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JP2012058219A - Gas barrier test universal measuring tool for packaging container - Google Patents

Gas barrier test universal measuring tool for packaging container Download PDF

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JP2012058219A
JP2012058219A JP2010214452A JP2010214452A JP2012058219A JP 2012058219 A JP2012058219 A JP 2012058219A JP 2010214452 A JP2010214452 A JP 2010214452A JP 2010214452 A JP2010214452 A JP 2010214452A JP 2012058219 A JP2012058219 A JP 2012058219A
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flat plate
container
gas
metal
gas inlet
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JP5116053B2 (en
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Shintaro Otani
新太郎 大谷
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Abstract

【課題】ガス導入出管をサンプル設置用平板に溶接固着して一体化した従来の容器測定治具では、使い捨て方式での測定は使用上困難で、サンプル容器と平板を接着剤から脱離する作業の危険性と作業時間を解決するため、平板とガス導入出管を圧着組立式にする治具を提供する。
【解決手段】サンプル設置用平板3と箱型ガス導入出部1を別個に切り離し独立させ、サンプル設置用平板3を箱型ガス導入出部1と押え上蓋2をビスにて圧着しサンプル設置用平板3を組立密着装着し、使い捨て方式での測定をできるようにした。
【選択図】図1
In a conventional container measuring jig in which a gas inlet / outlet pipe is integrated by welding and fixing to a flat plate for sample installation, measurement by a disposable method is difficult to use, and the sample container and the flat plate are detached from the adhesive. In order to solve the work danger and work time, a jig is provided that makes a flat plate and a gas inlet / outlet pipe into a pressure assembly type.
A sample installation flat plate 3 and a box-type gas introduction / extraction part 1 are separately separated and made independent, and the sample installation flat plate 3 is pressure-bonded to a box-type gas introduction / extraction part 1 and a presser upper lid 2 with a screw. The flat plate 3 was assembled and closely attached to enable measurement in a disposable manner.
[Selection] Figure 1

Description

本発明は、あらゆる形状の包装容器のガスバリア試験の接着剤剥離作業による不測の事故発生と相当の作業時間を解決するため、サンプルセット用金属平板とガス導入出ツールを組立式にし、金属平板の取り外しを可能にして使い捨て方式にして包装容器と金属平板の接着剤の剥離作業を省略し、安全かつ時間短縮での測定作業をできるようにしたものである。In order to solve the unexpected accident and the considerable work time due to the adhesive peeling work of the gas barrier test of the packaging container of any shape, the present invention makes the metal plate for sample setting and the gas introducing / extracting tool as an assembly type, It can be removed and made disposable, omitting the peeling operation of the adhesive between the packaging container and the metal flat plate so that the measuring operation can be performed safely and with reduced time.

従来の包装容器のガスバリア試験用測定治具は金属平板に2ケ所の穴を開け金属製ガス導入管と金属製ガス排出管を溶接固着して一体化施したものがある。2ケ所の穴から突起しているガス導入管とガス排出管の回りに試験容器の口径に対応した箇所にエポキシ樹脂を塗布する。塗布されたエポキシ樹脂上に樹脂が固化する前に試験容器の口部を当て、容器を手で支えながら金属平板と試験容器がやや固着するまで保持する。固着作業から数時間後ガスバリア試験用測定治具をガスバリア試験装置に取り付け、試験容器内にキャリアガスを流し、試験容器から透過してきた大気を酸素検出器や水蒸気検出器等でその透過量を測定する。透過量の測定が終了したら、ガスバリア試験用測定治具をガスバリア試験装置から取り外す。そして次の試験容器をガスバリア試験用測定治具に取り付けるには、測定終了容器と金属平板を接着剤から脱離させなければならない。よって従来は、あらゆる形状の包装容器を測定するための平板とガス導入出管隔離型使い切りガスバリア装置治具はなかった。There is a conventional measuring jig for gas barrier test of a packaging container in which two holes are formed in a metal flat plate and a metal gas introduction pipe and a metal gas discharge pipe are welded and fixed integrally. An epoxy resin is applied to a portion corresponding to the diameter of the test container around the gas inlet pipe and the gas outlet pipe protruding from the two holes. Before the resin solidifies on the applied epoxy resin, the mouth of the test container is applied and held until the metal flat plate and the test container are slightly fixed while supporting the container by hand. Several hours after the fixing operation, a gas barrier test measuring jig is attached to the gas barrier test device, a carrier gas is allowed to flow through the test container, and the amount of permeated air is measured with an oxygen detector or water vapor detector. To do. When the measurement of the permeation amount is completed, the gas barrier test measuring jig is removed from the gas barrier test apparatus. In order to attach the next test container to the measurement jig for gas barrier test, the measurement end container and the metal flat plate must be detached from the adhesive. Therefore, conventionally, there has been no flat plate and gas inlet / outlet pipe isolated single-use gas barrier device jig for measuring packaging containers of any shape.

