 Q P Corp Method for making bread and rich taste-imparting agent for bread

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01141570A (en) * 1987-11-06 1989-06-02 Curtis Barnes Inc Microbiologically stable food and method for its manufacture
JPH0343059A (en) * 1989-07-10 1991-02-25 Kagome Kk Mayonnaise-like food and its production
JPH0349661A (en) * 1989-07-17 1991-03-04 Kagome Kk Mayonnaise-like food and its preparation
JP2004535793A (en) * 2001-05-03 2004-12-02 ユニリーバー・ナームローゼ・ベンノートシヤープ Edible oil-in-water emulsions with low oil content
JP2004215539A (en) * 2003-01-14 2004-08-05 Q P Corp Oil-in-water emulsified pasta sauce packed in a container
JP2010051192A (en) * 2008-08-26 2010-03-11 Q P Corp Acidic oil-in-water emulsified food and use of the same
JP2010051191A (en) * 2008-08-26 2010-03-11 Q P Corp Acidic oil-in-water emulsified food and use of the same
JP2010227070A (en) * 2009-03-30 2010-10-14 Mitsukan Group Honsha:Kk Neutral egg yolk-containing liquid seasoning
JP2011177153A (en) * 2010-03-03 2011-09-15 Q P Corp Method for producing liquid food
JP2011177152A (en) * 2010-03-03 2011-09-15 Q P Corp Seasoned liquid food, and method for producing seasoned solid food using the same
JP2012039954A (en) * 2010-08-19 2012-03-01 Q P Corp Emulsified pasta sauce
JP2012178995A (en) * 2011-02-28 2012-09-20 Q P Corp Method for making bread and rich taste-imparting agent for bread

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2015039346A (en) * 2013-08-22 2015-03-02 キユーピー株式会社 Sea urchin-containing oil-in-water emulsified sauce
US10306907B2 (en) 2013-11-29 2019-06-04 Kewpie Corporation Acidic oil-in-water type emulsified condiment
WO2015079577A1 (en) * 2013-11-29 2015-06-04 キユーピー 株式会社 Acidic oil-in-water type emulsified seasoning
WO2015080232A1 (en) * 2013-11-29 2015-06-04 キユーピー 株式会社 Acidic oil-in-water type emulsified condiment
JP2015104332A (en) * 2013-11-29 2015-06-08 キユーピー株式会社 Method for producing stir-fried dish
CN105792669A (en) * 2013-11-29 2016-07-20 丘比株式会社 Acidic oil-in-water emulsified seasoning
JP2015154736A (en) * 2014-02-20 2015-08-27 キユーピー株式会社 Acidic oil-in-water type emulsion seasoning
JP5996732B1 (en) * 2015-07-07 2016-09-21 株式会社Mizkan Holdings Seasoning for stewed dishes, cooking method for stewed dishes, seasoning for heated dishes
WO2017006978A1 (en) * 2015-07-07 2017-01-12 株式会社Mizkan Holdings Liquid flavor enhancer, method for cooking by heating, and cooked food product
WO2019009217A1 (en) * 2017-07-04 2019-01-10 株式会社Mizkan Holdings Emulsified liquid seasoning containing ingredient material
JP2019013163A (en) * 2017-07-04 2019-01-31 株式会社Mizkan Holdings Ingredient-containing emulsive liquid seasoning
JP7654384B2 (en) 2020-01-07 2025-04-01 キユーピー株式会社 Liquid seasoning
CN113383937A (en) * 2021-06-23 2021-09-14 佛山市海天(高明)调味食品有限公司 Method for predicting water activity of food and application thereof

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