次回の試験容器をガスバリア試験用測定治具に取り付けるには、従来の溶接一体型平板アダプターでは、測定終了容器と金属平板を接着剤から脱離させなければならない。金属平板に塗布されたエポキシ樹脂接着剤と容器に固着したエポキシ樹脂接着剤を切り離す必要があり、ドライヤー等を使用してエポキシ樹脂接着剤に熱を与え、柔らかくし、ナイフ等で剥離させる。このような従来法の一体化型包装容器のガスバリア試験用測定治具では金属平板に固着された試験容器を脱離するには常に不測の事故発生懸念と相当の作業時間が必要であった。本発明はこのような課題を解決するためになされたものである。In order to attach the next test vessel to the gas barrier test measuring jig, in the conventional welded integrated flat plate adapter, the measurement-completed vessel and the metal flat plate must be detached from the adhesive. It is necessary to separate the epoxy resin adhesive applied to the metal flat plate and the epoxy resin adhesive fixed to the container. Heat is applied to the epoxy resin adhesive using a drier or the like, softened, and peeled off with a knife or the like. In such a conventional measuring jig for gas barrier test of an integrated packaging container, there has always been a fear of unexpected accidents and considerable work time to detach the test container fixed to the metal flat plate. The present invention has been made to solve such problems.

試験用測定治具として構成している金属平板と金属製ガス導入管および金属製ガス排出管を最初から別個に切り離し独立させ、サンプルセット用金属平板と箱型ガス導入出部を圧着し密閉した組立式にし、金属平板の取り外しを可能にして使い捨て方式にしたものであり、試験容器はアルミ箔の金属平板の中心に開けられた小穴に接触せず、さらに小さな径のキャリアガス導入管を試験容器内に挿入し、ガス排出口はそのガス導入管とアルミ箔の金属平板の中心に開けられた小穴の空間周囲を利用する。箱型ガス導入出部に水平に圧着設置されたアルミ箔平板の中心に開けられた小穴より、やや大きめの容器の口径に対応した箇所にエポキシ樹脂接着剤を塗布し、試験容器の口部を当て試験容器の底部に重しをのせて、アルミ金属平板に接着する。箱型ガス導入出管部とサンプル設置用金属平板を独立させ、互いを圧着装置組立式にした当発明ガスバリア試験用測定治具により、試験容器取り付け用平板を付け替え用とすることで、使い捨て方式にした。The metal flat plate, metal gas inlet tube, and metal gas outlet tube, which are configured as test jigs for testing, are separated separately from the beginning and made independent, and the metal plate for sample setting and the box-type gas inlet / outlet are crimped and sealed. It is an assembly-type, disposable metal plate that can be removed. The test container does not contact the small hole in the center of the aluminum foil metal plate, and tests a carrier gas inlet tube with a smaller diameter. It is inserted into the container, and the gas outlet uses the space around a small hole opened at the center of the gas introduction pipe and the metal plate of the aluminum foil. Apply epoxy resin adhesive to the location corresponding to the diameter of the slightly larger container from the small hole opened in the center of the aluminum foil flat plate that is horizontally crimped to the box-type gas inlet / outlet. Place a weight on the bottom of the test container and bond it to the aluminum metal plate. Disposal method by replacing the flat plate for attaching the test container with the measuring jig for gas barrier test of the present invention in which the box-type gas introduction / exit pipe part and the metal flat plate for sample installation are made independent and each other is a crimping device assembly type I made it.

アルミ箔等の試験容器サンプル設置用金属平板は、接着剤で接着された測定終了容器サンプルから脱離させる必要がなく、次の試験容器は別のアルミ箔等の金属平板を使用することができるので、接着剤からの脱離作業が不要となり、脱離作業そのものが省くことができる。よって不測の事故発生も減り、脱離作業時間が省略されるので、安全性の高い容器試験ができるようになる。また人手作業時間の短縮と装置稼働時間の改善も大幅に向上できる。つまり安全衛生面、装置稼働時間面に絶大な効果がある。また付け替え用のため常に新品の平板を使用でき、再利用による平板表面の傷からのガスリークの防止、平板とガス導入出管を隔離したことにより、溶接された突起状のガス導入管とガス排出管は不要となり、水平に設置されたアルミ箔板上で試験容器を固着できるので、作業性もよく、エポキシ接着剤の偏った溜まりもなく、個人差の小さい安定した接着強度が得ることができる。よって安定した試験測定結果が提供でき信頼性の高いデータを検出できる。It is not necessary to detach the metal plate for installing the test container sample such as aluminum foil from the measurement-completed container sample bonded with the adhesive, and the next test container can use another metal plate such as aluminum foil. Therefore, the detachment work from the adhesive becomes unnecessary, and the detachment work itself can be omitted. Therefore, the occurrence of unforeseen accidents is reduced and the detachment operation time is omitted, so that a highly safe container test can be performed. In addition, the reduction of manual work time and the improvement of equipment operating time can be greatly improved. In other words, it has a tremendous effect in terms of safety and health and equipment operation time. Also, a new flat plate can always be used for replacement, preventing gas leaks from scratches on the flat plate surface due to reuse, and separating the flat plate from the gas inlet / outlet pipe, so that the welded protruding gas inlet pipe and gas discharge Tubes are not required, and the test container can be fixed on an aluminum foil plate installed horizontally, so that workability is good, there is no uneven accumulation of epoxy adhesive, and stable adhesive strength with little individual difference can be obtained. . Therefore, stable test measurement results can be provided and highly reliable data can be detected.

本発明の使用状態を示す断面図である。It is sectional drawing which shows the use condition of this invention. 本発明の上面図である。It is a top view of the present invention.

まず初めにサンプル設置用穴付きアルミ平板3と測定用サンプル容器7の淵にエポキシ接着剤10を塗布し隙間なく平板の穴に接触しないように接着し、測定用サンプル容器7の底部に重しをのせ塗布した接着剤10が乾くのを待つ。アルミ平板3にサンプル容器7接着したものを箱型ガス導入出部ツール1とその押え蓋2で挟み、取付けネジ11を均等にねじ込み上下0リング4でアルミシート3の端部を圧着密閉する。ガス導入管口5とガス導出管口6をガスバリア測定装置と接続し、箱型ガス導入出部1の内部へガスを供給し、サンプル容器7内へ効率よくガスを送るためにキャリアガス導入延長管9をアルミシート吸排気穴8に通す。サンプル容器7から透過した外部のガスとの混合ガスがアルミシート吸排気穴8から箱型ガス導入出部1、そしてガス導出管口6へと通過してガスバリア透過率測定装置へと送られる。次のサンプル容器7に交換し測定する場合、先のサンプル容器7をアルミ板3と接着状態のまま取付けネジ11をゆるめ、押え上蓋2を外し、箱型ガス導入出部から取り外し、次のサンプル容器7を上記と同様にガス導入出部分ツールへ設置する。アルミシート3端を挟む上下0リング4には、それぞれにアピエゾンTもしくは、グリースを塗布する。押え上蓋2は、排気穴付サンプル設置用アルミシート平板3の端部を圧着密閉する必要があるため中央部くり抜き型のものとすることとする。First, the epoxy adhesive 10 is applied to the ridges of the aluminum flat plate 3 with the sample setting hole and the measurement sample container 7 so as not to come into contact with the hole of the flat plate without any gap, and is placed on the bottom of the measurement sample container 7. Wait for the applied adhesive 10 to dry. The sample container 7 bonded to the aluminum flat plate 3 is sandwiched between the box-type gas introduction / exit tool 1 and its presser lid 2, the mounting screws 11 are screwed in evenly, and the ends of the aluminum sheet 3 are crimped and sealed with the upper and lower 0 rings 4. The gas inlet pipe port 5 and the gas outlet pipe port 6 are connected to the gas barrier measuring device, the gas is supplied to the inside of the box-type gas inlet / outlet part 1, and the carrier gas introduction is extended in order to efficiently send the gas into the sample container 7. The tube 9 is passed through the aluminum sheet intake / exhaust hole 8. The mixed gas with the external gas permeated from the sample container 7 passes from the aluminum sheet intake / exhaust hole 8 to the box-type gas inlet / outlet 1 and the gas outlet pipe port 6 and is sent to the gas barrier permeability measuring device. When changing to the next sample container 7 and measuring, loosen the mounting screw 11 with the previous sample container 7 adhered to the aluminum plate 3, remove the presser lid 2, remove it from the box-type gas inlet / outlet, and remove the next sample The container 7 is installed in the gas introduction / extraction part tool in the same manner as described above. Apiezon T or grease is applied to each of the upper and lower 0 rings 4 sandwiching the end of the aluminum sheet 3. Since the presser upper lid 2 needs to be crimped and sealed at the end portion of the sample-installed aluminum sheet flat plate 3 with the exhaust hole, it is assumed that the presser upper lid 2 is of a center-cut type.

1 箱型ガス導入出部
2 押え上蓋
3 サンプル設置用アルミシート平板
4 ゴム製0リング
5 ガス導入管口
6 ガス導出管口
7 測定用サンプル容器
8 アルミシート吸排気穴
9 キャリアガス導入延長管
10 エポキシ接着剤
11 圧着用取付けネジ
DESCRIPTION OF SYMBOLS 1 Box type gas introduction / extraction part 2 Presser top cover 3 Aluminum sheet flat plate for sample installation 4 Rubber 0 ring 5 Gas introduction pipe port 6 Gas outlet pipe port 7 Sample container for measurement 8 Aluminum sheet intake / exhaust hole 9 Carrier gas introduction extension pipe 10 Epoxy adhesive 11 Mounting screw for crimping

Claims (2)

試験用測定治具として構成している平板とガス導入管およびガス排出管を別個に切り離し独立させ、平板とガス導入出口ツールとを圧着組立式にし、平板を取り外し式にする。試験用容器は、平板に開けた穴に接触せず、ガス導入管を試験用容器内に挿入し、ガス排出は、そのガス導入管と平板に開けられた穴の空間周囲を利用する。ガス導入出ツール部に水平に圧着設置された平板に開けられた穴より、大きめの容器の口径に対応した箇所に接着剤を塗布し、試験用容器の口部を当て、平板に接着する。つまり平板と試験用サンプル容器を接着し、その平板をガス導入管およびガス排出管があるガス導入出口部ツールに圧着組立装着し容器の測定をおこなうことによって、平板を付け替え用とし、測定終了後は、平板と試験用サンプル容器は使い捨て方式とする平板の取り替え方式である。A flat plate, a gas introduction pipe, and a gas discharge pipe that are configured as a test measurement jig are separately separated and made independent, and the flat plate and the gas introduction / exit tool are made into a crimping assembly type, and the flat plate is made to be a detachable type. The test container does not come into contact with the hole formed in the flat plate, the gas introduction tube is inserted into the test container, and the gas discharge uses the space around the hole formed in the gas introduction tube and the flat plate. Adhesive is applied to a location corresponding to the diameter of a larger container through a hole formed in a flat plate that is horizontally crimped and installed on the gas introduction / extraction tool, and the mouth of the test container is applied to adhere to the flat plate. In other words, the flat plate and the test sample container are bonded, and the flat plate is used for replacement by attaching the flat plate to the gas inlet / outlet tool with the gas inlet pipe and gas outlet pipe, and measuring the container. The flat plate and the test sample container are a single plate replacement method. あらゆる形状の容器に適用する測定治具として構成しているアルミ金属平板と金属製ガス導入管および金属製ガス排出管を別個に切り離し独立させ、容器サンプルセット用アルミ金属平板とステンレス製箱型ガス導入出部ツールをゴム0リングとビスと押え上蓋を使用してビスをねじ込むことで圧着組立式にし、サンプル設置用穴付きアルミシート平板の取り外しを可能にして測定終了後の使い捨て方式にしたものである。測定用サンプル容器は、アルミ箔の金属平板の中心に開けられた小穴に接触せず、さらに小さな径の窒素ガス導入管を試験容器内に挿入し、ガス排出口はそのガス導入管とアルミ箔の金属平板の中心に開けられた小穴の空間周囲を利用する。ステンレス製箱型ガス導入出部とその圧着用の押え上蓋をネジで締めこむことにより、上下ゴム0リングでアルミシートを挟み、水平に密着圧着設置されたアルミ箔サンプル設置用アルミシート平板の中心に開けた小穴よりやや大きめの容器の口径に対応した箇所にエポキシ樹脂接着剤を塗布し、測定用サンプル容器の口部を当て測定用サンプル容器の底部に重しをのせて、アルミ金属平板に接着する。金属製ステンレス箱型ガス導入出管部とサンプル設置用アルミ金属平板を独立させて金属製ステンレス箱型ガス導入出管部を本体部と圧着用の蓋に分けてその間に中心部に穴のあいたサンプル設置用アルミ金属平板の端をゴム製0リングにアピエゾンTやグリースを塗布し、上下の0リングでネジを締めて互いのステンレス治具の締付により圧着し挟みこみ、サンプル設置用アルミ平板を接着剤なしの圧着方式でステンレス製箱型押え蓋付きアダプターへ組立式にした当治具により、試験用サンプル容器取り付け用アルミ平板を付け替え用とすることで、アルミ板とそれに接着剤で接着された測定用サンプルを使い捨て方式にした。金属製ステンレス箱型ガス導入出管部とそのふたには、ゴム製0リングをはめ込む溝を設ける。アルミシート押えるための上ふたと金属製ステンレス箱型ガス導入出管部には、互いを圧着するための取付けネジ部を均等に8か所以上ねじ切りしたものを設ける。サンプル設置用アルミシートは、表面が水平で傷がないものを使用する。ステンレス製箱型ガス導入出部ツールのガス導入口とガス排出口は、ユニオンジョイントで接続し、ガスバリア測定装置本体へと接続する。押え上蓋2は、中央部くり抜き型のものとする。Separately and independently separate the aluminum metal flat plate, metal gas introduction pipe and metal gas discharge pipe, which are configured as measuring jigs applicable to containers of all shapes, and the container metal sample set aluminum plate and stainless steel box gas The lead-out tool is a crimp assembly type by screwing a screw using a rubber 0-ring, a screw and a presser upper lid, and it is possible to remove the aluminum sheet flat plate with a hole for sample installation, and a disposable method after the measurement is completed. It is. The sample container for measurement does not contact the small hole opened in the center of the metal plate of the aluminum foil, and a nitrogen gas inlet tube with a smaller diameter is inserted into the test container, and the gas outlet is connected to the gas inlet tube and the aluminum foil. The space around a small hole opened in the center of the metal plate is used. The center of the aluminum sheet flat plate for the installation of aluminum foil samples, which is tightly crimped horizontally by sandwiching the aluminum sheet with the upper and lower rubber 0-rings, by tightening the stainless steel box-type gas inlet / outlet and the presser upper cover with screws Apply epoxy resin adhesive to the location corresponding to the diameter of the container that is slightly larger than the small hole opened in the hole, place the mouth of the measurement sample container on the bottom of the measurement sample container, and place it on the aluminum metal plate. Glue. The metal stainless steel box-type gas inlet / outlet and the aluminum metal flat plate for sample installation are made independent, and the metal stainless steel box-type gas inlet / outlet is divided into a main body and a crimping lid, with a hole in the center. Apply Apiezon T or grease to the end of the aluminum metal flat plate for sample installation on the rubber 0-ring, tighten the screws with the upper and lower 0-rings, and press and hold them by tightening each other's stainless steel jig. By using this jig that has been assembled into an adapter with a stainless steel box-type presser lid using a crimping method without an adhesive, the aluminum plate for attaching the test sample container can be replaced with an aluminum plate and bonded to it with an adhesive. The measured measurement sample was made disposable. The metal stainless steel box type gas inlet / outlet pipe and its lid are provided with a groove for fitting a rubber 0-ring. The upper lid for holding the aluminum sheet and the metal stainless steel box type gas inlet / outlet pipe section are provided with eight or more mounting screw parts for equally crimping each other. The sample installation aluminum sheet should be horizontal and have no scratches. The gas inlet and gas outlet of the stainless steel box-type gas inlet / outlet tool are connected by a union joint and connected to the gas barrier measuring device main body. The presser upper lid 2 is of a center cut-out type.
JP2010214452A 2010-09-06 2010-09-06 Measuring jig for gas barrier testing of packaging containers Active JP5116053B2 (en)

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JP2012058219A true JP2012058219A (en) 2012-03-22
JP5116053B2 JP5116053B2 (en) 2013-01-09

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CN109693938A (en) * 2018-12-14 2019-04-30 汕头市东方科技有限公司 A kind of stir-fry piece machine pot cover automatic handing system
JP2021018165A (en) * 2019-07-22 2021-02-15 株式会社住化分析センター Gas transmitting cell, sample fixing tool, and device and method for measuring transmittance of gas
CN116735793A (en) * 2023-06-06 2023-09-12 南京国环科技股份有限公司 Atmospheric pollution monitoring device and monitoring method

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CN116735793B (en) * 2023-06-06 2023-12-29 南京国环科技股份有限公司 Atmospheric pollution monitoring device and monitoring method

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